• 제목/요약/키워드: nanometer-size

검색결과 168건 처리시간 0.027초

Microstructure and Third Order Optical Nonlinearities of Ion-Implanted and Thermally Annealed $Cu-SiO_2$ Thin Films

  • 채이;이민영;김현경;문대원
    • Bulletin of the Korean Chemical Society
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    • 제18권8호
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    • pp.886-889
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    • 1997
  • The crystal structure and optical properties of copper nanoparticles, prepared in fused silica by ion-implantation and subsequent heat-treatment, were characterized by X-ray, TEM, linear absorption, and degenerate four-wave mixing (DFWM) technique. The X-ray data show fcc lattice structure of the nanocrystals and their size was measured as 8-20 nanometer by high resolution TEM. Using DFWM, the third-order nonlinear optical coefficient of the Cu-SiO2 thin films was measured as 0.4-1.1×10-8 esu in the surface plasmon resonance absorption region (540-570 nm).

Ultra-fine Grinding Mechanism of Pharmaceutical Additive by Stirred Ball Mill - Consideration of particle size distribution on ground nano-particle

  • Park, Woo-Sik;Choi, Hee-Kyu
    • 대한약학회:학술대회논문집
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    • 대한약학회 2003년도 Proceedings of the Convention of the Pharmaceutical Society of Korea Vol.2-2
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    • pp.234.2-234.2
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    • 2003
  • Recently, the need for ultra-fine particles, especially nano-sized particles has increased in the fields preparing raw powders such as pharmaceutical additive and high value added products in the Nano-Technology processes. Therefore, the research in ultra-fine grinding is very important, especially, in nanometer grinding. In the previous paper, a series of wet grinding experiments using grinding aids using a stirred ball mill have been performed on grinding rate constant based on grinding kinetics. (omitted)

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반응로내 이온주입에 의한 초미세입자의 합성 및 응집제어 (Synthesis and Control of Ultrafine Particles by Ion-Injection in Furnace)

  • 윤진욱;김영원;안강호
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2001년도 춘계학술대회논문집D
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    • pp.91-96
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    • 2001
  • Ultrafine particles have been widely used in many high technology industrial areas. The spherical nonagglomerated and uniform nanometer-size $SiO_{2}$ particles are synthesized by the injection of TEOS vapor, ions and reaction gas in furnace. Ions were generated by Corona discharge electrode and these ions charge $SiO_{2}$ particles. As a result, spherical, nonagglomerated and ultrafine particles are generated in various conditions, it's morphology, charging portion and size distribution are examined by using TEM, ESP and SMPS. As the applied voltage of electrode changes from 0 kV to 5.0 kV, it is observed that the mean diameter of $SiO_{2}$ particle decreases from 94 nm to 42 nm.

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전기적으로 분류 입경의 제어가 가능한 가상 임팩터을 이용한 대기 중 나노 입자의 분류 (Size Classification of Airborne Nanoparticles Using Electrically Tunable Virtual Impactor)

  • 권순명;김용호;박동호;황정호;김용준
    • 한국정밀공학회지
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    • 제26권2호
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    • pp.118-125
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    • 2009
  • This paper reports the size classification of nanoparticles as well as electrical tuning techniques for the cut-off diameter and collection efficiency. Classifying particles < 100 nm in diameter is quite a technical challenge using a virtual impactor with the cut-off diameter being determined geometrically. However, the proposed virtual impactor can classify particles <100 nm and tune the cut-off diameter by electrically accelerating the particles. The cut-off diameter of the proposed device was tuned from 15 to 50nm.

콜로이드 Ag 나노입자 합성시 계면활성제의 영향 (Effect of Surfactant on Synthesis of Colloidal Ag Nanoparticles)

  • 이종국;최남규;서동석
    • 한국재료학회지
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    • 제15권5호
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    • pp.340-347
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    • 2005
  • Silver nanoparticles were synthesized by chemical reduction method from aqueous silver nitrate solution ana hydrazine as a reduction agent. The morphology, particle size and shape were dependent on the mixing method, reaction temperature and time, molar ratio of hydrazine and silver nitrate, the kind of surfactant, and the addition of surfactant. The stability of the colloidal silver was achieved by the adsorption of surfactant molecules onto the particle. Silver nanoparticles have a characteristic absorption maximum at 430 nm under UV irradiation. It was found that the colloid was nanometer m size and formed very stable dispersion of silver. The Ag nanoparticles obtained showed the spherical shape with the size range of 10-30 nm.

금속분말의 고압비틀림 성형시 나노결정화 (Nanocrystallization of Metallic Powders during High Pressure Torsion Processing)

  • 윤승채;곽은정;김택수;홍순익;김형섭
    • 소성∙가공
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    • 제16권5호통권95호
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    • pp.360-363
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    • 2007
  • Microstructure and microhardness of metallic powders of pure copper were studied after high pressure torsion(HPT) processing with 10 turns of die rotation and high pressure of 6 GPa. The grain size of copper decreases drastically after HPT and reaches nanometer size ranges. During HPT, the hardness of consolidates of copper powders increases with increasing the temperature of HPT processing. Examinations of the fracture surfaces indicated evidence of ductile fracture. The results proved that HPT of copper powders has a beneficial effect for homogeneous deformation with reducing grain size.

대기압 반응로 내 코로나 이온을 이용한 나노입자 형상의 제어 (Corona ion Assisted Nano-Particle Morphology Control in an Atmospheric Pressure Furnace Reactor)

  • 안강호;윤진욱;김영원
    • 대한기계학회논문집B
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    • 제26권5호
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    • pp.710-715
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    • 2002
  • The spherical nonagglomerated and uniform nanometer-size SiO$_2$particles are synthesized by the injection of TEOS vapor, irons and reaction gas in a furnace. Ions are generated by corona discharge and these ions charge SiO$_2$particles. As a result, spherical, nonagglomerated and ultrafine particles are generated in various conditions. Their morphology, charging portion and size distribution are examined by using TEM, ESP and SMPS. As the applied voltage of electrode changes from 0 to 5.0 kV, it is observed that the melon diameter of SiO$_2$particle decreases from 94 nm to 42 nm.

L-ascorbic acid가 포집된 BGsome의 특성 및 안정화 효과 (Characteristics of L-Ascorbic Acid Encapsulated BGsome and its Stabilization Effect)

  • 황수연;진병석
    • 한국응용과학기술학회지
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    • 제28권3호
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    • pp.313-320
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    • 2011
  • Encapsulation of L-ascorbic acid(AA) into BGsome was attempted to improve its stability. BGsome is a bio-compatible vesicular system prepared by dispersion of hydrated liquid crystalline phase formed through hydration of 1,3-butylene glycol(BG)-dissolved lecithin with an aqueous solution containing hydrophilic component. The characteristics of AA encapsulated BGsome, such as droplet size, surface charge, and solution appearance, was investigated. The concentration of AA solution had considerable effect on droplet size and surface charge of BGsome. Several tens nanometer droplet made by sonication treatment did not showed any change of size with storage time. Stability of AA was improved by encapsulation into BGsome, which was verified through DPPH test and HPLC assay.

Femtosecond Laser Ablation of Polymer Thin Films for Nanometer Precision Surface Patterning

  • Jun, Indong;Lee, Jee-Wook;Ok, Myoung-Ryul;Kim, Yu-Chan;Jeon, Hojeong
    • 한국표면공학회지
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    • 제49권1호
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    • pp.20-25
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    • 2016
  • Femtosecond laser ablation of ultrathin polymer films on quartz glass using laser pulses of 100 fs and centered at ${\lambda}=400nm$ wavelength has been investigated for nanometer precision thin film patterning. Single-shot ablation craters on films of various thicknesses have been examined by atomic force microscopy, and beam spot diameters and ablation threshold fluences have been determined by square diameter-regression technique. The ablation thresholds of polymer film are about 1.5 times smaller than that of quartz substrate, which results in patterning crater arrays without damaging the substrate. In particular, at a $1/e^2$ laser spot diameter of $0.86{\mu}m$, the smallest craters of 150-nm diameter are fabricated on 15-nm thick film. The ablation thresholds are not influenced by the film thickness, but diameters of the ablated crater are bigger on thicker films than on thinner films. The ablation efficiency is also influenced by the laser beam spot size, following a $w_{0q}{^{-0.45}}$ dependence.