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An Evaluation of Cast Stainless Steel (CF8M) Fracture Toughness Caused by Thermal Aging at 43$0^{\circ}C$

  • Kwon, Jae-Do;Ihn, Jae-Hyuj;Park, Joong-Cheul;Park, Sung-Jong
    • Journal of Mechanical Science and Technology
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    • v.16 no.7
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    • pp.902-910
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    • 2002
  • Cast stainless steel may experience embrittlement when it is exposed approximately to 300$\^{C}$ for a long period. In the present investigation, the three classes of the thermally-aged CF8M specimen were prepared using an artificially-accelerated aging method. After the specimens were held for 300, 1800 and 3600hrs. at 430$\^{C}$, respectively, the specimens were quenched in water which is at room temperature. Load versus load line displacement curves and J-R curves were obtained using the unloading compliance method. talc values were obtained using the ASTM E813-87 and ASTM E 813-81 methods. In addition to these methods, talc values were obtained using the SZW (stretch zone width) method described in JSME S 001-1981. The results of the unloading compliance method are J$\_$Q/=543.9kJ/㎡ for virgin materials. The values of J$\_$IC/ for the degraded materials at 300, 1800 and 3600hrs. are obtained 369.25kJ/㎡, 311.02kJ/㎡, 276.7kJ/㎡, respectively. The results obtained by the SZW method are compared with those obtained by the unloading compliance method. Both results are quite similar. Through the elastic-plastic fracture toughness test, it is found that the value of loc is decreased with an increase of the aging time.

Procedures and Items for Royal Wedding Ceremonies of Princesses on 『Hwasunongju-garyedeungrok(和順翁主嘉禮謄錄)』 (『화순옹주가례등록(和順翁主嘉禮謄錄)』에 나타난 가례 절차와 물목 연구)

  • Kim, Jiyeon
    • Journal of the Korean Society of Costume
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    • v.65 no.3
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    • pp.131-150
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    • 2015
  • This article studied the procedures and items used in royal princess weddings by examining "Garyedeungrok(嘉禮謄錄)" which describes Princess Hwasun(和順翁主, 1720-1758)'s wedding in 1732. This was the first wedding by a princess during King Yeongjo(英祖)'s reign. Preparation for the wedding was made based on the previous weddings of royal princesses, but it did not follow the old tradition. The wedding costs were cut down, and it was done in a simpler way than before. However, the simplification of elaborate wedding outfits were not part of this change as ceremonial robes such as No-ui(露衣), Jangsam(長衫) and Chopo(綃袍) were used without much alteration. The wedding ceremony of Princess Hwasun shows the transition process from the royal princess wedding ceremony traditions and rituals in the late 17th century to "Gukhonjeongrye", which emerged and became solidified as a new social norm in the 18th century. A legitimate royal princess and a de facto princess from King's concubine were hardly different when it came to their royal outfitting but the disparity in social status between the two was found in the materials used to make clothes for their respective husbands. Princess Hwasun's wedding procedure shown in "Garyedeungrok" is similar to that of "Gukjo-orye-ui(國朝五禮儀)": Napchae(納采), Nappye(納幣), Chinyeong(親迎), Dongroe(同牢), Hyeongugo(見舅姑), Hyeonsadang(見祠堂), and Seojohyeon(壻朝見). But "Garyedeungrok" deals with the procedures of Gantaek(揀擇), Buma-guanrye(駙馬冠禮), and Seonon(宣醞), which are not included in "Gukjo-orye-ui", and also with the process of preparation for wedding items and the information of related people. However, it is hard to learn about its specific shapes and features because it is often restricted to lists such as a list of clothing. Collecting new materials and an in-depth and succeeding study are required in the future.

Investigation of Structural and Optical Properties of III-Nitride LED grown on Patterned Substrate by MOCVD (Patterned substrate을 이용하여 MOCVD법으로 성장된 고효율 질화물 반도체의 광특성 및 구조 분석)

  • Kim, Sun-Woon;Kim, Je-Won
    • Korean Journal of Materials Research
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    • v.15 no.10
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    • pp.626-631
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    • 2005
  • GaN-related compound semiconductors were grown on the corrugated interface substrate using a metalorganic chemical vapor deposition system to increase the optical power of white LEDs. The patterning of substrate for enhancing the extraction efficiency was processed using an inductively coupled plasma reactive ion etching system and the surface morphology of the etched sapphire wafer and that of the non-etched surface were investigated using an atomic force microscope. The structural and optical properties of GaN grown on the corrugated interface substrate were characterized by a high-resolution x-ray diffraction, transmission electron microscopy, atomic force microscope and photoluminescence. The roughness of the etched sapphire wafer was higher than that of the non-etched one. The surface of III-nitride films grown on the hemispherically patterned wafer showed the nano-sized pin-holes that were not grown partially. In this case, the leakage current of the LED chip at the reverse bias was abruptly increased. The reason is that the hemispherically patterned region doesn't have (0001) plane that is favor for GaN growth. The lateral growth of the GaN layer grown on (0001) plane located in between the patterns was enhanced by raising the growth temperature ana lowering the reactor pressure resulting in the smooth surface over the patterned region. The crystal quality of GaN on the patterned substrate was also similar with that of GaN on the conventional substrate and no defect was detected in the interface. The optical power of the LED on the patterned substrate was $14\%$ higher than that on the conventional substrate due to the increased extraction efficiency.

Fabrication of AC4A/$SiC_w$composite by squeeze casting(II) (용탕단조법에 의한 AC4A/$SiC_w$복합재교 제조에 관한 연구(ll)-가압력 및 시효특성-)

  • Mun, Gyeong-Cheol;Lee, Chun-Hui
    • Korean Journal of Materials Research
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    • v.3 no.6
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    • pp.606-613
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    • 1993
  • This was studied about aging characteristic of AC4A/$SiC_{w}$ 10-30v/o reinforced composite. Aging hardenability was decreased $SiC_{w}$ 30% > 10% > 20%. Aging hardening of T6 treatmented composite was higher absolute value than AC4A I/M material. And this results indicated initial hardening phenomenon according to increase $SiC_{w}$ volume fraction. Reinforced effect by pressure was the same effect as before aging treatment and the best condition pressure at 75MPa. Similar to reinforced effect according to $SiC_{w}$ volume fraction was 30 % > 10 % > 20 %. In case of pressure is low, whisker is not break the same time press with base metal after wetting. After it is wetting with base metal, a part transformed or wetting part break and whisker maintain original shape or a part transformed on the otherhand, in case of pressure is high, whisker is break in same time it was not against pressure and whisker's shape is near a polygon or spherical shape.

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A study on the Creep Behavieo of Rene 80 Superalloy (Rene 80초내열 합금의 크리프 거동에 관한 연구)

  • Han, Seong-Ho;Lee, Gi-Ryong;Jo, Chang-Yong;Kim, In-Bae;Kim, Hak-Min
    • Korean Journal of Materials Research
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    • v.3 no.6
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    • pp.575-584
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    • 1993
  • The effects of atmosphere on the creep rupture properties of Ni-base superalloy Ren6 80 were investigated. Creep rupture tests were performed at $760^{\circ}C$, 657MPa and 982%, 157MPa under Ar gas atmospheres. Creep rupture mode and rupture properties (rupture life and elongation) were similar in two different atmospheres under the condition of $760^{\circ}C$, 657MPa. However, the results at $982^{\circ}C$, 157MPa showed different creep rupture mode and life between air and Ar gas atmospheres. In air, it was shown that creep cracks were initiated at surface-exposed grain boundaries and propagated along grain boundaries. In Ar gas atmosphere, the cracks were initiated at inner grain boundaries and coalesced to surface cracks which cause cup-and-cone type fracture. Due to protective oxide layer formation, air test showed longer rupture life than Ar test.

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Crystallographic Site Dependent $^{16}\textrm{O}^{18}\textrm{O}$ Exchange Reaction in Bi-2212 High $\textrm{T}_{\textrm{c}}$ Oxide Superconductors (Bi-2212산화물 고온초전도체의 결정학적 위치에 의존하는 $^{16}\textrm{O}^{18}\textrm{O}$ 교환반응)

  • Kim, Byeong-Guk
    • Korean Journal of Materials Research
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    • v.7 no.2
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    • pp.157-161
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    • 1997
  • The crystallographic site dependent substitution of $^{18}O$ for $^{16}O$ in $Bi_{2}Sr_{2}Ca_{0.8}Y_{0.2}Cu_{2}^{16}O_{8+\delta}$ has heen investigated. In the Kaman spectra of $Bi_{2}Sr_{2}Ca_{0.8}Y_{0.2}Cu_{2}^{16}O_{8+\delta}$ three prominent Raman bands are observed at 297. 464, and $623cm^{-1}$. As the $^{16}O$ arc replaced hy $^{18}O$, all the three bands shift to lower wavewnumbers. The rate of this isotopic shift is similar for the hands at 397 and $464cm^{-1}$. whereas it is quite slower for the hand at $623cm^{-1}$ '['his implys that the $^{16}O-^{18}O$ exchange reaction is crystallographic sites dependent. .Assuming a tetragonal symmetry, we assign the bands at 623. 464, and $297cm^{-1}$ to the vibrations of $O_{pl}(A_{g}),\;O_{ap}\;and\;O_{Bi}$ respectively.

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Fatigue Behavior of 23Cr26Ni Heat Resistant Steel (23Cr26Ni 내열강의 피로 특성)

  • Lee, H.W.;Kwun, S.I.
    • Journal of the Korean Society for Heat Treatment
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    • v.24 no.2
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    • pp.92-98
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    • 2011
  • The influence of the cooling condition after solution treatment on the high temperature fatigue resistance of 23Cr-26Ni heat resistant steel was investigated. Two different cooling conditions were applied to the steel after solution treatment at $1200^{\circ}C$ for 3 hours. One specimen was water quenched immediately after the solution treatment. The other one was furnace cooled at a rate of $0.5^{\circ}C/min$ down to $750^{\circ}C$ after the solution treatment. Then, both specimens were aged at $750^{\circ}C$ for 5 hours. Under two different heat treatment conditions, the low cycle fatigue (LCF) test was performed at $600^{\circ}C$ and room temperature (RT). Only cyclic hardening continued from the beginning until fracture at all strain amplitudes during LCF at $600^{\circ}C$. This phenomenon was attributed to the increase in the dislocation density due to cyclic deformation, which resulted in the interaction between the newly created dislocations and precipitates. Cyclic hardening followed by saturation and cyclic softening was observed at RT. Cyclic softening was attributed to the dislocation annihilation rate exceeding the dislocation generation rate. Other probable factor for cyclic softening was some cavities formed around grain boundaries after 20 cycles. WQ and FC have a similar LCF behavior at RT and $600^{\circ}C$ as shown in the cyclic stress response curves.

An Experimental Study on Estimate of the Optimal Grout Injection Ratio for Stabilization of Mudstone fill (이암 성토지반의 안정화를 위한 최적주입률 산정에 관한 실험적 연구)

  • Lee, Jungsang;Lee, Seungjun;Kim, Yunjoong;Kim, Taesoo;Do, Jongnam;Chun, Byungsik
    • Journal of the Korean GEO-environmental Society
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    • v.13 no.7
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    • pp.31-38
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    • 2012
  • Water glass chemical grouts are primarily used in ground injection projects. Natural and Durable Stabilizer (NDS), Space Grout Rocket (SGR), and other similar materials composing of inorganic accelerating agents with ultra fine cement have been gaining popularity as ground improvement material in South Korea. However, there are questions as to grouting results and environmental issues caused by NDS grout. This study uses the injection method in mudstone embarkment to evaluate the differences in strength, permeability, and optimum injection volume through the use of uniaxial and triaxial compression tests and fish poison tests for NDS and SGR materials. After 28 days, results showed SGR and NDS to have a 50% increase in strength and 50% decrease in permeability with the proper injection rate at 50%.

Difference in Solidification Process between Al-Mg Alloy and Al-Si Alloy in Die-Casting (Al-Mg계 합금과 Al-Si계 합금의 다이캐스팅 응고과정의 차이)

  • Choi, Se-Weon;Kim, Young-Chan;Cho, Jae-Ik;Kang, Chang-Seog;Hong, Sung-Kil
    • Korean Journal of Materials Research
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    • v.22 no.2
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    • pp.82-85
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    • 2012
  • The effect of the alloy systems Al-Mg alloy and Al-Si alloy in this study on the characteristics of die-casting were investigated using solidification simulation software (MAGMAsoft). Generally, it is well known that the casting characteristics of Al-Mg based alloys, such as the fluidity, feedability and die soldering behaviors, are inferior to those of Al-Si based alloys. However, the simulation results of this study showed that the filling pattern behaviors of both the Al-Mg and Al-Si alloys were found to be very similar, whereas the Al-Mg alloy had higher residual stress and greater distortion as generated due to solidification with a larger amount of volumetric shrinkage compared to the Al-Si alloy. The Al-Mg alloy exhibited very high relative numbers of stress-concentrated regions, especially near the rib areas. Owing to the residual stress and distortion, defects were evident in the Al-Mg alloy in the areas predicted by the simulation. However, there were no visible defects observed in the Al-Si alloy. This suggests that an adequate die temperature and casting process optimization are necessary to control and minimize defects when die casting the Al-Mg alloy. A Tatur test was conducted to observe the shrinkage characteristics of the aluminum alloys. The result showed that hot tearing or hot cracking occurred during the solidification of the Al-Mg alloy due to the large amount of shrinkage.

Electrical Switching Characteristics of Ge-Se Thin Films for ReRAM Cell Applications

  • Kim, Jang-Han;Nam, Ki-Hyun;Chung, Hong-Bay
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.08a
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    • pp.343-344
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    • 2012
  • It has been known since the mid 1960s that Ag can be photodissolved in chalcogenide glasses to form materials with interesting technological properties. In the 40 years since, this effect has been used in diverse applications such as the fabrication of relief images in optical elements, micro photolithographic schemes, and for direct imaging by photoinduced Ag surface deposition. ReRAM, also known as conductive bridging RAM (CBRAM), is a resistive switching memory based on non-volatile formation and dissolution of a conductive filament in a solid electrolyte. Especially, Ag-doped chalcogenide glasses and thin films have become attractive materials for fundamental research of their structure, properties, and preparation. Ag-doped chalcogenide glasses have been used in the formation of solid electrolyte which is the active medium in ReRAM devices. In this paper, we investigated the nature of thin films formed by the photo-dissolution of Ag into Ge-Se glasses for use in ReRAM devices. These devices rely on ion transport in the film so produced to create electrically programmable resistance states. [1-3] We have demonstrated functionalities of Ag doped chalcogenide glasses based on their capabilities as solid electrolytes. Formation of such amorphous systems by the introduction of Ag+ ions photo-induced diffusion in thin chalcogenide films is considered. The influence of Ag+ ions is regarded in terms of diffusion kinetics and Ag saturation is related to the composition of the hosting material. Saturated Ag+ ions have been used in the formation of conductive filaments at the solid electrolyte which is the active medium in ReRAM devices. Following fabrication, the cell displays a metal-insulator-metal structure. We measured the I-V characteristics of a cell, similar results were obtained with different via sizes, due to the filamentary nature of resistance switching in ReRAM cell. As the voltage is swept from 0 V to a positive top electrode voltage, the device switches from a high resistive to a low resistive, or set. The low conducting, or reset, state can be restored by means of a negative voltage sweep where the switch-off of the device usually occurs.

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