• 제목/요약/키워드: Peeling Rate

검색결과 54건 처리시간 0.029초

STS 316L 소결체의 부식 저항 특성에 미치는 금속산화물 첨가의 영향 (The Effect of Oxides Additives on Anti-corrosion Properties of Sintered 316L Stainless Steel)

  • 이종필;홍지현;박동규;안인섭
    • 한국분말재료학회지
    • /
    • 제22권4호
    • /
    • pp.271-277
    • /
    • 2015
  • As wrought stainless steel, sintered stainless steel (STS) has excellent high-temperature anti-corrosion even at high temperature of $800^{\circ}C$ and exhibit corrosion resistance in air. The oxidation behavior and oxidation mechanism of the sintered 316L stainless was reported at the high temperature in our previous study. In this study, the effects of additives on high-temperature corrosion resistances were investigated above $800^{\circ}C$ at the various oxides ($SiO_2$, $Al_2O_3$, MgO and $Y_2O_3$) added STS respectively as an oxidation inhibitor. The morphology of the oxide layers were observed by SEM and the oxides phase and composition were confirmed by XRD and EDX. As a result, the weight of STS 316L sintered body increased sharply at $1000^{\circ}C$ and the relative density of specimen decreased as metallic oxide addition increased. Compared with STS 316L sintered parts, weight change ratio corresponding to different oxidation time at $900^{\circ}C$ and $1000^{\circ}C$, decreased gradually with the addition of metallic oxide. The best corrosion resistance properties of STS could be improved in case of using $Y_2O_3$. The oxidation rate was diminished dramatically by suppression the peeling on oxide layers at $Y_2O_3$ added sintered stainless steel.

군용 섬유제품에 적합한 파스너 테이프의 품질수준 연구 (A Study on Setting Quality Level of Fastener Tape for Military Textile Products)

  • 김성욱;이민희;홍성돈;이정순
    • 한국염색가공학회지
    • /
    • 제29권3호
    • /
    • pp.162-170
    • /
    • 2017
  • Fastener tapes are widely used as auxiliary materials in textile products, and military textiles products are also applied. However, in Korea, the HL3-WA class of KS K 1309 was applied to military uniforms without consideration of the operating environment. Instead of adopting the standard of initial strength for Korean military uniforms, the US military applied the value after 3 washings, and presented different properties according to the items. Also in Japan, the standard was applied differently according to products in general clothing. The purpose of this study in to examine the quality level of fastener tapes used for military materials. The changes of tensile shear strength and peel strength of military and commercial fastener tape were studied after washing. As a result, the initial strength of the current military fastener tapes was higher than commercial one, but the strength retention rate was rapidly decreased as the number of washing. So it was confirmed that the decrease in strength was relatively lower than commercial one. It is necessary to improve the durability by adjusting the adhesive strength to suit the purpose of the product, and it is necessary to consider the priority of maintaining the durability according to the initial performance and repeated use according to the use environment, respectively.

천연광물을 활용한 저온소결 세라믹 사이딩의 특성에 관한 연구 (A Study on the Characteristics of Low Temperature sintering Ceramic Siding Using Natural Minerals)

  • 김순호;최정민
    • 대한건축학회논문집:구조계
    • /
    • 제35권12호
    • /
    • pp.149-156
    • /
    • 2019
  • Recently, skyscraper building and apartment fires, which were rapidly spread out from a low floor to a rooftop, have become a frequent occurrence in mass media. This fire problems have a fatal disadvantage that the exterior wall finish of the building emits toxic gas in case of fire by using dry bit method or organic insulating material. Therefore, in order to remedy these problems, many exterior wall finishing construction methods have been proposed, but the current trend is to use existing construction methods due to problems such as economy, weight, and durability. On the other hand, in countries such as Germany and Japan, ceramic sidings are used as exterior finishing material for buildings, which is environmentally friendly, excellent natural beauty, long life, easy maintenance and high-quality exterior materials. However, those ceramic sidings have still the problems such as manufacturing cost and weight problem because of boosting the sintering temperature up to 1,350℃ or more. Also, conventional CRC, MgO, FRP sidings which are composed of pulp, glass fiber and organic materials, have been reports of deformation due to ultraviolet rays, discoloration, corrosion and scattering, surface rupture, lifting and peeling. Therefore, in this study as an alternative to solve this problem, halosite nano kaolin produced in Sancheong in Korea and frit flux were used to satisfy the required properties as ceramic siding using low temperature sintering (below 1,000℃) and lightweight materials such as pearlite. This study aims to design the optimal formulation and process of materials and to study the characteristics of nano-coated ceramic siding material development and to present relevant basic data. The findings show that ceramic siding for nanocoated building materials is excellent as a natural ceramic siding building material. The fire resistance of natural minerals and nano particle refining technology satisfy the bending strength of 80kgf / cm2, the volume ratio of 2.0 and the absorption rate of less than 10.0%.

MRT(Moisture Responded Transformable)섬유의 의료용 압박소매 적용에 관한 연구 (A Study on the Application of Medical Compression Arm Sleeves Using a MRT(Moisture Responded Transformable) Fibers)

  • 조대현;정태두;박은희;박영미
    • 한국염색가공학회지
    • /
    • 제33권2호
    • /
    • pp.87-95
    • /
    • 2021
  • In this study, the application of a medical compression sleeve of Moisture Responded Transformable(MRT) fibers to the treatment of lymphedema after surgery in breast cancer patients was investigated. MRT fibers were manufactured with PET and Nylon6 bi-component cross-section yarns, and compression sleeves of sleeves 1, 2, 3, and 4 were knitted in order of size, and then the physical properties and clinical tests were evaluated. As a result, the pressure of compression sleeve in wrinkle was the lowest in sleeve 1 with 3.81 kPa, and the highest in sleeve 4 with 5.22 kPa. Elastic recovery rate is that all parts except the top of the sleeve 1 exhibited 100%. The air permeability was good at 12.1 ~ 16.1 cm3/cm2/sec, and peeling was also comparatively excellent as grade 3. In addition, the weight of the compression sleeves 1, 2, and 3 decreased as 18.3 ~ 23.0 g/m2 depend on size, while the compared sample was heavier with 17.39 ~ 32.61 g/m2. In lymphoscintigraphy test, it was confirmed that the function of remaining lymph node was good in all patients. Although there were no differences between samples in skin irritation and tightness in wearing comfort, the manufactured sleeves showed better fit, lightness, fashion and breathability than the comparable sleeves.

유/무기하이브리드 코팅액에 의한 Al6061-T6의 내식 특성 (Corrosion Resistance of Al6061-T6 by Organic/Inorganic Hybrid Coating Solution)

  • 박미향;신기항;최병철;안병현;이금화;남기우
    • 한국산업융합학회 논문집
    • /
    • 제26권4_2호
    • /
    • pp.591-598
    • /
    • 2023
  • In this study, the corrosion resistance by salt spray was evaluated using A6061-T6 for an electric vehicle battery pack case coated with an organic/inorganic hybrid solution. The lowest curing temperature of 190 ℃ resulted in significant corrosion and pitting. Meanwhile, no corrosion was observed in the coated specimens at 210 ℃ and 230 ℃ except at 210 ℃ - 6 min and 8 min. The surface of the as-received coating specimen observed by FE-SEM exhibited streaks and dents in the rolling direction, but the coating surface was clean. On the 190 ℃ - 6 min coating specimen, which had a lot of corrosion, rolling streaks spread, and dents were caused by corrosion. The 200 ℃ - 12 min coating specimen did not show corrosion, but it showed an etched surface. In the line profile, Si, the main component of the coating solution, was detected the most, and Ti was also detected. In the coating specimens with salt spray, O increased and Si decreased, regardless of corrosion. The peeling rate by adhesion evaluation was 26 - 87% for the 190 ℃ coating specimen, 4 - 83% for the 210 ℃ coating specimen, and 94 - 100% for the 230 ℃ coating specimen. The optimal curing conditions for the coating solution used in this study were 210 ℃ for 10 min.

한국(韓國)에 있어서 벼기생선충에 관(關)한 연구(硏究) I. 벼이삭선충의 피해율(被害率) 및 침종(浸種)에 의한 선충분리율 조사(調査) (Nematodes Associated with Rice in Korea I. Survey on White Tip Nematode (Aphelenchoides besseyi) Damage to Rice and Detection of the Nematode in Rice Seed)

  • 최영연;최동로;최영식
    • 한국응용곤충학회지
    • /
    • 제25권3호
    • /
    • pp.159-167
    • /
    • 1986
  • 1. 벼이삭선충의 피해(被害)를 알기 위하여 경상남북도(慶尙南北道) 전라남도등(全羅南道等) 3개도(個道) 36개군(個郡) 111개면(個面)을 조사(調査)한 결과(結果) 피해경율(被害莖率)이 경남(慶南)에서는 창영군(昌寧郡)이 28.3%, 경북(慶北)에서는 영천군(永川郡)이 69.3%, 전남(全南)에서는 보성군(寶城郡)이 40.6% 로 각각 가장 높게 나타났다. 2. 벼이삭선충에 대(對)한 품종별(品種別) 피해경율(被害莖率)은 다수계(多收系) 품종(品種)에서는 원풍만 3.4%를 나타냈고 나머지 품종(品種)들은 전혀 white tip 증상(症狀)을 나타내지 않는 반면에 일반계(一般系)는 모두 $13.2{\sim}100%$ 의 피해경율(被害莖率)을 나타냈다. 종자내(種子內) 선충밀도는 다수계(多收系)나 일반계(一般系) 별차(別差)없이 같게 나타났으며 다수계(多收系)에서는 신광벼가 10gr당(當) 1,997마리, 일반계(一般系)에서는 동진벼가 10gr당(當) 1,023마리로서 각각(各各) 가장 높게 나타났다. 3. 침종전(浸種前)에 종자(種子)를 미박피구는 박피구에 비하여 선충분리율은 품종(品種)에 따라서 다소차이(多少差異)는 있으나 신선찰, 한강찰, 서광, 영풍, 밀양 23 호, 수정, 대청, 서남등(等) 8개품종(個品種)을 제외하고는 5% 이하(以下)의 낮은 분리율(分離率)을 나타냈다. 4. 온도별(溫度別) 침종시간(浸種時間)에 따른 선충분리율은 박피구와 미박피구 다같이 온도(溫度)가 높을수록 점차 분리율(分離率)이 높았으며 $25^{\circ}C$에서는 미박피구가 박피구보다 9일(日) 이후(以後)부터는 더 많이 분리(分離)되었다. 그리고 적산온도(積算溫度) $100^{\circ}C$를 기준(基準)하여 보면 미박피구는 박피구에 비하여 $10^{\circ}C$에서는 6%, $15^{\circ}C$에서 는 6.7%, $200^{\circ}C$에서는 13.4%, $25^{\circ}C$에서는 18.9% 분리(分離)되었다.

  • PDF

초경석고와 메타카올린 혼합재료의 물성실험 및 적용 (Physical Properties Testing and Practical Applications of Restoration Materials Made with Extra Hard Stone and Metakaolin)

  • 김현숙;이해순
    • 박물관보존과학
    • /
    • 제17권
    • /
    • pp.101-116
    • /
    • 2016
  • 기존의 석고복원재로 복원한 문화재는 대기 중의 수분을 반복하여 흡·방출하면서 물성이 약화되어 형태가 변형되고 채색층 박락이 진행된다. 본 논문에서는 이러한 단점을 보완하기 위해 일반석고보다 더 강한 초경석고를 실험대상으로 두었으며 메타카올린(Metakaolin)을 혼합하여 도자기 복원재료로 적합하도록 물성을 개선하였다. 초경석고와 메타카올린 혼합재료의 압축강도(119MPa)는 일반석고(26MPa)보다 월등히 높았으며, 마모율(0.88%)은 일반석고의 마모율 2.53% 보다 낮게, 흡수율(2.9%)은 일반석고(17.2%) 보다 약 5배 낮게 측정되었다. 특히, 주사전자현미경 관찰결과 혼합재료의 경화치밀도가 단미의 초경석고보다 높았다. 즉, 메타카올린을 첨가함으로써 초경석고의 강도와 수분저항성을 높이고 표면을 치밀하게 하여 도자기 복원재료로서 적합하게 물성을 개선시켰다. 그리고 이 혼합재료를 실재 문화재인 토제수반(신안18892), 분청사기조화문병(접수2034), 분청사기 국문내인화문대접(접수1730)의 결손부 복원에 적용해봄으로써, 혼합재료가 주입 및 적층성형에 유리하고 경화표면이 균질하여 자연스러운 채색이 가능한 재료임을 확인하였다.

Sub-0.2${\mu}m$ 다층 금속배선 제작을 위한 Cu Dual-dmascene공정 연구 (Studies on Cu Dual-damascene Processes for Fabrication of Sub-0.2${\mu}m$ Multi-level Interconnects)

  • 채연식;김동일;윤관기;김일형;이진구;박장환
    • 전자공학회논문지D
    • /
    • 제36D권12호
    • /
    • pp.37-42
    • /
    • 1999
  • 본 논문에서는 차세대 집적회로의 핵심공정으로 부각되고 있는 CMP를 이용한 Cu Damascene 공정을 연구하였다. E-beam lithography, $SiO_2$ CVD 및 RIE, Ti/Cu CVD등의 제반 단위 공정을 연구하였으며, 연구된 단위공정으로 2창의 Cu금속 배선을 제작하였다. CMP 단위공정 연구결과, hend 압력 4 PSI, table 및 head 속도 25rpm, 진동폭 10mm, 슬러리 공급량 40ml/min에서 연마율 4,635 ${\AA}$/min, Cu:$SiO_2$의 선택율 150:1, 평탄도 4.0%를 얻었다. E-beam 및 $SiO_2$ vialine 공정연구결과, 100 ${\mu}C/cm^2$ 도즈와 6분 30초의 현상 및 1분 10초의 에칭시간으로 약 0.18 ${\mu}m\;SiO_2$ via-line을 형성하였다. 연구된 단위공정으로 sub-0.2 ${\mu}$의 Cu 금속라인을 제작하였으며, Cu void 및 Cu의 peeling으로 인한 다층공정시의 문제점과 재현성 향상 방법에 대해 논의하였다.

  • PDF

Research on the Multi-electrode Plasma Discharge for the Large Area PECVD Processing

  • Lee, Yun-Seong;You, Dae-Ho;Seol, You-Bin
    • 한국진공학회:학술대회논문집
    • /
    • 한국진공학회 2012년도 제42회 동계 정기 학술대회 초록집
    • /
    • pp.478-478
    • /
    • 2012
  • Recently, there are many researches in order to increase the deposition rate (D/R) and improve film uniformity and quality in the deposition of microcrystalline silicon thin film. These two factors are the most important issues in the fabrication of the thin film solar cell, and for the purpose of that, several process conditions, including the large area electrode (more than 1.1 X 1.3 (m2)), higher pressure (1 ~ 10 (Torr)), and very high frequency regime (VHF, 40 ~ 100 (MHz)), have been needed. But, in the case of large-area capacitively coupled discharges (CCP) driven at frequencies higher than the usual RF (13.56 (MHz)) frequency, the standing wave and skin effects should be the critical problems for obtaining the good plasma uniformity, and the ion damage on the thin film layer due to the high voltage between the substrate and the bulk plasma might cause the defects which degrade the film quality. In this study, we will propose the new concept of the large-area multi-electrode (a new multi-electrode concept for the large-area plasma source), which consists of a series of electrodes and grounds arranged by turns. The experimental results with this new electrode showed the processing performances of high D/R (1 ~ 2 (nm/sec)), controllable crystallinity (~70% and controllable), and good uniformity (less than 10%) at the conditions of the relatively high frequency of 40 MHz in the large-area electrode of 280 X 540 mm2. And, we also observed the SEM images of the deposited thin film at the conditions of peeling, normal microcrystalline, and powder formation, and discussed the mechanisms of the crystal formation and voids generation in the film in order to try the enhancement of the film quality compared to the cases of normal VHF capacitive discharges. Also, we will discuss the relation between the processing parameters (including gap length between electrode and substrate, operating pressure) and the processing results (D/R and crystallinity) with the process condition map for ${\mu}c$-Si:H formation at a fixed input power and gas flow rate. Finally, we will discuss the potential of the multi-electrode of the 3.5G-class large-area plasma processing (650 X 550 (mm2) to the possibility of the expansion of the new electrode concept to 8G class large-area plasma processing and the additional issues in order to improve the process efficiency.

  • PDF

가열온도곡선 변화에 따른 고강도 콘크리트의 폭렬방지특성 (Spalling Prevention of High Strength concrete Corresponding to the Various Heating Curves)

  • 한천구;배장춘
    • 한국구조물진단유지관리공학회 논문집
    • /
    • 제13권3호통권55호
    • /
    • pp.127-134
    • /
    • 2009
  • 본 연구는 고강도 콘크리트의 복합유기섬유 혼입률 변화 및 ISO와 RABT의 가열온도곡선 변화에 따른 내화시험을 실시한 후 폭렬방지성상 및 잔존압축강도 특성 등을 분석한 것으로, 그 결과를 요약하면 다음과 같다. 복합유기섬유 혼입 콘크리트의 기초적 특성으로 유동성은 섬유혼입률이 증가할수록 직선적으로 저하하는 경향이었고, 공기량은 약간의 증가 또는 감소의 경향은 있었으나 큰 차이 없었으며, 28 일 압축강도는 완만한 감소경향을 나타내었다. 내화특성으로, RABT 가열온도곡선의 경우는 ISO 가열온도곡선에 비해 복합 유기섬유 혼입률이 많은 범위까지 폭렬양상을 나타내었으나, 주로 박리폭렬일뿐 내부까지 극심한 폭렬양상은 발생하지 않았다. 결국 W/B 25%인 고강도 콘크리트의 경우 ISO 가열온도곡선은 섬유의 혼입률 0.04%이상에서, RABT 가열온도곡선의 경우는 섬유의 혼입률 0.10%이상에서 폭렬이 방지되는 것으로 나타났다. 가열온도곡선 변화에 따른 질량감소율은 폭렬이 방지된 경우 ISO 가열온도곡선은 7%전후, RABT 가열온도 곡선은 9%전후로 나타났다. 가열온도곡선변화에 따른 잔존압축강도율은 폭렬이 방지된 경우 ISO 가열온도 곡선은 50%~60%, RABT 가열온도곡선은 30%~35%를 나타내었다.