• Title/Summary/Keyword: 내구성 실험

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MICROLEAKAGE OF COMPOSITE RESIN RESTORATION ACCORDING TO THE NUMBER OF THERMOCYCLING (열순환 횟수에 따른 복합레진의 미세누출)

  • Kim, Chang-Youn;Shin, Dong-Hoon
    • Restorative Dentistry and Endodontics
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    • v.32 no.4
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    • pp.377-384
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    • 2007
  • Present tooth bonding system can be categorized into total etching bonding system (TE) and self-etching boding system (SE) based on their way of smear layer treatment. The purposes of this study were to compare the effectiveness between these two systems and to evaluate the effect of number of themocycling on microleakage of class V composite resin restorations. Total forty class V cavities were prepared on the single-rooted bovine teeth and were randomly divided into four experimental groups: two kinds of bonding system and another two kinds of thermocycling groups. Half of the cavities were filed with Z250 following the use of TE system, Single Bond and another twenty cavities were filled with Metafil and AQ Bond, SE system. All composite restoratives were cured using light curing unit (XL2500, 3M ESPE, St. Paul, MN, USA) for 40 seconds with a light intensity of $600mW/cm^2$. Teeth were stored in distilled water for one day at room temperature and were finished and polished with Sof-Lex system. Half of teeth were thermocycled 500 times and the other half were thermocycled 5,000 times between $5^{\circ}C$ and $55^{\circ}C$ for 30 second at each temperature. Teeth were isolated with two layers of nail varnish except the restoration surface and 1 mm surrounding margins. Electrical conductivity (${\mu}A$) was recorded in distilled water by electrochemical method. Microleakage scores were compared and analyzed using two-way ANOVA at 95% level. From this study, following results were obtained: There was no interaction between variables of bonding system and number of thermocycling (p = 0.485). Microleakage was not affected by the number of thermocycling either (p = 0.814). However, Composite restoration of Metafil and AQ Bond, SE bond system showed less microleakage than composite restoration of Z250 and Single Bond, TE bond system (p = 0.005).

Effects of Exhaust Gas Recirculation on Power and Thermal Efficiency of Reactivity Controlled Compression Ignition in Different Load Conditions with a 6-L Engine (6 L급 압축착화 기관에서 천연가스-디젤 반응성 조정 연소 시 부하에 따른 배기 재순환율이 출력 및 열효율에 미치는 영향 분석)

  • Lee, Sunyoup;Lee, Seok-Hwan;Kim, Chang-Gi;Lee, Jeong-Woo
    • Journal of the Korean Institute of Gas
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    • v.24 no.6
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    • pp.1-10
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    • 2020
  • Reactivity controlled compression ignition (RCCI) combustion is one of dual-fuel combustion systems which can be constructed by early diesel injection during the compression stroke to improve premixing between diesel and air. As a result, RCCI combustion promises low nitrogen oxides (NOx) and smoke emissions comparing to those of general dual-fuel combustion. For this combustion system, to meet the intensified emission regulations without emission after-treatment systems, exhaust gas recirculation (EGR) is necessary to reduce combustion temperature with lean premixed mixture condition. However, since EGR is supplied from the front of turbocharger system, intake pressure and the amount of fresh air supplementation are decreased as increasing EGR rate. For this reason, the effect of various EGR rates on the brake power and thermal efficiency of natural gas/diesel RCCI combustion under two different operating conditions in a 6 L compression ignition engine. Varying EGR rate would influence on the combustion characteristic and boosting condition simultaneously. For the 1,200/29 kW and 1,800 rpm/(lower than) 90 kW conditions, NOx and smoke emissions were controlled lower than the emission regulation of 'Tier-4 final' and the maximum in-cylinder pressure was 160 bar for the indurance of engine system. The results showed that under 1,200 rpm/29 kW condition, there were no changes in brake power and thermal efficiency. On the other hand, under 1,800 rpm condition, brake power and thermal efficieny were decreased from 90 to 65 kW and from 37 to 33 % respectively, because of deceasing intake pressure (from 2.3 to 1.8 bar). Therefore, it is better to supply EGR from the rear of compressor, i.e. low pressure EGR (LP-EGR) system, comparing to high pressure EGR (HP-EGR) for the improvement of RCCI power and thermal efficiency.

Freeze-thaw Resistance Estimation of Concrete using Surface Roughness and Image Analysis (콘크리트의 동결융해 저항성 추정을 위한 표면 거칠기 및 이미지 분석의 적용성)

  • Lee, Binna;Lee, Jong Suk
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.22 no.3
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    • pp.1-7
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    • 2018
  • As part of a research dedicated to the field evaluation of the durability of concrete subjected to freezing-thawing, this study analyzes the relationship between the surface roughness and the relative dynamic elastic modulus through image analysis. Four mix compositions with water-to-binder ratios (W/B) of 40%, 50%, 60% and 70% and without AE agent were considered to provoke early freezing. The basic physical properties of the mixes including the relative dynamic elastic modulus and the compressive strength were first evaluated experimentally according to W/B. Then, tests were performed to measure the surface roughness followed by photographs and SEM image analysis. The measured surface roughness tended to increase with larger number of freezing-thawing cycles regardless of W/B. The relative dynamic elastic modulus appeared to increase gradually with the number of cycles for the relatively denser mixes with W/B of 40% and 50%. Besides, the surface roughness increased only at rupture for the mixes with W/B of 60% and 70%. Moreover, the analysis of the photographs of the surface of the mixes with W/B of 40% and 50% revealed that the degradation progressed gradually from the surface with the freezing-thawing cycles. However, for the mixes with W/B of 60% and 70%, apparent change of the surface remained very insignificant until rupture at which damage like cracking could be observed. Consequently, the analysis of surface photograph or the measurement of the surface roughness presented some limitation in assessing the degree of freezing-thawing-induced degradation in case of relatively porous specimens. On the other hand, the photograph and surface roughness appeared to be sufficient for assessing such degradation for the mixes with W/B of 40% and 50%. Accordingly, the image of the surface and the surface roughness are potentially applicable on site for the assessment of freezing-thawing damages in relatively dense mixes.

Permeability and Freeze-Thaw Resistance of Latex Modified Concrete (라텍스 개질 콘크리트의 투수성 및 동결융해 저항 특성)

  • 김기헌;이종명;홍창우;윤경구
    • Journal of the Korea Concrete Institute
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    • v.13 no.5
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    • pp.484-490
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    • 2001
  • This study focused on the investigation of durability of latex modified concrete in the points of chloride ion permeability and freeze-thaw resistance as latex content variated such as 5%, 10%, 15% and 20%. When latex was mixed in concrete and cured, the concrete consisted of hydrated cement and aggregate interconnected by a film of latex particles. An increasing the amount of latex produced concrete with increased flexural strength, but with slightly lower compressive strength. The increase in flexural strength might be attributed to the latex films between the hydrated cement and aggregates, and the decrease in compressive strength to the flexibility of the latex component named by Butadiene. The rapid chloride permeability test was used to evaluate the relative permeability of latex-modified concretes and conventional concretes. The results showed that the permeability of latex-modified concretes was considerably lower than conventional concretes tested, which might be due to the latex filled in voids and interconnections of hydrated cement and aggregates by a film of latex particles. The freeze-thaw resistance of LMC was quite good comparing to conventional concrete. Air entraining agent has been used in conventional concrete to improve the freeze/thaw resistance, but latex modified concrete does not need additional air entraining agent for freeze-thaw resistance provided adequate cure occurs.

Design of MMA-Type Thermosetting Road Markings to Improve Reflectivity (재귀반사도 개선을 위한 MMA계 열경화성 차선도료의 설계)

  • Lee, Seung Bum;Lee, Chang Geun;Hong, In Kwon
    • Applied Chemistry for Engineering
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    • v.26 no.4
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    • pp.439-444
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    • 2015
  • Several attempts to design the best-available thermosetting road markings by using MMA to improve the durability and retroreflectivity are presented in this paper. In order to improve field applicability, the components of main materials were designed by means of reducing the hardening time lower than eight minutes. The optimum mixing ratio of thermosetting road marking was TSRM-6 composed of 15.6 wt% of MMA monomer ($Tg=105^{\circ}C$), 6.0 wt% of PMMA (MW = 70,000, $Tg=60^{\circ}C$) and 1.2 wt% of TMPTA (MW = 338, $Tg=27^{\circ}C$). Also the homogeneous mixing of all components was necessary. The use of ceramic glass beads with an optimized TSRM-6 exhibited excellent performance by achieving retroreflectivity coefficients of 431, 354 and $172mcd{\cdot}m^{-2}{\cdot}lux^{-1}$ for dry, wet and rainy test condition, respectively at two hundred thousand cycles.

Development of CMP process for reducing scratches during ILD CMP (ILD CMP중 Scratch 감소를 위한 CMP 공정기술 개발)

  • Kim, In-Gon;Kim, In-Kwon;Prasad, Y. Nagendra;Choi, Jea-Gon;Park, Jin-Goo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.06a
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    • pp.59-59
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    • 2009
  • 현재 CMP분야는 광역 평탄화 반도체 소자의 집적화 및 소형화가 진행됨에 따라서 CMP 공정의 중요성은 날로 성장하고 있다. 하지만 이러한 CMP공정은 불가피하게도 scratch, pit, CMP residue와 같은 defect들을 발생시키고 있으며, 점점 선폭이 작아짐에 따라, 이러한 defect들이 반도체 수율에 미치는 영향은 심각해지고 있다. Defect들 중에 특히 scratch는 반도체에 치명적인 circuit failure를 일으키게 된다. 또한 반도체 내구성과 신뢰성을 감소시키게 되고, 누전전류를 증가시키는 등 바람직하지 못한 현상들이 생기게 된다. 본 연구에서는 scratch 와 같은 deflect들을 효율적으로 검출, 분석하고, scratch를 감소시키는데 그 목적이 있다. 본 실험을 위해 8" TEOS wafer와 commercial oxide slurry 및 friction polisher (Poli-500, G&P tech., Korea)를 사용하여 CMP 공정을 진행하였으며, CMP 공정조건은 각각 80rpm/80rpm/1psi(Platen speed/Head speed/Pressure)에서 1분 동안 연마를 한 후 scratch 발생 경향을 살펴보았다. CMP 후 wafer위에 오염되어 있는 slurry residue들을 제거하기 위해 SC-1, HF 세정을 이용하여 최적화된 post-CMP 공정기술을 제안하였다. Scratch 검출 및 분석을 위해 wafer surface analyzer (Surfscan 6200, Tencor, USA)와 optical microscope (LV100D, Nicon, Japan)를 사용하였다. CMP 공정 변수들에 따른 scratch 발생정도를 비교하였으며, scratch 발생 요인들에 따른 scratch 형태 및 발생정도를 살펴보았다. 최적화된 post-CMP 세정 조건은 메가소닉과 함께 SC-1 세정을 실시하여 slurry residue들을 제거한 후, HF 세정을 실시하여 잔여 오염물들을 제거하고 검출이 용이하도록 scratch를 확장시킬 수 있도록 제안하였으며, 100%의 particle removal efficiency (PRE)를 얻을 수 있었다. 실제 CMP 공정후 post-CMP 세정 단계별 scratch 개수를 측정한 결과, SC-1 세정 후 약 220개의 scratch가 검출되었으며, 검출되지 않았던 scratch가 HF 세정 후 확장되어 드러남에 따라 약 500개의 scratch 가 검출되었다.

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An Experimental Study on the Durability Properties of Repair Mortar for Sewer Spread with Liquefied Antibiotic (액상 항균제를 도포한 하수시설용 단면복구재의 내구특성에 관한 실험적 연구)

  • Lee Dong-Heck;Jang Jae-bong;Na Chul-Sung;Cho Bong-Suk;Kim Jae-hwan;Kim Moo-Han
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2005.05a
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    • pp.211-214
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    • 2005
  • Recently, Deterioration of the concrete sewer concrete structures by biochemical corrosion has been issued and a development of the inhibition system of corrosion that has been demanded. The sulfuric acid may react with the hardened cement paste and originate expansive products which can induce swelling and breakless of concrete. Also, a sulphuric acid reacts with calcium hydroxide to from $CaSO_4\;\cdot\;2H_2O$. This reaction accounts for consumption of the calcium hydroxide present in hardened cement paste. In this study, To present from biochemical corrosion of the sewer repair mortar that was spread with liquefied antibiotic and then its experimental properties were experimentally investigated and to estimate the effect of absorbed condition of restorative mortar, the number of coating times and coating contents with antibiotic on the durability properties of restorative mortar spread with antibiotics. Also, testing items such as carbonation depth, choloride ion penetration depth and chemical resistance was tested to estimate the durability properties in third study. In results, the novellus bacillus inhabiting in sewer concrete structures was restrained by antibiotics developed in this study. And carbonation depth, choloride ion penetration depth and chemical resistance of restorative mortar spread with antibiotics was superior to that of plain mortar.

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An Analysis of Intrusion Pattern Based on Backpropagation Algorithm (역전파 알고리즘 기반의 침입 패턴 분석)

  • Woo Chong-Woo;Kim Sang-Young
    • Journal of Internet Computing and Services
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    • v.5 no.5
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    • pp.93-103
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    • 2004
  • The main function of the intrusion Detection System (IDS) usee to be more or less passive detection of the intrusion evidences, but recently it is developed with more diverse types and methodologies. Especially, it is required that the IDS should process large system audit data fast enough. Therefore the data mining or neural net algorithm is being focused on, since they could satisfy those situations. In this study, we first surveyed and analyzed the several recent intrusion trends and types. And then we designed and implemented an IDS using back-propagation algorithm of the neural net, which could provide more effective solution. The distinctive feature of our study could be stated as follows. First, we designed the system that allows both the Anomaly dection and the Misuse detection. Second, we carried out the intrusion analysis experiment by using the reliable KDD Cup ‘99 data, which would provide us similar results compared to the real data. Finally, we designed the system based on the object-oriented concept, which could adapt to the other algorithms easily.

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A Study on Experiment and Structural Analysis for High-Durability of Orthotropic Steel Deck Bridge (고내구성을 위한 강바닥판교의 실험 및 해석 연구)

  • Kong, Byung-Seung;Kim, Min-Ho
    • Proceedings of the KSR Conference
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    • 2007.11a
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    • pp.462-467
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    • 2007
  • From the research which it sees verification of the whole interpretation and local interpretation of the durability steel deck bridge a static test and it produces the test body which it sells with character and it executes smallness pul lek detailed interpretation it leads and the appropriate characteristic of smallness pul lek detailed interpretation and to sleep a nominal stress price and it compares it judges it does. The stress quality from each structure region which it follows in load stock location it analyzes and from the hazard which evaluates, the objective region the length rib and the bottom grater weld zone, the length rib and width rib connection department and the width rib with the father it divided. It investigated the stress distribution of the test body from these objective location, FEM interpretation it led and the conduct against each structure state tax it analyzed. General conduct the load stock location the floor plate is located in the center with interpretation price together symmetry characteristic to seem, it cannot be like that it cannot there is one actual test price. Like this reason the length rib and width rib connection actually production even production characteristic security it is a day when it is impossible with the curvature junction department which it blows, it follows in examination body deferment condition and form feed with the fact that it is visible a big difference even with error of some it becomes. Consequently for a data and the research which are more accurate it is judged with the fact that the effort which is prudent will be necessary.

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Chloride Diffusion Coefficients in Cold Joint Concrete with GGBFS (고로슬래그 미분말을 혼입한 콜드조인트 콘크리트의 염화물 확산계수)

  • Oh, Kyeong-Seok;Mun, Jin-Man;Kwon, Seung-Jun
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.20 no.5
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    • pp.44-49
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    • 2016
  • Among the deteriorating agents, chloride ion is reported to be one of the most harmful ions due to its rapid diffusion and direct effect on steel corrosion. Cold joint which occurs in mass concrete placing is vulnerable to shear resistance and more severe deterioration. The paper presents an quantitative evaluation of chloride diffusion coefficient in OPC(Ordinary Portland Cement) and GGBFS(Ground Granulated Blast Furnace Slag) concrete containing cold joint. GGBFS concrete shows $6.6{\times}10^{-12}m^2/sec$ which is almost 30% level of OPC concrete results and the trend is repeated in the case of cold joint concrete. Compared with OPC concrete, GGBFS concrete is evaluated to have better resistance to chloride penetration, showing 0.30 times of chloride diffusion coefficient in concrete without cold joint 0.39 times with cold joint, respectively.