• 제목/요약/키워드: MOD method

검색결과 236건 처리시간 0.028초

Comparison of removal torques between laser-etched and modified sandblasted acid-etched Ti implant surfaces in rabbit tibias

  • Park, Kyung-Soon;Al Awamleh, Abdel Ghani Ibrahim;Cho, Sung-Am
    • The Journal of Advanced Prosthodontics
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    • 제10권1호
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    • pp.73-78
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    • 2018
  • PURPOSE. The purpose of this study was to analyze the effects of two different implant surface treatments on initial bone connection by comparing the Removal Torque Values (RTQs) at 7 and 10 days after chemically modified, sandblasted, large-grit and acid-etched (modSLA), and Laser-etched (LE) Ti implant placements. MATERIALS AND METHODS. Twenty modSLA and 20 LE implants were installed on the left and right tibias of 20 adult rabbits. RTQs were measured after 7 and 10 days in 10 rabbits each. Scanning electron microscope (SEM) photographs of the two implants were observed by using Quanta FEG 650 from the FEI company (Hillsboro, OR, USA). Analyses of surface elements and components were conducted using energy dispersive spectroscopy (EDS, Horiba, Kyoto, Japan). RESULTS. The mean RTQs were $12.29{\pm}0.830$ and $12.19{\pm}0.713$ Ncm after 7 days (P=.928) and $16.47{\pm}1.324$ and $16.17{\pm}1.165$ Ncm after 10 days (P=.867) for LE and modSLA, respectively, indicating no significant inter-group differences. Pore sizes in the LE were $40{\mu}m$ and consisted of numerous small pores, whereas pore sizes in the modSLA were $5{\mu}m$. In the EDS analysis, Ti, O, and C were the only three elements found in the LE surfaces. Na, Ca, Cl, and K were also observed in modSLA, in addition to Ti, O, and C. CONCLUSION. The implants showed no significant difference in biomechanical bond strength to bone in early-stage osseointegration. LE implant can be considered an excellent surface treatment method in addition to the modSLA implant and can be applied to the early loading of the prosthesis clinically.

TFA-MOD 방법에 의한 YBCO 박막제조에서 nano size $Y_2O_3$ 첨가효과 (Effect of nano size $Y_2O_3$ addition on the superconducting properties and microstructure of YBCO thin film prepared by TFA-MOD method.)

  • 박진아;김병주;홍계원;이희균;유재무;김영국
    • 한국초전도ㆍ저온공학회논문지
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    • 제8권3호
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    • pp.13-17
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    • 2006
  • The effect of the addition of the nano size $Y_2O_3$ powder on the microstructurte and superconducting properties of YBCO thin film deposited on LAO single crystalline substrate by TFA-MOD method was studied. Nano size $Y_2O_3$ powder was added to the stoichiometric precursor solution with a cation ratio of Y : Ba . Cu = 1 : 2 : 3 prepared using TFA as chelating agent. Precursor solutions with and without $Y_2O_3$ addition were coated on $LaAlO_3(100)$ single crystalline substrates by dip coating method. Calcination and conversion heat treatments were performed in controlled atmosphere containing moisture Current carrying capacity(Jc) of YBCO film was enhanced about 50% by $Y_2O_3$ doping and it is thought to be due to the better connectivity of YBCO grains and/or the flux pinning by the $Y_2O_3$ particles embedded in YBCO grains.

IKONOS 영상을 이용한 EO-1 Hyperion Hyperspectral 영상자료의 고해상도 구축 (High Resolution Reconstruction of EO-1 Hyperion Hyperspectral Images Using IKONOS Images)

  • 이상훈
    • 대한원격탐사학회지
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    • 제24권6호
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    • pp.631-639
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    • 2008
  • 본 연구에서는 상업용 위성에 탑재된 센서에서 감지된 고해상도의 범색 영상과 다중분광 영상을 이용하여 저해상도의 초분광 영상을 고해상도로 재구축하는 방법을 IKONOS영상과 30-1의 Hyperion 영상에 대한 적용을 통하여 제시하고 있다. 제안된 초분광 영상의 고해상도 재구축은 Lee(2008b)에 의해 개발된 FitPAN-Mod를 기반으로 하여 30m 급의 공간해상도의 초분광 영상을 1m 급의 공간해상도의 범색 영상 수준으로 공간해 상도를 향상시킨다. 본 연구에서는 세 번의 FitPAN-Mod를 사용하는 저해상도의 영상의 고해상도 재구축 과정을 걸쳐 범색 영상의 파장구간에 속하는 초분광 영상의 50개 밴드에 대해 재구축이 이루어졌다. 실험 결과는 재구축된 영상은 시각적 평가에서 실험 대상 지역 내 범색 영상이 갖고 있는 자세한 공간적 구조를 잘 표현하고 있으며 저해상도에서 세부적 위치에 따라 구분하여 표현할 수 없는 지표면의 좁은 밴드대역의 분광특성을 잘 표현하고 있음을 보여준다. 이러한 결과는 제안된 재구축 방법이 현재의 센서 기술로 수집할 수 없는 고해상도의 초분광 영상의 대체 영상을 생성할 수 있는 기술로서 잠재력을 갖고 있음을 보여준다.

MOD 법으로 제작된 Bi3.25La0.75Ti3O12 박막의 강유전 특성 (Ferroelectric Properties of Bi3.25La0.75Ti3O12 Thin Films Prepared by MOD)

  • 김경태;김창일;권지운;심일운
    • 한국전기전자재료학회논문지
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    • 제15권6호
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    • pp.486-491
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    • 2002
  • We have fabricated $Bi_{3.25}La_{0.75}Ti_3O_12$ (BLT) thin films on the Pt/Ti/$SiO_2$/Si substrates using a metalorganic decomposition (MOD) method with annealing temperature from $550^{\circ}C$ to $750^{\circ}C$. The structural properties of BLT films examined by x-ray diffraction (XRD). From XRD analysis. BLT thin films show polycrystalline structure. The layered-perovskite phase was obtained by spin-on films at above $600^{\circ}C$ for 1h. Scanning electron microscopy (SEM) showed uniform surface composed of rodlike grains. The grain size of BLT films increased with increasing annealing temperature. The BLT film annealed at $650^{\circ}C$ was measured to have a dielectric constant of 279, dielectric loss of 1.85(%), remanent polarization of $25.66\mu C/\textrm{cm}^2$, and coercive field of 84.75 kV/cm. The BLT thin films showed little polarization fatigue test up to $3.5{\times}10^9$ bipolar cycling at 5 V and 100 kHz.

Oxide precursor-based MOD processing of YBCO thin films

  • Kim, Young-Kuk;Yoo, Jai-Moo;Ko, Jae-Woong;Chung, Kook-Chae;Heo, Soon-Young
    • 한국초전도ㆍ저온공학회논문지
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    • 제6권4호
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    • pp.5-8
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    • 2004
  • A low cost MOD processing using YBCO oxide powder as a starting precursor was employed for fabrication of YBCO thin films. YBCO oxide is advantageous over metal acetates or TFA salts which are popular starting precursors for conventional MOD-TFA process. YBCO thin films were prepared by oxide-precursor-based MOD process and annealing condition was optimized. The YBCO thin film annealed at 78$0^{\circ}C$ shows no transport $I_c$ and poor microstructure. However, the YBCO thin film annealed at higher temperature shows improvement in microstructure and current transport property. In order to improve critical current, YBCO thin film was prepared by double coating method. YBCO thin film prepared with double coating approach shows enhanced superconducting performance ($I_c$>100A/cm-w).

REBCO 초전도 박막제조를 위한 Fluorine-free MOD 전구체 용액 개발 (Development of Fluorine-free MOD Precursor Solution for fabricating REBCO Superconducting Films)

  • 김병주;임선원;김호진;홍계원;이희균
    • Progress in Superconductivity
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    • 제7권2호
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    • pp.152-157
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    • 2006
  • New precursor solution with dichloroacetic acid (DCA) was developed for fabricating high $J_c$ REBCO film. DCA based-precursor solution was coated on $LaAlO_3$(001) substrate by dip coating method. Processing parameters such as oxygen partial pressure, water vapor, ramping rate and pyrolysis temperature were controlled in order to obtain a good epitaxial film. The film with thickness of 0.5 micrometer was obtained by single coating and no crack was observed at calcined films. Oxygen partial pressure was controlled in the range of $100{\sim}1,000$ ppm and conversion heat treatment was carried out at the temperature range of $705-765^{\circ}C$. A critical transition temperature ($T_c$) of 90 K and a critical transport current density ($J_c$) of $>0.5\;MA/cm^2$ (77 K and self-field) were obtained for the GdBCO film. It is thought that fluorine-free MOD solution using DCA is promising precursor solution for fabricating high quality REBCO films.

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MOD 법으로 제조한 강유전성 SBT 박막에서 하부전극이 유전 및 전기적 특성에 미치는 영향 (Effects of Bottom Electrode to Dielectric and Electrical Properties of MOD Derived Ferroelectric SBT Thin Films)

  • 김태훈;송석표;김병호
    • 한국전기전자재료학회논문지
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    • 제13권8호
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    • pp.694-699
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    • 2000
  • S $r_{0.9}$/B $i_{2.1}$/T $a_{2}$/ $O_{9}$ solutions was synthesized by MOD (metalorganic decomposition) method. SBT thin films with 2000$\AA$ thickness were prepared on Ir $O_2$/ $SiO_2$/Si and Pt/Ti/ $SiO_2$/Si substrates using the spin coating process and then investigated the dielectric and electrical properties of them. In the case of using Ir $O_2$bottom electrode the hysteresis loop was saturated at lower temperature than Pt/Ti electrode but the breakdown phenomenon was occurred at low voltage because of the rough surface morphology and porous microstructure of SBT thin films. As the results of the fatigue and imprint characteristics related to the lifetime and reliability of devices after 10$^{10}$ cycles the fatigue rates were about 10% at the Ir $O_2$and Pt/Ti bottom electrodes. Both SBT thin films with Ir $O_2$ and with Pt/Ti bottom electrodes show a slight tendency to imprint after 10$^{9}$ cycles but do not lead to a failure.e.e.

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MOD 공정에 의한 산화물 완충층 제조 (Fabrication of oxide buffer layers for coated conductors)

  • 김영국;유재무;고재웅;정국채
    • 한국초전도ㆍ저온공학회논문지
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    • 제8권3호
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    • pp.37-40
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    • 2006
  • Oxide buffer layers for YBCO coated conductors were fabricated using MOD processing and development of microstructure and texture were investigated. A $CeO_2$ buffer layers were formed on RABiTS tape. Acetate-based precursor solution was employed to synthesize the precursor solution. Subsequently, the precursor solution was stabilized and modified with triethanolamine. $CeO_2$ precursor gel film was coated and annealed in $Ar/H_2$ atmosphere at high temperature. An annealed $CeO_2$ film shows mixed orientation with high (001) texturing. It was shown that (111) texture of $CeO_2$ layers were enhanced by multiple coating. This degradation was attributed to development of microcracks in the multiply coated $CeO_2$ films. Also discussed are the synthesis and the characterization of $La_2Zr_2O_7$ (LZO) buffer layers on RABiTS tape. A biaxially textured LZO buffer layer was fabricated with MOD processing method using metal alkoxide based precursor solution. It was shown that the LZO film were epitaxially grown on RABiTS tape and crack-free & uniform surface was obtained after annealing in $Ar/H_2$ atmosphere.

Effect of chemically modified precursor solution on MOD-processed YBCO thin films

  • Jaimoo Yoo;Kim, Young-Kuk;Jaewoong Ko;Soonyoung Heo;Hyungsik Chung
    • 한국초전도ㆍ저온공학회논문지
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    • 제5권3호
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    • pp.23-25
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    • 2003
  • Effect of chemically modified precursor solution on YBCO coated conductor prepared by MOD-TFA method was investigated. YBCO thin films were deposited on (l00)-oriented single crystalline LaAlO$_3$ substrates by conventional MOD-TFA process. The microstructures of YBCO thin films contain maze-like patterns. The origin of this microstructure was delineated by compositional inhomogeneity during the pyrolysis process and it was shown that addition of diethanolamine (DEA) improve the microstructure of grown YBCO films. In addition, it was demonstrated that the chemical modification of precursor solution makes no harmful effect on biaxial texture of YBCO thin films.

AutoMod를 활용한 효율적 작업배정에 관한 연구 (A Study on the Job Dispatching using AutoMod)

  • 김봉선;이승무;이석환
    • 대한안전경영과학회:학술대회논문집
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    • 대한안전경영과학회 2007년도 추계학술대회
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    • pp.163-180
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    • 2007
  • The purpose of this paper is to develop an efficient production strategy with changing factors to influence the productivity. The factors would be the number of Multi-Function worker, the method of job dispatching, and lot size. A simulation model has been developed for this study. We used AutoMod simulation and the process activity was animated to follow the flow of process easily. The alternatives have been tested through the simulation model, and the various alternatives is proposed for the efficient production strategy. We hope that the system is applied to similar types of small and medium-sized enterprises to develop an efficient production strategy and to achieve the satisfactory result.

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