• Title/Summary/Keyword: XRD analysis

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Temperature Dependent Hall Effect Characteristics of InSb Thin Film (InSb 박막 홀효과의 온도의존성)

  • 이우선;조준호;최권우;김남오;김상용
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.07a
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    • pp.21-24
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    • 2000
  • lnSb temperature dependent hall effect of multilayerd structures were investigated. According to variation of magnetic field measured hall coefficient, Hall mobility, carrier density and hall voltage. For the measurement of electrical properties of hall device, evaperated InSb thin film fabricated with series and parallel multilayers. We found that the XRD analysis of InSb thin film showed good properties at 20$0^{\circ}C$, 60 minutes. Resistance of ohmic contact increased linearly due to increasing current. Some of device fabrication technique and analysis of Hall effect were discussed.

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Ultrasonic Synthesis of CoSe2-Graphene-TiO2 Ternary Composites for High Photocatalytic Degradation Performance

  • Ali, Asghar;Oh, Won-Chun
    • Journal of the Korean Ceramic Society
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    • v.54 no.3
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    • pp.205-210
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    • 2017
  • In this study, we examined the photo-degradation efficiency of $CoSe_2$-Graphene-$TiO_2$ ($CoSe_2-G-TiO_2$) nanocomposites under visible light irradiation using rhodamine B (RhB) as standard dye. $CoSe_2-G-TiO_2$ nanocomposites were synthesized by ultrasonication and characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Raman spectroscopic analysis and UV-Vis absorbance spectra analysis. Our results show that the $CoSe_2-G-TiO_2$ nanocomposite exhibited significant photo degradation efficiency compared to pure $TiO_2$ and $CoSe_2-G$, approximately 85.2% of the rhodamine (Rh B) degraded after 2.5 h. It is concluded that the $CoSe_2-G-TiO_2$ nanocomposite is a promising candidate for use in dye pollutants.

Development of The Magnetic Abrasive Using Barium Ferrite (Ba-Ferrite를 이용한 자기 연마재 개발)

  • 김희남;송승기;정윤중;윤여권;김희원;조상원;심재환
    • Journal of the Korean Society of Safety
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    • v.18 no.2
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    • pp.46-49
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    • 2003
  • The magnetic polishing is the useful method to finish some machinery fabrications by using magnetic power. This method is one of the precision techniques and has m aim for clean technology in the transportation of the pure gas in the clean pipes. The magnetic abrasive polishing method is not so common in the field of machine that it is not known to widely. There are rarely researcher in this field because of non-effectiveness of magnetic abrasive. Therefore, in this paper we deals with the development of the magnetic abrasive with the use of Ba-Ferrite. In this development, abrasive grain WA has been made by using the min bond fabricated at low temperature. And magnetic abrasive powder was fabricated from the Ba-Ferrite which was crushed into 200 mesh. The XRD analysis result shows that only WA abrasive and Ba-Ferrite crystal peaks were detected, explaining that resin bond was not any more to contribute chemical reaction. From SEM analysis, we found that WA abrasive and Ba-Ferrite were strongly bonding with each other.

Effects of RF pulsing and axial magnetic field onionized magnetron sputtering

  • Joo. Junghoon
    • Journal of Korean Vacuum Science & Technology
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    • v.2 no.2
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    • pp.133-138
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    • 1998
  • To enhance the ionization level of I-PVD and reduce the coil voltage two approaches were tried and as a diagnostic, optical emission spectroscopy and impedance analysis of the plasma was done with a range of Ar pressures and RF power along with XRD analysis of deposited Ag films. RF sputtering power was pulsed with various on/off time scales to recover the ICP quenched by sputtered metals. This in average enhances the ionization of the sputtered atoms with 10 ms/10 ms and 100 ms/100ms pulse on/off time duration and gives higher (200) preferred orientation over (111) in deposited Ag films. Secondly, Small axial B field about 8G remarkably reduced RF coil sputtering and showed scaled relationship between RF power and magnetic field strength for optimal process condition. From OES of Ar0 and Ar+, wave-like dispersion structure appeared and reduced the coil voltage about 20% at very weak field strength of 8G. This should be studied further to have nay relation with low mode helicon wave launching.

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Substrate Temperature Effects on Structural and Optical Properties of RF Sputtered CdS Thin Films

  • Hwang, Dong-Hyeon;Choe, Jeong-Gyu;Son, Yeong-Guk
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.08a
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    • pp.218.2-218.2
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    • 2013
  • In this study, CdS thin films were deposited onto glass substrates by radio frequency magnetron sputtering. The films were grown at various substrate temperatures in the range of 100 to $250^{\circ}C$. The effects of substrate temperatures on the structural and optical properties were examined. The XRD analysis revealed that CdS films were polycrystalline and retained the mixed structure of hexagonal wurtzite and cubic phase. The percentages of hexagonal structured crystallites in the films were seen to be increased by increasing substrate temperatures. The film grown at $250^{\circ}C$ showed a relatively high transmittance of 80% in the visible region, with an energy band gap of 2.45 eV. The transmittance date analysis indicated that the optical band gap was closely related to the substrate temperatures.

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Critical evaluation of a Nigerian sub-bituminous coal potential for energy derivation

  • Odeh, Andrew O.
    • Advances in Energy Research
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    • v.4 no.3
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    • pp.203-211
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    • 2016
  • A good understanding of the chemical composition and structural characteristics of a carbonaceous material is essential in conversion processes. Understanding how the composition and structural changes influence the burning behaviour of coal is important when assessing a coal's potential for utilization. To explore the potentials of a typical Nigerian coal, both conventional and advanced analytical techniques such as proximate analysis, ultimate analysis, calorific value, surface area analyser, SEM, FTIR, XRD and SAXS were employed. The results obtained from these characterizations agree favourable well with a typical South African coal that is of enormous contribution to the gross domestic product (GDP) of the nation economy.

이트리아를 이용한 기체상루테늄의 포집특성

  • 박장진;조영현;전관식;신진명;김연구
    • Proceedings of the Korean Nuclear Society Conference
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    • 1997.05b
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    • pp.324-328
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    • 1997
  • 이트리아와 RuO$_2$의 반응특성 및 반응생성물의 고온안정성 등을 DTA(Differential Thermal Analysis), TGA(Thermo-Gravimetric Analysis)를 이용하여 분석하였고 반응생성물은 XRD(X-ray diffractometry)와 XPS(K-ray photoelectron Spectroscopy), 주사 전자현미경를 이용하여 분석하였다. 이트리아와 RuO$_2$의 혼합물은 약 95$0^{\circ}C$ 이상에서 표면이 거친 $Y_2$Ru$_2$O$_{7}$를 형성하였고 생성된 $Y_2$Ru$_2$O$_{7}$은 공기분위기하에서 140$0^{\circ}C$까지 가열하여도 무게변화가 없는 안정한 물질이었다.이었다.

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Studies on the Adsorptive Properties of Korean Kaolin(I) Physico-chemical Properties of Korean Kaolin (국산카올린의 흡착성에 관한 연구(I) 국산카올린의 물성)

  • 이계주;정필조
    • YAKHAK HOEJI
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    • v.29 no.2
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    • pp.96-102
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    • 1985
  • Innovated utilization of Korean kaolins as pharmaceuticals is attempted, for which relevant properties including adsorptive behaviours are observed in connection with their mineralogical structures. In practice, physico-chemical properties are assessed by means of IR, XRD and thermal analysis including DTA, TG and DSC. Elemental analysis of the ore specimens under investigation is carried out in conventional manners. It is found that the chemical compositions are varied significantly with sampling sites and primary classifications. The clay ores thus analyzed are mainly composed of halloysite species. Proper benefication of the raw clays is necessary so that authentic requirements for medicinal use may be satisfied. White-colored premium grade halloysite could be utilized as therapeutics with relative ease after purification. Evidence indicates that gibbsite-like impurities are intercalated between the 1 : 1 layered moieties. Thermal behaviours may be characterized in such a fashion that loss of free water occurs near 100.deg. C and further heatings result in liberation of bound water near 500.deg. C, with subsequent transformation into amorphous metastable entities. Through thermal activation, enhanced pharmaceutical effects could be envisaged.

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Adsorption Characteristics of Hydrogen Sulfide on Iron Hydroxide-based Adsorbent (수산화철계 흡착제의 황화수소 흡착 특성)

  • Ryu, Seung Hyeong;Seo, Youngjoo;Park, Joonwoo;Kim, Shin Dong;Park, Seong Soon
    • Journal of Korea Society of Waste Management
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    • v.34 no.5
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    • pp.468-473
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    • 2017
  • This study was carried out to examine the characteristics of hydrogen sulfide adsorption using an iron hydroxide-based adsorbent. The prepared adsorbent was discussed with regard to its adsorption capacity and analyzed via surface analysis methods to illustrate the physical characteristics of hydrogen sulfide adsorption. As the drying temperature increased, the adsorption capacity of the adsorbent decreased from 29.15wt% to 22.73wt%. The adsorption capacity was decreased as the space velocity increased and showed an adsorption capacity of about 3.65 at $3,157.6h^{-1}$. The effect of sulfur dioxide was to decrease the adsorption capacity from 29.15wt% to 27.94wt%. The adsorbent exhibited the amorphous type in its physical appearance based on XRD and EDS analysis.

The effect of metal composition on the structure and properties of Ti-Cu-N superhard nanocomposite coatings

  • Myung, Hyun S.;Lee, Hyuk M.;Han, Jeon G.
    • Journal of Surface Science and Engineering
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    • v.34 no.5
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    • pp.429-434
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    • 2001
  • Ti-Cu-N nanocomposite films deposited by arc ion plating and magnetron sputter hybrid system with various copper contents. The microstructure and mechanical properties of Ti-Cu-N superhard nanocomposite films depend on the Cu concentration. In X-ray diffraction (XRD) analysis, intensity of TiN (111) and TiN (220) peak decreased and peak broadness increased with increasing the copper contents and Cu peak was not detected. The grain size of films decreased with increasing at%Cu and Transmission Electron Microscopy (TEM) analysis also showed that Ti-Cu-N film containing 1.5at%Cu was composed of very fine (<10nm) nanocrystalline grains. The maximum hardness of Ti-Cu-N (1.5at%Cu) film reached to 45GPa and friction coefficient was measured 0.3.

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