• Title/Summary/Keyword: spraying method

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Study on the PVdF Nanofibers and Graphene Oxide Hybrid Membrane (PVdF 나노섬유와 Graphene Oxide 하이브리드막에 관한 연구)

  • Jung, Hyemin;Chen, Weidong;Yang, Woo Seok;Byun, Hongsik
    • Membrane Journal
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    • v.23 no.3
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    • pp.204-210
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    • 2013
  • Recently, many applications with grapheneoxide (GO) have been reported. But GO membrane for water treatment has not been developed. In this study we prepared polyvinylidene difluoride (PVdF) nanofiber/GO hybrid membrane (FG) for the microfiltration application. The PVdF substrate membrane was prepared by using the electrospinning method with a solution of PVdF in N,N-dimethylacetamide (DMAc) and acetone. GO sheets used in this study were prepared by modified Hummer's method. The PVdF/GO hybrid membrane was finally prepared by spraying the GO solution dispersed in ethanol on the PVdF nanofiber. The successfully prepared FG was thoroughly examined by SEM, Raman, contact angle, porometer and UTM, and water-flux was measured with designed cell (Dead-End Cell). From the contact angle results, it was found that the surface of FG membrane was reformed by hydrophilic property and the water permeability was increased about 2.5 times than that of the nascent PVdF membrane, indicating the possible alternative of the commercial MF membrane.

A Simple Method for the Assessment of Fusarium Head Blight Resistance in Korean Wheat Seedlings Inoculated with Fusarium graminearum

  • Shin, Sanghyun;Kim, Kyeong-Hoon;Kang, Chon-Sik;Cho, Kwang-Min;Park, Chul Soo;Okagaki, Ron;Park, Jong-Chul
    • The Plant Pathology Journal
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    • v.30 no.1
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    • pp.25-32
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    • 2014
  • Fusarium head blight (FHB; scab) caused mainly by Fusarium graminearum is a devastating disease of wheat and barley around the world. FHB causes yield reductions and contamination of grain with trichothecene mycotoxins such as deoxynivalenol (DON) which are a major health concern for humans and animals. The objective of this research was to develop an easy seed or seedling inoculation assay, and to compare these assays with whole plant resistance of twenty-nine Korean winter wheat cultivars to FHB. The clip-dipping assay consists of cutting off the coleoptiles apex, dipping the coleoptiles apex in conidial suspension, covering in plastic bag for 3 days, and measuring the lengths of lesions 7 days after inoculation. There were significant cultivar differences after inoculation with F. graminearum in seedling relative to the controls. Correlation coefficients between the lesion lengths of clip-dipping inoculation and FHB Type II resistance from adult plants were significant (r=0.45; P<0.05). Results from two other seedling inoculation methods, spraying and pin-point inoculation, were not correlated with adult FHB resistance. Single linear correlation was not significant between seed germination assays (soaking and soak-dry) and FHB resistance (Type I and Type II), respectively. These results showed that clip-dipping inoculation method using F. graminearum may offer a real possibility of simple, rapid, and reliable for the early screening of FHB resistance in wheat.

Evaluation of Adhesion and Electrical Properties of CNT/PU Topcoat with Different CNT Weight Fraction for Aircraft (탄소나노튜브의 함량에 따른 항공기용 탄소나노튜브/폴리우레탄 탑코트의 접착 및 전기적 특성 평가)

  • Kim, Jong-Hyun;Shin, Pyeong-Su;Kim, So-Yeon;Park, Joung-Man
    • Composites Research
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    • v.33 no.1
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    • pp.1-6
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    • 2020
  • Dispersion and electrical resistance (ER) properties of polyurethane (PU) type topcoat were evaluated using carbon nanotube (CNT) with different CNT weight fraction. CNT was dispersed in PU type topcoat using ultra sonication dispersion method. CNT/PU topcoat was coated on carbon fiber reinforced epoxy composite (CFRC) surface using gravity feed spraying method. Static contact angles of CFRC and CNT/PU topcoat were performed using 4 types of solvents to calculate the work of adhesion between CNT/PU topcoat and CFRC surface. Surface resistance of CNT added PU topcoat was measured to determine CNT dispersion. Adhesion property between CNT/PU topcoat and CFRC was determined via cross hatch cutting test based on ASTM D3359. The optimized condition of CNT weight fraction was found.

Deposition of YBCO Films on Moving Substrate by a Spray Pyrolysis method (분무 열분해 CVD법으로 이동 중인 LaAlO_3(100) 단결정 위에 증착시킨 YBCO 박막의 특성)

  • Kim, Jae-Gun;Hong, Suk-Kwan;Kim, Ho-Jin;Yu, Seok-Koo;Cho, Han-Woo;Ahn, Jin-Hyun;Joo, Jin-Hoo;Lee, Hee-Gyoun;Hong, Gye-Won
    • Progress in Superconductivity
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    • v.8 no.1
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    • pp.93-97
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    • 2006
  • YBCO films were deposited on a moving substrate by a spray pyrolysis method using nitrate aqueous solution as precursors. Deposition was made on $LaAlO_3$(100) single crystal substrate by spraying precursor droplets generated by a concentric nozzle. The cation ratio of precursor solution was Y:Ba:Cu=1:2.65:4.5. The distance between nozzle and substrate was 15 cm. Substrate was transported with a speed ranging from 0.23 cm/min to 0.5 cm/min. Films were deposited at the pressure ranging from 10 Torr to 20 Torr and the deposition temperature was ranged from $740^{\circ}C\;to\;790^{\circ}C$. Oxygen partial pressure was controlled between 1 Tow and S Torr. Superconducting YBCO films were obtained from $740^{\circ}C\;to\;790^{\circ}C$ with an oxygen partial pressure of 3 Torr. Scanning electron microscope(SEM) and X-ray diffraction(XRD) observation revealed that films are smooth and highly texture with(001) plans parallel to substrate plane. Highest Jc was 0.72 $MA/cm^2$ at 77K and self-field for the film with a thickness of 0.15 m prepared at a substrate temperature of $740^{\circ}C$ and $PO_2$=3 Torr.

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Enhancing resistance to major fungal pathogens of Panax ginseng, by BTH-induced systemic resistance (BTH 처리한 배배양 인삼에서 주요 진균병 저항성 증진 효과)

  • Ryu, Hojin
    • Journal of Plant Biotechnology
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    • v.43 no.1
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    • pp.99-103
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    • 2016
  • In perennial ginseng plantations, the effective control of various diseases is one of the most critical factors for increasing yields. Enhancing the resistance to disease through induced systemic resistance (ISR) and anti-microbial activity of beneficial soil bacteria, is currently considered to be a potential promising approach to integrate pathogen management for sustainable agriculture. However, the effective in vitro culture systems for testing ISR in ginseng plants have been rarely reported. In this study, I have successfully developed an in vitro germ-free culture system of Panax ginseng seedling for diverse purposes. With this useful system, we also tested BTH-induced priming effects against Botrytis cinerea and Colletotrichum panacicola. Compared to the drain method for enhancing ISR effects to ginseng seedlings, the direct method of spraying leaves somewhat increased the defense activity to these major fungal pathogens. Consistently, the expression of pathogen related PgPR10 and PgCAT were greatly and rapidly enhanced in the BTH-treated ginseng seedlings by treatment with C. panacicola. Our results revealed that the in vitro culture system can be used for developing eco-friendly and versatile bio-control agents for harmful diseases in ginseng cultivation.

A Study on the high Temperature Properties of the Graded Thermal Barrier Coatings by APS and PAS (APS법으로 제조된 열장벽 피막과 PAS법으로 제조된 열장벽 성형체의 고온 물성에 관한 연구)

  • 강현욱;권현옥;한주철;송요승;홍상희;허성강;김선화
    • Journal of Surface Science and Engineering
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    • v.32 no.2
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    • pp.144-156
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    • 1999
  • Thermal Barrier Coating with Functional Gradient Materials (FGM-TBC) can play an important role to protect the parts from harmful environments in high temperatures such as oxidation, corrosion, and wear and to improve the efficiency of aircraft engine by lowering the surface temperature on turbine blade. FGM-TBC can increase the life spans of product and improve the operating properties. Therfore, in this study the evaluations of mechanical and thermal properties of FGM-TBC such as fatigue, oxidation and wear-resistance at high temperatures have been conducted. The samples of both the TBC with 2, 3, 5 layers (YSZ/NiCrAlY) to be produced by Air Plasma Spray method (APS) and the bulk TBC with 6 layers to be produced by Plasma Assisted Sintering method (PAS) were used. Furthermore, residual stress, bond strength, and thermal conductivity were evaluated. The average thickness of the APS was 500$\mu\textrm{m}$ to 600$\mu\textrm{m}$ and the average thickness of the PAS was 3mm. The hardness number of the top layer of APS was 750 Hv to 810Hv and that of PAS was 950 Hv to 1440Hv. The $ZrO_2$ coating layer of APS was composed of tetragonal structure after spraying as the result of XRD analysis. As shown in the results of the high temperature wear test, the 3 layer coating of APS had the best wear resistance at $800^{\circ}C$ and the 5 layer coating of APS had the best wear resistance at $600^{\circ}C$. But, these coatings had the tendency of the low-temperature softening at $300^{\circ}C$. The main mechanism of wear was the adhesive wear and the friction coefficient of coatings was increased as increasing the test temperatures. A s results of thermal conductivity test, the ${\Delta}T$ of the APS coating was increased as number of layer and the range of thermal conductivity of the PAS was $800^{\circ}C$ to $1000^{\circ}C$.

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Effects of different surface treatments on the shear bond strength of veneering ceramic materials to zirconia

  • Abdullah, Adil Othman;Hui, Yu;Sun, Xudong;Pollington, Sarah;Muhammed, Fenik Kaml;Liu, Yi
    • The Journal of Advanced Prosthodontics
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    • v.11 no.1
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    • pp.65-74
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    • 2019
  • PURPOSE. To evaluate and compare the effect of different materials and techniques on the shear bond strength of veneering ceramic materials to zirconia. MATERIALS AND METHODS. 136 sintered zirconia cubes were prepared and randomly divided into four study groups according to corresponding methods of surface treatment and materials: GLN (grinding followed by laser scanning using Noritake Cerabien ZR), SLN (sandblasting followed by laser scanning using Noritake Cerabien ZR), GLV (grinding followed by laser scanning using VITA VM 9), and SLV (sandblasting followed by laser scanning using VITA VM 9). Spraying technique was performed to coat the core. Profilometer, SEM, XRD, EDS, universal testing machine, and stereomicroscope were used to record surface roughness Ra, surface morphology, phase transformation, elemental compositions, shear bond strength SBS values, and failure types, respectively. Specimens were investigated in unaged (not immersed in artificial saliva) and aged (stored in artificial saliva for a month) conditions to evaluate SBS values. RESULTS. Grinding and GLN as first and second surface treatments provided satisfactory Ra values in both conditions ($1.05{\pm}0.24{\mu}m$, $1.30{\pm}0.21{\mu}m$) compared to sandblasting and other groups (P<.05). The group GLN showed the highest SBS values in both conditions ($30.97{\pm}3.12MPa$, $29.09{\pm}4.17MPa$), while group SLV recorded the lowest ($23.96{\pm}3.60MPa$, $22.95{\pm}3.68Mpa$) (P<.05). Sandblasting showed phase transformation from t-m. Mixed failure type was the commonest among all groups. CONCLUSION. GLN showed to be a reliable method which provided satisfactory bond strength between the veneer ceramic and zirconia. This method might preserve the integrity of fixed dental crowns.

A Study on Mechanical Properties of SM490-TMC Back Plate(40 mm) Steel by SAW Welding (SM490-TMC 후판(40 mm) 강재의 SAW 용접을 통한 기계적 특성 연구)

  • Lee, Soung-Jun
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.22 no.3
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    • pp.88-93
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    • 2021
  • SAW (Submerged Arc Welding) is often used for ship construction or welding pressure vessels and involves spraying a flux in a powder form to a welding site to a certain thickness and continuously supplying electrode wires therein. This welding method enables high current welding up to 1,500 to 3,000 A. Arc efficiency is higher than 95% and the technique allows clean work as it creates less welding fume, which is composed of fine metal oxide particles, and the arc beam is not exposed. In this study, SM490C-TMC thick plates were heterogeneously welded by SAW. Mechanical properties of welds were measured, and welds were assessed macroscopically and for adhering magnetic particles. The following conclusions were drawn. Bending tests showed no spots exploded on sample surfaces or any other defect, and plastic deformation testing confirmed sufficient weld toughness. These results showed the 1F welding method has no shortcomings in terms of bending performance.

Effect of Microbially Induced Calcite Precipitation on Plant Growth (미생물에 의해 생성된 탄산 칼슘 침전이 식물 생장에 미치는 영향)

  • Kim, Tae-Young ;Nawaz, Muhammad Naqeeb;Do, Jinung ;Chong, Song-Hun
    • Journal of the Korean Geotechnical Society
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    • v.39 no.8
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    • pp.41-48
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    • 2023
  • Microbially induced calcite precipitation(MICP) is a novel cementation method meant to enhance soil engineering properties through the use of microorganisms. This study investigates the effect of different MICP concentrations on plant growth. Tall fescue seeds are grown in plant columns filled with Jumunjin sand. Following plant growth, the soil samples are treated with MICP via spraying method. The results indicate that the MICP-treated plants exhibit hampered growth compared with the untreated plants. pH and electrical conductivity(EC) tests are performed to analyze the changes in soil properties by MICP. The MICP-treated soils exhibit a pH = 7, similar to the untreated soil. However, the EC dramatically increases with the increase in the MICP concentration, which leads to an increase in the osmotic pressure of the soil surrounding the plant roots. Eventually, the higher osmotic pressure in MICP-treated soil hinders the absorption of water and nutrients in plant roots, thus inhibiting plant growth.

Selection of Low Toxic Pesticides and Residual Toxicity to Cotesia glomerata (배추나비고치벌 (Cotesia glomerata)에 대한 저독성 약제 및 잔류독성)

  • Choi, Byeong-Ryeol;Lee, Si-Woo;Park, Hyung-Man
    • Korean journal of applied entomology
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    • v.46 no.2
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    • pp.251-259
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    • 2007
  • For the development of integrated pest management system by harmonizing biological and chemical control, some experiments wee carried out to select low toxic pesticides against natural enemies. and their residual toxicity were evaluated. Leaf dipping method, body dipping method, and diet treatment method were set up for the toxicity evaluation against Cotesia glomerata adults. We had tested 46 different pesticides (31 insecticides, 11 fungicides, 4 herbicides) at recommending concentration commonly used to control diamond back moth, disease and up-land weeds in chinese cabbage field. Twenty three insecticides, eleven fungicides, and four herbicides were shown to be low toxic to C. glomerata adults in the treatment of body dipping. After insecticide spraying at recommending dose on the chinese cabbage, we examined residual effect of insecticides by introducing natural enemies on different days. Safety interval for the introduction of C. glomerata adults was established according to the residual toxicity of pesticides. Safe insecticides for the introduction of C. glomerata adults at one day after treatment (DAT) were thiacloprid, acephate, chlorfenapyr, clothianidin and at 3 DAT were imidacloprid, deltamethrin, thiamethoxam, dimethylvinphos, emamectin benzoate.