• 소성∙가공
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• 제6권2호
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• pp.145-151
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• 1997

In order to obtain high quality products in powder metallurgy, it is important to control and understand the densification behavior of metal powders. The effect of the characters of powders on the compaction behavior was studied in this study by using three types of powders produced by the gas atomization, the centrifugal atomization and the twin roll-pulverization. The shape of the powders was a major factor in the apparent or tap density, and the deformation resistance of the matrix of the powders was a major factor in compactibility. Han's yield function (eq.2) for metal powders was simplified from the relationship based on the experimental results of copper powders. In spite of some assumptions, the calculated compaction curves using a new yield functionw was in accordance with the experimental results.

• 대한금속재료학회지
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• 제49권10호
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• pp.790-796
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• 2011

To reduce the heat released during intermetallic reaction, Ni-50at%Al powder compact has been previously annealed at several conditions before the reaction. The effects of the pre-annealing conditions on the reaction synthesis process have been investigated. Experimental results show that the heat released during the reaction synthesis decreased proportionally with increase of the pre-annealing temperature and duration time. The reaction duration period was significantly increased when the intermetallics were formed in the powder compact during the pre-annealing. This was attributed to the fact that the reaction occurred by solid-state diffusion between the un-reacted elemental atoms and that the $NiAl_3$ phase formed predominantly during pre-annealing.

• 대한금속재료학회지
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• 제47권9호
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• pp.567-572
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• 2009

The densification behaviors of mixtures of copper and steel powders during cold die compaction were investigated. We proposed the pressure-dependent yield function based on the rule of the mixtures of each yield function of a critical relative density type. The constitutive equations were implemented into a finite element program (DEFORM2D) to analyze the densification and deformation behavior of powder mixtures, and the simulated results are in good agreement with the experimental results in reference studies.

• 한국구조물진단유지관리공학회 논문집
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• 제23권2호
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• pp.130-134
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• 2019

본 논문에서는 레이저기반 응력측정을 위한 비접촉식 로드셀을 개발을 위하여, 실내실험을 통하여 기술을 검증하고, 실규모 실험을 통하여 문제점을 파악하였으며, 최종적으로 현장적용에 적합한 응력측정용 비접촉식 로드셀 프로토타입을 개발하였다. 이를 위하여, 중심공 압축타입의 로드셀 제작에 사용되는 로드셀 몸체 표면에 용사코팅기술을 이용하여 알루미나를 도포하고, 레이저를 기반으로한 압분광법을 이용하여, 비접촉식으로 응력을 계측하였다. 이때, 인가되는 응력과 스펙트럼 이동간의 관계가 선형임을 확인하였다. 해당 기술의 현장 적용성 확인을 위하여, 실규모 프리스트레스 콘크리트 시편을 제작하고, 레이저를 조사하여 인가된 응력을 확인하는 과정에서, 반복적인 상황 하에서 레이저 조사 위치가 동일해야 함을 확인하였다. 이를 보완하기 위하여 프로브를 고정할 수 있는 케이싱이 포함된 로드셀 프로토타입을 제작하였고, 실내일축압축시험을 통하여 압축력과 스펙트럼 이동간의 선형성을 확인하였다. 따라서, 본 연구를 통하여 개발된 비접촉식 로드셀을 이용하여, 압축력을 효과적으로 측정할 수 있을 것으로 기대된다.

• 자원리싸이클링
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• 제12권4호
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• pp.51-57
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• 2003

케퍼시터용 Ta 분말제조공정에서 발생하는 waste 분말을 이용하여 TaC 분말을 자전고온합성법에 의하여 합성하였다. waste TA는 합성반응의 활성 및 산화방지를 위하여 전처리공정에서 미분쇄 및 탈산처리가 필요하였다. 합성반응에서는 TaC 단일상은 6∼7wt.％C의 조성범위에서 얻을 수 있었다. 또한 반응온도는 시료의 압축력에 영향을 받으며, 압축력 1600psi에서 최고반응온도를 나타냈다.

• 소성∙가공
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• 제26권4호
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• pp.216-221
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• 2017

Recently, interest in multifunctional energetic structural materials (MESMs) has grown due to their multifunctional potential, especially in military applications. However, there are few studies about extrinsic factors that govern the reactivity of MESMs. In this paper, a shock compaction process was performed on the nano Ni/Al-mixed powder to investigate the effect of particle size on the shock reaction condition. Additionally, heating the statically compacted specimen was also performed to compare the mechanical properties and microstructure between reacted and unreacted material. The results show that the agglomerated structure of nanopowders interrupts the reaction by reducing the elemental boundary. X-ray diffraction analysis shows that the NiAl and $Ni_3Al$ intermetallics are formed on the reacted specimen. The microhardness results show that the $Ni_3Al$ phase has a higher hardness than NiAl, but the portion of $Ni_3Al$ in the reacted specimen is minor. In conclusion, using Ni/Al composites as a reactive material should focus on energetic use.

• 한국재료학회지
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• 제8권6호
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• pp.551-559
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• 1998

장경비가 큰 탄화규소를 탄소와 규소간의 고온연소반응으로 제조하기 위하여 공정변수에 따른 연소거동과 미세조직의 변화를 조사하였다. 연소합성된 생성물은 주로 $\beta$-SiC이며 연소반응이 충분히 진행되지 못하였을 경우에는 미량의 잔류 반응물과 $\alpha$-SiC가 관찰되었다. 생성된 탄화규소의 평균입도는 약 5$\mu\textrm{m}$로 작았으며, $1300^{\circ}C$ 이상의 예열 조건에서 장경비가 30이상인 탄화규소를 합성할 수 있었다. 압분 강도가 69MPa인 분말의 성형체에서 평균 연소 온도와 평균 전파 속도는 각각 약 $1425^{\circ}C$와 2.1mm/sec 범위이며, 연소 온도는 흑연 분말을 사용하였을 경우가 탄소 섬유를 사용한 경우보다 약 $10^{\circ}C$ 높았다. 연소 반응을 임의로 중단시킨 시편의 계면을 EDX와 Auger 전자 현미경으로 분석한 결과 상호 확산층이 관찰되지 않았다. 이는 탄화규조의 연소합성이 용해-석출 모델에 의하여 진행됨을 시사한다. 예열 온도에 따른 연소 반응 중의 온도 분포를 유한 요소법으로 해석함으로써 $2500^{\circ}C$의 초기 연소 개시 온도에 대하여 예열 온도 $300^{\circ}C$에서는 연소파가 거의 전파할 수 없으며 예열 온도가 $1300^{\circ}C$에서는 시료 내부에 자체 전파가 가능한 $2000^{\circ}C$이상의 온도 구역이 존재함을 알았다.

• 한국분말재료학회지
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• 제18권5호
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• pp.406-410
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• 2011

Green strength is an important property of powders since high green strength guarantees easy and safe handling before sintering. The green strength of a powder compact is related to mainly mechanical and surface characters, governed by interlocking of the particles. In this study, the effect of powder surface roughness on the green strength of iron powders was investigated using a transverse rupture test. Three-dimensional laser profiler was employed for quantitative analyses of the surface roughness. Two different surface conditions, i.e. surface roughness, of powders were compared. The powders having rough surfaces show higher green strength than the round surface powders since higher roughness leads increasing interlocked area between the contacting powders.

• 한국자동차공학회논문집
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• 제11권5호
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• pp.50-59
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• 2003

It was known that high pressure injection is an effective method to enhance thermal efficiency and decrease exhaust emissions in diesel engines. If injection pressure becomes ultra high, it is predicted that there may be a suitable injection pressure which the enhancement rate of spray characteristics is moderate. Also, there may be a limit injection pressure which spray characteristics is reversed and get worse. But these are unknown. To investigate a suitable injection pressure and a limit injection pressure, ultra high pressure injection equipment(UHPIE), which can realize the injection pressure of 3,200bar, was developed. UHPIE is a basic apparatus of single shot injection, and ultra high pressure was achieved by second stage rapid compression in short time. From the evaluation of UHPIE, a injection curve like a conventional diesel engine(jerk type) was realized. Also, it was proved that repetition of experiment was excellent. Therefore it was found that there was no problem to perform the study on the ultra high pressure injection with UHPIE. Consequently, the foundation of the study on ultra high pressure injection could be established.

• 소성∙가공
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• 제21권4호
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• pp.228-233
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• 2012

In this study, powder compaction of AZO (alumina doped zinc oxide) powder was performed with a MTS 810 test system using a cylindrical die having a diameter of 10mm. Pressure-density curves were measured based on the load cell and displacement of the punch. The AZO powder compacts with various densities were formed to investigate the mechanical properties such as fracture stress of the AZO powder as a function of the compact density. Two types of compression tests were conducted in order to estimate the fracture stress using different loading paths: a diameteral compression test and a uniaxial compression test. The pressure-density curves of the AZO powder were obtained and the fracture stress of the compacted powders with various densities was estimated. The results show that the compact pressure dramatically increases as the density increases. Based on the experimental results, calibration of the modified Drucker-Prager/Cap model of the AZO powder for use in FE simulations was developed.