Journal of the Korean Chemical Society (대한화학회지)

2024

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2023

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2022

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2021

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2020

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2019

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2018

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2017

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2016

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2015

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2014

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2013

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2012

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2011

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2010

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2009

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2008

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2007

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2006

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2005

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2004

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2003

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2002

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2001

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2000

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1999

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1998

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1997

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1996

Volume 40 Issue 12
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1995

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1994

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1993

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1992

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1991

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1990

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1989

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1988

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1987

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1986

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1985

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1984

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1983

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1982

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1981

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1980

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1979

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1978

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1977

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1976

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1975

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1974

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1973

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1972

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1971

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1970

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1969

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1968

Volume 12 Issue 4
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1967

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1966

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1965

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1964

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1963

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1962

Volume 6 Issue 2
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1961

Volume 5 Issue 1

1957

Volume 4 Issue 1

1954

Volume 3 Issue 1

1952

Volume 2 Issue 1

1949

Volume 1 Issue 1

DOI 출판

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Volume 40 Issue 10

A Study on the Electronic Properties and Redox Reaction of Palladium(Ⅱ) and Platinum(Ⅱ) Alkylsulfoxide Complexes in Aprotic Solvent [Ⅱ]

Choe, Chil Nam;Son, Hyo Youl;Kim, Se Bong 649

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유기 리간드 tetramethylenesulfoxide(TMSO)을 Pd(II)와 Pt(II)의 착물들에 대한 거동을 UV-vis 분광학적, 자기적, 그리고 전기화학적 방법에 의해 조사하였다. 이들 착물들의 스펙트라에서 두 개의 에너지 흡수 띠가 관찰되었다. 결정장 갈라짐 에너지와 스핀 짝지움 에너지 그리고 결합 세기는 착물들의 스펙트라로부터 얻었다. 착물들의 전자적 성질은 비편재화이고, 낮은 스핀 상태임을 알았다. 리간드와 금속들은 강한 결합세기 였다. 이들 착물들은 반자기성 이었다. 착물들의 산화${\cdot}$환원 반응과정은 비수용매 속에서 순환${\cdot}$전압 전류법에 의해 조사하였다. 착물들의 산화${\cdot}$환원 과정은 일전자 일단계 반응이었으며, 확산과 반응 지배적 이었다.
Solid State $^{27}Al$, $^{29}Si$ MAS NMR Spectroscopic Studies on Crystallization of ZSM-5 Synthesized at Low Temperature and Atomospheric Pressure

Yun, Young Ja;Ha, Jae Mok 656

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저온상압법에 의해 Si/Al의 비가 100정도되는 ZSM-5를 합성하였으며 시간 경과에 따른 결정화과정을 $^{27}Al$ 및 $^{29}Si$ MAS NMR spectea 및 FT-IR로 고찰하였다. 저온상압 하에서 합성한 결과 초기 반응물질 및 성분비에 따라 화학적 이동은 기종의 연구와는 다른 경향을 보였으나 반응이 진행됨에 따라 최종 생성물의 화학적 이동은 전형적이 ZSM-5 영역에서 나타나고 있음을 확인하였다. 그리고 국부결함은 소성에 의해 제거되었으며 최종생성물의 XRD 및 SEM의 결과에서도 합성된 물질이 ZSM-5임을 확인하였다.
Kinetic Studies on the Nucleophilic Addition of Thioglycolic Acid to S-Phenyl-S-vinyl-N-p-tosylsulfilimine Derivatives

Kim, Tae Rin;Han, Man So;Pyun, Sang Yong 663

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Vinylsulfilimine(VSI) 유도체($p-OCH_3$, H, p-Cl 및 p-Br)에 대한 thioglycolic acid의 친핵성 첨가반응속도를 자외선 분광법으로 측정하여 넓은 pH 범위에서 적용될 수 있는 속도식을 구하였다. pH에 따른 속도상수의 변화, general base 및 치환기 효과 등을 바탕으로 반응 메카니즘을 제안하였다. 즉 pH3.0 이하에서는 sulfilimine의 질소에 양성자가 먼저 첨가된 다음 중성 thioglycolic acid 분자가 탄소 이중결합에 첨가되고, pH 3.0-9.0 영역에서 thioglycolic acid의 중성분자와 음이온의 첨가가 경쟁적으로 일어나며, pH 9.0 이상에서는 황화 음이온이 첨가되는 전형적인 Michael type의 반응이 진행됨을 알았다.
Synthesis of 4-Pyranone Derivatives and Their Reactivity as Dienophiles in Diels-Alder Reaction

Kim, No-Soo 670

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Chemistry of F₁,F₀-ATPase Inhibitor : Crystal Structure of (-)-Citreoviridin, C₂₃H₃₀O₆·CH₃OH

Suh, Hong-Suk;Huh, Hai-Kyung;Suh, Il-Hwan;Lee, Jin-Ho;Wilcox, Craig S. 674

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Synthesis of Methoxybenzoylbenzisothiazine Derivatives by Gabriel-Colman Rearrangement

Kwon, Soon Kyoung;Park, Myung Sook 678

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