• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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• pp.381-382
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• 2007

IZO/Ag/IZO (IAI) anode films for flexible organic light emitting diodes (OLEDs) were grown on PC (polycarbonate) substrate using DC sputter (IZO) and thermal evaporator (Ag) systems as a function of Ag thickness. To investigate electrical and optical properties of IAI stacked films, 4-point probe and UV/Vis spectrometer were used, respectively. From a IAI stacked film with 12nm-thick Ag, sheet resistance of $6.9\;{\Omega}/{\square}$ and transmittance of above 82 % at a range of 500-550 nm wavelength were obtained. In addition, structural and surface properties of IAI stacked films were analyzed by XRD (X-ray diffraction) and SEM (scanning electron microscopy), respectively. Moreover, IAI stacked films showed dramatically improved mechanical properties when subjected to bending both as a function of number of cycles to a fixed radius. Finally, OLEDs fabricated on both flexible IAI stacked anode and conventional ITO/Glass were fabricated and, J-V-L characteristics of those OLEDs were compared by Keithley 2400.

• 한국재료학회지
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• 제30권5호
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• pp.231-238
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• 2020

The composition of martensite transformation in NiAl alloy is determined using pure nickel and aluminum powder by vacuum hot press powder metallurgy, which is a composition of martensitic transformation, and the characteristics of martensitic transformation and microstructure of sintered NiAl alloys are investigated. The produced sintered alloys are presintered and hot pressed in vacuum; after homogenizing heat treatment at 1,273 K for 86.4 ks, they are water-cooled to produce NiAl sintered alloys having relative density of 99 % or more. As a result of observations of the microstructure of the sintered NiAl alloy specimens quenched in ice water after homogenization treatment at 1,273 K, it is found that specimens of all compositions consisted of two phases and voids. In addition, it is found that martensite transformation did not occur because surface fluctuation shapes did not appear inside the crystal grains with quenching at 1,273 K. As a result of examining the relationship between the density and composition after martensitic transformation of the sintered alloys, the density after transformation is found to have increased by about 1 % compared to before the transformation. As a result of examining the relationship between the hardness (Hv) at room temperature and the composition of the matrix phase and the martensite phase, the hardness of the martensite phase is found to be smaller than that of the matrix phase. As a result of examining the relationship between the temperature at which the shape recovery is completed by heating and the composition, the shape recovery temperature is found to decrease almost linearly as the Al concentration increases, and the gradient is about -160 K/at% Al. After quenching the sintered NiAl alloys of the 37 at%Al into martensite, specimens fractured by three-point bending at room temperature are observed by SEM and, as a result, some grain boundary fractures are observed on the fracture surface, and mainly intergranular cleavage fractures.

• Journal of Welding and Joining
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• 제30권3호
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• pp.26-31
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• 2012

Three-dimensional integrated circuit (3D IC) technology has become increasingly important due to the demand for high system performance and functionality. We have evaluated the effect of Buffered oxide etch (BOE) on the interfacial bonding strength of Cu-Cu pattern direct bonding. X-ray photoelectron spectroscopy (XPS) analysis of Cu surface revealed that Cu surface oxide layer was partially removed by BOE 2min. Two 8-inch Cu pattern wafers were bonded at $400^{\circ}C$ via the thermo-compression method. The interfacial adhesion energy of Cu-Cu bonding was quantitatively measured by the four-point bending method. After BOE 2min wet etching, the measured interfacial adhesion energies of pattern density for 0.06, 0.09, and 0.23 were $4.52J/m^2$, $5.06J/m^2$ and $3.42J/m^2$, respectively, which were lower than $5J/m^2$. Therefore, the effective removal of Cu surface oxide is critical to have reliable bonding quality of Cu pattern direct bonds.

• 대한금속재료학회지
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• 제46권5호
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• pp.321-327
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• 2008

Cu based amorphous ($Cu_{54}Zr_{22}Ti_{18}Ni_6$) coating was produced by cold spraying as a new fabrication process. The microstructure and macroscopic properties of amorphous coating layer was investigated and compared with those of cold sprayed pure Cu coating. Amorphous powders were prepared by gas atomization and Al 6061 was used as the substrate plate. X-ray diffraction results showed that Cu based amorphous powder could be successfully deposited by cold spraying without any crystallization. The Cu based amorphous coating layer ($300{\sim}400{\mu}m$ thickness) contained 4.87% porosity. The hardness of Cu based amorphous coating represented $412.8H_v$, which was correspond to 68% of the hardness of injection casted bulk amorphous material. The wear resistance of Cu based amorphous coating was found to be three times higher than that of pure Cu coating. The 3-point bending test results showed that the adhesion strength of Cu based amorphous coating layer was higher than that pure Cu coating. It was also observed that hard Cu base amorphous particle could easily deform soft substrate by particle collisions and thus generated strong adhesion between coating and substrate. However, the amorphous coating layer unexpectedly represented lower corrosion resistance than pure Cu coating, which might be resulted from the higher content of porosity in the cold sprayed amorphous coating.

• Design & Manufacturing
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• 제14권4호
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• pp.65-70
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• 2020

Partial reinforcement of sheet metal parts with CFRP patch is a technology that can realize ultra-lightweight body parts while overcoming the high material cost of carbon fiber. Performing these patchworks with highly productive press equipment solves another issue of CFRP: high process costs. The A-pillar is the main body part and has an undercut shape for fastening with other parts such as roof panels and doors. Therefore, it is difficult to bond CFRP patches to the A-pillar with a general press forming tool. In this paper, a flexible system that applies uniform pressure to complex shapes using ceramic particles and silicone rubber is proposed. By benchmarking various A-pillars, a reference model with an undercut shape was designed, and the system was configured to realize a uniform pressure distribution in the model. The ceramic spherical particles failed to realize the uniform distribution of high pressure due to their high hardness and point contact characteristics, which caused damage to the CFRP patch. Compression equipment made of silicone rubber was able to achieve the required pressure level for curing the epoxy. Non-adhesion defects between the metal and the CFRP patch were confirmed in the area where the bending deformation occurred. This defect could be eliminated by optimizing the process conditions suitable for the newly developed flexible system.

• 한국구조물진단유지관리공학회 논문집
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• 제12권1호
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• pp.101-108
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• 2008

본 연구에서는 철근과 같은 기계적 맞물림 현상을 활용하기 위하여 이형리브가 형성되어 있는 GFRP 보강근을 제작하여 철근대체 재료로 사용하기 위해 FRP 보강근의 부착성능을 규명하고자 한다. 하지만 지금까지 많은 기존 연구자들이 부착성능에 대한 실험으로 단순 1방향(수직, 수평)인장실험으로 철근과 콘크리트 또는 FRP 보강근과 콘크리트사이의 부착특성을 고찰하여 두 재료 사이의 부착-슬립에 관한 제안식을 도출해왔다. 국내에서는 아직까지 GFRP 보강근의 부착에 대한 관심이 증대대고 있는 실정이지만 피로부착에 관한연구는 미흡한 편이이어서 GFRP 보강근의 피로 연구가 필요로 하다. 본 연구에서는 BRITISH STANDARD에서 규정하고 있는 방법에 의하여 휨 부착 시험체를 제작하여 정적 휨 부착실험 최대파괴하중의 70% ~ 90%의 하중으로 반복하중재하 후 정적실험을 통하여 GFRP로 보강된 콘크리트 피로부착 성능을 검증하였다.

• 한국구조물진단유지관리공학회 논문집
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• 제12권2호
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• pp.171-180
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• 2008

본 논문의 목적은 채널형 단부정착장치를 사용하여 CFRP판으로 보강한 철근콘크리트 보의 구조적 거동을 평가하는 것이다. 총 12개의 시험체를 제작하였으며, 이 중에는 보강판의 효율성을 높이기 위해 채널형 단부정착장치를 사용한 시험체와 사용하지 않은 시험체가 있다. 모든 시험체의 단면 크기는 동일하며, 주철근량과 콘크리트의 강도를 변화시켰다. 하중재하는 모든 시험체에서 4점 휨시험으로 진행되었으며, 각 재료의 변형률, 균열, 하중, 및 파괴모드가 시험 중에 측정되었다. 모든 시험체의 시험결과는 변형, 강도, 그리고 파괴모드 측면으로 분석되었다. 실험결과에 대한 분석를 통해서 채널형 단부정착장치를 사용한 RC보는 그 파괴모드가 급작스런 부착파괴에서 변형이나 강도적 측면에서 구조적 성능이 매우 향상된 연성적 파괴모드로 전환되는 것을 확인할 수 있었다.

• Korean Chemical Engineering Research
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• 제45권5호
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• pp.466-472
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• 2007

웨이퍼 레벨(WL) 3차원(3D) 집적을 구현하기 위해 저유전체 고분자를 본딩 접착제로 이용한 웨이퍼 본딩과, 적층된 웨이퍼간 전기배선 형성을 위해 구리 다마신(damascene) 공정을 사용하는 방법을 소개한다. 이러한 방법을 이용하여 웨이퍼 레벨 3차원 칩의 특성 평가를 위해 적층된 웨이퍼간 3차원 비아(via) 고리 구조를 제작하고, 그 구조의 기계적, 전기적 특성을 연속적으로 연결된 서로 다른 크기의 비아를 통해 평가하였다. 또한, 웨이퍼간 적층을 위해 필수적인 저유전체 고분자 수지를 이용한 웨이퍼 본딩 공정의 다음과 같은 특성 평가를 수행하였다. (1) 광학 검사에 의한 본딩된 영역의 정도 평가, (2) 면도날(razor blade) 시험에 의한 본딩된 웨이퍼들의 정성적인 본딩 결합력 평가, (3) 4-점 굽힘시험(four point bending test)에 의한 본딩된 웨이퍼들의 정량적인 본딩 결합력 평가. 본 연구를 위해 4가지의 서로 다른 저유전체 고분자인 benzocyclobutene(BCB), Flare, methylsilsesquioxane(MSSQ) 그리고 parylene-N을 선정하여 웨이퍼 본딩용 수지에 대한 적합성을 검토하였고, 상기 평가 과정을 거쳐 BCB와 Flare를 1차적인 본딩용 수지로 선정하였다. 한편 BCB와 Flare를 비교해 본 결과, Flare를 이용하여 본딩된 웨이퍼들이 BCB를 이용하여 본딩된 웨이퍼보다 더 높은 본딩 결합력을 보여주지만, BCB를 이용해 본딩된 웨이퍼들은 여전히 칩 back-end-of-the-line (BEOL) 공정조건에 부합되는 본딩 결합력을 가지는 동시에 동공이 거의 없는 100%에 가까운 본딩 영역을 재현성있게 보여주기 때문에 본 연구에서는 BCB가 본딩용 수지로 더 적합하다고 판단하였다.

• 대한치과교정학회지
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• 제36권3호
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• pp.188-197
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• 2006

교정 치료 시 사용되는 섬유 강화 컴포지트(FRC, fiber reinforced composite)는 구강 내에서 저작압 등의 지속적인 응력과 수분 흡수 등의 이유로 파절이 일어나는 경우가 있다. 이 때 모든 FRC를 제거하지 않고 수리(repair)하는 경우에 적절한 강도를 얻기 위해 첨가해야 할 FRC의 양 및 그 파절 양상을 알아보고자 하였다. 두 개의 FRC strips를 1, 2, 3, 그리고 4mm 만큼 겹쳐(E1, E2, E3, E4군) 시편을 만드는 방법으로 수리를 재현한 후 light emitting diode 광중합기로 중합하고, 3점 굽힘 실험을 시행하여 겹침 길이와 접합 강도간의 관계에 대해 조사하였다. 최대 하중치는 E4군에서 2.67N으로 최대였고, 대조군(2.39N), E3군(2.35N), E2군(2.10N), 그리고 E1군(1.75N)의 순이었다. 강성 역시 최대 하중치와 같이 E4군(2.32 N/mm)에서 최대치를 기록하였으나, E3군(2.06N/mm)의 강성이 대조군(1.88N/mm)보다 더 큰 값을 보였다. 겹침 길이가 길수록 완전히 두 조각으로 파절되기 보다 가운데 또는 critical section 에서 굽힘 양상을 보였다. 반면 겹침 길이가 짧은 경우 두 조각으로 부러지는 파절 양상을 보였다. 이상의 실험에서 길이 10 mm인 연결자 형태의 FRC의 수리 시 적절한 강도를 얻기 위해서는 최소 3 mm의 strips를 겹쳐야 하고, 이 때 주로 나타나는 실패 양상인 굽힘을 최소화하기 위해 연결 부위에 바로 인접하여 두께가 급격하게 변하는 critical section의 보강이 필요할 것으로 사료된다.

• 대한치과보철학회지
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• 제33권4호
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• pp.780-806
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• 1995

The purpose of this study was to describe the application of 3D finite element analysis to determine resultant stresses on the bone anchored fixed prosthesis, implants and supporting bone of the mandible according to fixture numbers and load conditions. 4 or 6 fixtures and the bone anchored fixed prosthesis were placed in 3D finite element mandibular arch model which represents an actual mandibular skull. A $45^{\circ}$ diagonal load of 10㎏ was labiolingually applied in the center of the prosthesis(P1). A $45^{\circ}$ diagonal load of 20㎏ was buccolingually applied at the location of the 10mm or 20mm cantilever posterior to the most distal implant(P2 or P3). The vertical distribution loads were applied to the superior surfaces of both the right and the left 20mm cantilevers(P4). In order that the boundary conditions of the structure were located to the mandibular ramus and angle, the distal bone plane was to totally fixed to prevent rigid body motion of the entire model. 3D finite element analysis was perfomed for stress distribution and deflection on implants and supporting bone using commercial software(ABAQUS program. for Sun-SPARC Workstation. The results were as follows : 1. In all conditions of load, the hightest tensile stresses were observed at the metal lates of prostheses. 2. The higher tensile stresses were observed at the diagonal loads rather than the vertical loads 3. 6-implants cases were more stable than 4-implants cases for decreasing bending and torque under diagonal load on the anterior of prosthesis. 4. From a biomechanical perspective, high stress developed at the metal plate of cantilever-to-the most distal implant junctions as a consequence of loads applied to the cantilever extension. 5. Under diagonal load on cantilever extension, the 6-implants cases had a tendency to reduce displacement and to increase the reaction force of supporting point due to increasing the bendign stiffness of the prosthesis than 4-implants cases. 6. Under diagonal load on cantilever extension, the case of 10mm long cantilever was more stable than that of 20mm long cnatilever in respect of stress distribution and displacement. 7. When the ends of 10mm or 20mm long cantilever were loaded, the higher tensile stress was observed at the second most distal implant rather than the first most distal implant. 8. The 6-implants cases were more favorable about prevention of screw loosening under repeated loadings because 6-implants cases had smaller deformation and 4-implants cases had larger deformation.