• Title/Summary/Keyword: Simultaneous measurements

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Simultaneous Detection of Tartrazine-Sunset Yellow in Food Samples Using Bioxide/Carbon Paste Microcomposite with Lanthanum and Titanium

  • Nagles, Edgar;Ceroni, Mario;Hurtado, John
    • Journal of Electrochemical Science and Technology
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    • v.11 no.4
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    • pp.421-429
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    • 2020
  • This report describes the simultaneous detection of the two dyes most commonly used in food, tartrazine (TZ) and sunset yellow (SY), based on a microcomposite of carbon paste decorated with La2O3 and TiO2. Anodic currents for SY-TZ were observed at 0.89-1.21 V by cyclic voltammetry (CV) separated with a ΔV of 0.32 V. The increased anodic peak currents compared to that of the unmodified carbon paste electrode were almost 50 and 41% for SY-TZ, respectively. The detection limits with the optimal amount of La2O3-TiO2 were 0.02 and 0.03 µmol/L, respectively. The relative standard deviation (RSD) based on fifty measurements was less than 3%. The versatility and novelty of the sensor were tested with food samples containing these substances and other substances.

Quantitative Measurements of Soot Particles in a Laminar Diffusion Flame Using a LII/LIS Technique (LII/LIS 기법을 이용한 층류확산화염 매연입자의 정량화)

  • Chung, J.W.;Lee, W.;Han, Y.T.;Kim, B.S.;Lee, C.B.;Kim, D.J.;Lee, K.H.
    • 한국연소학회:학술대회논문집
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    • 2002.11a
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    • pp.113-121
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    • 2002
  • The distribution of volume fraction, mean diameter and number density of soot particles are measured quantitatively in a co-flow ethylene diffusion flame using a simultaneous LII/LIS measurement technique. The LII/LIS system and the measured values are, respectively, calibrated and evaluated by comparing to the informations obtained from laser light. extinction/scattering experiments, LII signal shows some sensitivity to the laser light intensity when laser power density exceeds a certain value(threshold). It is also found that there is an optimal laser intensity and a delay time in order to obtain the best result using the simultaneous LII/LIS measurement technique.

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Interlaboratory Study of Sampling and Analysis Techniques for Ambient VOCs under Field Conditions (현장중심의 동시측정을 통한 환경대기 중 휘발성유기화합물의 측정방식 비교 연구)

  • 김기현;김조천;이강웅;허귀석;이병규
    • Journal of Korean Society for Atmospheric Environment
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    • v.16 no.6
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    • pp.685-691
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    • 2000
  • In order to provide basis for an accurate concentration determination of volatile organic compounds(VOCs) in air, four different institutions participated in simultaneous measurements of several VOC species under the experimental scheme of the Measurement and Analysis Division(MAD) of the Korea Society for Atmospheric Environment(KOSAE). Two types of experiments were undertaken by collecting and analyzing ambient air samples from the 7th floor of Natural Science Building, Han Tang University during two day periods of the late May 1998. The first typer of experiment was conducted as five consecutive experiments at 2-hour intervals by two institutions. On the other hand. the second type of experiment was performed as two -10hr sampling by three different institutions. The data obtained from different type of experiments were examined using various statistical approaches. In general, the results of these experiments indicated that the VOC data produced by a number of Korean institutions be fairly agreeable.

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Competition between Phase Separation and Crystallization in a PCL/PEG Polymer Blend Captured by Synchronized SAXS, WAXS, and DSC

  • Chuang Wei-Tsung;Jeng U-Ser;Sheu Hwo-Shuenn;Hong Po-Da
    • Macromolecular Research
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    • v.14 no.1
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    • pp.45-51
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    • 2006
  • We conducted simultaneous, small-angle, X-ray scattering/differential scanning calorimetry (SAXS/DSC) and simultaneous, wide-angle, X-ray scattering (WAXS)/DSC measurements for a polymer blend of poly($\varepsilon$-caprolactone)/poly(ethylene glycol)(PCL/PEG). The time-dependent SAXS/DSC and WAXS/DSC results, measured while the system was quenched below the melting temperature of PCL from a melting state, revealed the competitive behavior between liquid-liquid phase separation and crystallization in the polymer blend. The time-dependent structural evolution extracted from the SAXS/WAXS/DSC results can be characterized by the following four stages in the PCL crystallization process: the induction (I), nucleation (II), growth (III), and late (IV) stages. The influence of the liquid-liquid phase separation on the crystallization of PCL was also observed by phase-contrast microscope and polarized microscope with 1/4$\lambda$ compensator.

A Comparative Study on Simultaneous Adjustment of Geodetic Networks between with $varphi,\lambda$ Coordinates and with X, Y coordinates ($varphi,\lambda$망과 X, Y망의 조정에 관한 비교 연구)

  • 백은기;김원익;최윤수
    • Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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    • v.4 no.1
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    • pp.37-42
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    • 1986
  • This paper deals with comparison of simultaneous geodetic networks between with geographical coordinates and with plane coordinates. The adjustment computation is performed by variation of coordinates. Provisional values for observation equations are computed by extended Guass mid-latitude formula using, official coordinates ($\varphi,\lambda$) in geographical network abjustment, measurements are reduced to plane by origin scale factor (=1.0000) Bessel ellipsoid and unit weight are adopted, and geographical coordinates are projected by Guass conformal double projection. The processing results of a test-network by distances yield the average root mean square error of position 6ㆍ2cm for adjustment with $\varphi,\lambda$ and 5.8cm for adjustment with X, Y. RMSE of discrepancy between two methods is 1.7cm. This result conform to required accracy.

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Simultaneous determination of low molecular weight amines and quaternary ammonium ions by IC/ESI-MS

  • Jung, Joo-Young;Park, Han-Seok;Kim, Kang-Jin
    • Analytical Science and Technology
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    • v.20 no.3
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    • pp.255-260
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    • 2007
  • A new method for the simultaneous determination of low molecular weight amines and quaternary ammonium ions based on the separation by IC with a suppressor and the detection by MS with ESI has been developed. The method has been applied to the analysis of a mixture containing tetramethylammonium ion, tetraethylammonium ion, tetrapropylammonium ion, triethanolamine, trimethylamine and triethylamine. The constituents were separated by isocratic elution using an IonPac CS17 column, a cation-exchange column, and detected by conductivity and mass spectrometry. The newly developed method for the six components demonstrated that the repeatability in terms of relative standard deviation for three measurements was in the range of 0.1-0.5 %. The detection limits were between 0.2 and $0.9{\mu}g/mL$ by the IC/ESI-MS.

Comparison Between Performance of a Sound-Triggered Measurement and an Amplitude-Triggered Measurement in Shaking Table Tests (진동대를 이용한 모바일 진동 계측 기기의 사운드 트리거 계측과 진폭 트리거 계측 성능 비교)

  • Mapungwana, S.T.;Lee, Jong-Ho;Yoon, Sung-Won
    • Journal of Korean Association for Spatial Structures
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    • v.19 no.1
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    • pp.117-126
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    • 2019
  • Micro-Electro-Mechanical Systems (MEMS) sensors have been widely used in Structural Health Monitoring due to their convenience and lower costs in comparison to conventional sensors. Triggered measurements are relevant in events such as earthquakes because unlike continuous measurements, they only record the structural response once an event happens. This is more cost effective and it makes the data more manageable because only the required measurements from the event are recorded. The most common method of triggering is amplitude triggering. However, lower input amplitudes (less than 0.1g) cannot be triggered by using this method. In this paper, sound triggering was introduced to allow triggered measurements for lower input amplitude values. The performance of the sound triggering and amplitude triggering were compared by a series of shaking-table tests. It was seen that sound-triggering method has a wider frequency (0.5~10Hz) and amplitude (0.01~1.0g) range of measurements. In addition, the sound triggering method performs better than the amplitude triggering method at lower amplitudes. The performance of the amplitude triggering, in terms of the triggering being simultaneous improves at higher input amplitudes.

Geocentric parallax measurements of Near-Earth Asteroid using Baselines with domestic small-size observatories (국내 소형천문대 기선을 이용한 근접 소행성 지심시차 측정)

  • Jeong, Eui Oan;Sohn, Jungjoo
    • Journal of the Korean earth science society
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    • v.37 no.7
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    • pp.398-407
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    • 2016
  • We cooperated with four domestic educational astronomical observatories to construct a baseline and perform simultaneous observations to determine the geocentric parallax, distance, and motion of 1036 Ganymed, an Amor asteroid near the Earth. Observations were made on the day when simultaneous observations were possible from September to November 2011. Measured distances of 1036 Ganymed were 0.394 AU on Sept. 26, 0.365 AU on Oct. 11, and 0.340 AU on Oct. 25, respectively, which were within the error range as compared with the measured distances proposed by the US Jet Propulsion Laboratory. The 1036 Ganymed showed a tilting motion during the observation period, and the tangential angular velocities were measured at $0.037-0.052^{{\prime {\prime}}\;sec^{-1}$. Through this study, it was shown that the simultaneous observations among educational astronomical observations can obtain distance measurements with an error range of about 5% for asteroids near 0.4 AU. And it expected to be used as a research & education program emphasizing collaborative observation activities based on a network between observatories.

A STUDY ON BONE STRENGTH AND THE DEGREE OF CONVERSION OF DENTIN BONDING AGENTS (수종 상아질 접착제의 결합강도와 중합률에 관한 연구)

  • Kim, Byung-Hyun;Kwon, Hyuk-Choon
    • Restorative Dentistry and Endodontics
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    • v.23 no.1
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    • pp.68-93
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    • 1998
  • The physical properties of polymer are greatly influenced by the extent to which a resin cures. The presence of un reacted monomer can, have a plasticizing effect on the polymer, thereby altering the physical and mechanical properties of dentin bonding agent (DBA). If the DBA does not polymerize sufficiently, it will leave a weak bonding layer and lead to lower bond strength. The purpose of this study was to evaluate the shear bond strengths(SBS) and the degree of conversion (DC) of 4 commercialy avilable dentin bonding systems which are composed of 2 multi-bottle systems [Scotchbond Multi-Purpose (SMP), AeliteBond(AB)] and 2 onebottle systems [SingleBond(SB), One-Step(OS)]. For shear bond strength measurement, labial surfaces of freshly extracted bovine incisors were ground with # 600 grit SiC paper to expose dentin. Four different groups of samples were formed, with 10 samples. being made for each of the 4 commercial DBA in each group according to the curing sequences of DBA and overlayer thickness of composites: Group I (standard cure and 1mm thick composites) : The DBA was light cured and the composites of 1mm thickness was applied ; Group II (standard cure and 2mm thick composites) : The DBA was light cured and the composites of 2mm thickness was applied; Group III (simultaneous cure and 1mm thick composites) : The DBA was not light-cured and simultaneously cured with composites of 1mm thickness; Group N (simultaneous cure and 2mm thick composites) : The DBA was. not light-cured and simultaneously cured with composites of 2mm thickness. The SBS was measured immediately after the composites was bonded to the bovine dentin using an Instron machine. The DC of the DBA was examined in a thin film under simulated conditions of the experimental groups according to the curing sequences and overlayer thickness of composites in the SBS test. using a Fourier transform Infrared(FTIR) spectrometer. The following results were obtained from SBS tests and DC measurements 1. In SBS tests, the multi-bottle DBA(SMP, AB) had a generally higher bond strength values than the one bottle DBA(SB, OS). In DC measurements, the one bottle DBA(SB, OS) had a significantly higher DC than the multi-bottle DBA(SMP, AB). 2. In all DBAs except OS, there was no significant difference between the bond strength of group I (standard cure and 1mm thick composites) and that of group III (simultaneous cure and 1mm thick composites). SMP, SB in Group I had a significantly higher DC than those in group III, but AB, OS in group I had a significantly lower DC than those in group III 3. All DBAs in Goup II (standard cure and 2mm thick composites) had significantly higher bond strength and DC than those in Group N (simultaneous cure and 2mm thick composites). 4. In all DBAs, there was no significantly different SBS and DC between Group I and Group II, but all DBAs in Group III had significantly higher SBS and DC than those in Group IV.

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MEASUREMENTS OF AMBIENT NOISE GENERATED BY LARGE-AMPLITUDE INTERNAL WAVES IN LUZON STRAIT: THE FIRST EXPERIENCE

  • Serebryany, Andrey;Okhrimenko, Nikolay
    • Proceedings of the KSRS Conference
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    • v.2
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    • pp.943-945
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    • 2006
  • The experiment on study of ambient nose generated by large-amplitude internal waves in Luzon Strait is analyzed. Simultaneous observations of internal waves and characteristics of ambient noise generated by them were carried out. Fast 50-m solitary internal wave propagated to the northwest direction with speed more than 3 m/s was observed. It was revealed an enhancing of ambient noise level (at frequency range 1-2 kHz) at a time of passing the face side of the solitary wave.

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