• Title/Summary/Keyword: $DO_3$ phase

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Effects of the Cooling Rate After Annealing Treatment on the Microstructure and the Mechanical Properties of Super-Duplex Stainless Steel (슈퍼 듀플렉스 스테인레스강의 미세조직 및 기계적 특성에 미치는 열처리 후 냉각속도의 영향)

  • Kwon, Gi-Hyoun;Na, Young-Sang;Yoo, Wee-Do;Lee, Jong-Hoon;Park, Yong-Ho
    • Korean Journal of Metals and Materials
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    • v.50 no.10
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    • pp.735-743
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    • 2012
  • The aim of this study was to analyze the effect of the cooling rate after heat treatment on the microstructure and mechanical properties of 2507 duplex stainless steels. Heat treatment was carried out at $1050^{\circ}C$ for 1 hr, followed by controlled cooling. The cooling rates were $175.6{\times}10^{-3}^{\circ}C/s$, $47.8{\times}10^{-3}^{\circ}C/s$, $33.3{\times}10^{-3}^{\circ}C/s$, $16.7{\times}10^{-3}^{\circ}C/s$, $11.7{\times}10^{-3}^{\circ}C/s$, $5.8{\times}10^{-3}^{\circ}C/s$ and $2.8{\times}10^{-3}^{\circ}C/s$, which resulted in variations of the microstructure, such as the fractional change of the ferrite phase and sigma phase formation. Fatigue, hardness, impact and tensile tests were performed on the specimens with different cooling rates. The precipitation of the ${\sigma}$ phase caused a hardness increase and a sharp decrease of toughness and tensile elongation. The fatigue limit of the sample with a cooling rate of $5.8{\times}10^{-3}^{\circ}C/s$ was 26 MPa higher than that of the sample with a cooling rate of $175.6{\times}10^{-3}^{\circ}C/s$. Our observations of the fracture surface confirmed that the higher fatigue resistance of the specimen with a cooling rate of $5.8{\times}10^{-3}^{\circ}C/s$ was caused by the delay of the fatigue crack growth, in addition to higher yield strength.

Analysis of growth environment of Flammulina velutipes using the smart farm cultivation technology (병재배 팽이버섯의 스마트팜 재배를 통한 생육환경 분석)

  • Lee, Kwan-Woo;Jeon, Jong-Ock;Lee, Kyoung-Jun;Kim, Young-Ho;Lee, Chan-Jung;Jang, Myoung-Jun
    • Journal of Mushroom
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    • v.17 no.4
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    • pp.197-204
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    • 2019
  • In this study, smart farm technology was used by farmers cultivating 'CHIKUMASSHU T-011' in order to develop an optimal growth model for the precision cultivation of bottle-grown winter mushroom and the results of the same are mentioned herein. Farmers participating in the experiment used 60 ㎡ of bed area with 4 rows and 13 columns of shelf shape, 20 horsepower refrigerator, 100T of sandwich panel for insulation, 6 ultrasonic humidifiers, 12 kW of heating, and 20,000 bottles of Flammulina velutipes mushroom spores. The temperature, humidity, and carbon dioxide concentrations, which directly affect the growth of the mushroom, were collected and analyzed from the environmental sensors installed at the winter mushroom cultivation area. The initial temperature was found to be 14.5℃, which was maintained at 14℃ to 15℃ until the 10th day. In the restriction phase, the initial temperature was 4℃ and was maintained between 2℃ and 3℃ until the 15th day, while during the growth phase, it was maintained between 7.5℃ to 9.5℃. Analysis of the humidity data revealed initial humidity to be 100%, which varied between 88% to 98% during primordia formation period. The humidity remained between 77% to 96% until the 15th day, in the restriction phase and between 75% to 83% during the growth phase. The initial carbon dioxide concentration was 3,500 ppm and varied between 3,500 ppm to 6,000 ppm during primordia formation period and was maintained at 6,000 ppm until the 15th day. During the growth phase, the carbon dioxide concentration was found to be over 6,000 ppm. Fruiting body characteristics of 'CHIKUMASSHU T-011' cultivated in the farmhouse were as follows: Pileus diameter of 7.5 mm and thickness of 4.1 mm, stipe thickness of 3.3 mm, and length of 154.2 mm. The number of valid fruiting bodies was 1,048 unit per 1,400 mL bottle, and the individual weight was 0.71 g per unit. The yield of fruiting bodies was 402.8 g per 1,400 mL bottle.

Aroma Characteristic of Chungkukjang with Astragalus membranaceus (황기청국장의 향기특성)

  • Yoon Hyang-Sik;Choi Hye-Sun;Joo Seon-Jong;Kim Ki-Sik;Kim Sook-Jeong
    • Food Science and Preservation
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    • v.13 no.2
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    • pp.269-272
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    • 2006
  • Aroma compounds in chungkukjang with Astragalus membranaceus (Hwangki) were extracted by the simultaneous distillation and extraction (SDE), headspace and solid phase microextraction (SPME), and aroma compounds obtained by this method were identified with GC-MS. Thirty compounds were identified, including six ketones, eight alcohols, three heterocyclic compounds, three aldehydes, five hydrocarbones and five other compounds. Major aroma compounds were identified as 3-hydroxy-2-butanone, 2-furanmethanol, 2-methoxy-4-vinylphenol, and 4-vinylphenol in SDE, 2,3-butanedione, 3-hydroxy-2-butanone, ethanol, 2,6-dimethyl pyrazine and acetic acid in headspace and acetone, ethanol, 2,5-dimethyl pyrazine, tetramethyl pyrazine and acetic acid in SPME. The content of pyrazines identified in headspace and SPME methods was higher than that of SDE method, and the content of pyrazines containing 2,5-dimethyl pyrazine, 2,6-dimethyl pyrazine and tetramethyl pyrazine in chungkukjang was higher than that of Hwangki chungkukjang.

Refractive media flatness measurement by phase shifting digital holography (위상천이 디지털 홀로그래피를 이용한 평판의 표면 평면도 측정)

  • Jeon, Sung-Bin;Kim, Do-Hyung;Cho, Jang-Hyun;Park, No-Cheol;Yang, Hyun-Seok;Park, Kyoung-Su;Park, Young-Pil
    • Transactions of the Society of Information Storage Systems
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    • v.8 no.2
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    • pp.44-49
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    • 2012
  • We measured the surface flatness of both sides for refractive media using the transmitted digital holography method. To enhance the accuracy of the result, phase-shifting system was used. With two different phase modulation of reference beam, the phase profile of object can be easily obtained. Thus, we proposed the surface measurement method which can measure large area fast, compared with conventional methods. To guarantee the reliability of obtained result, we compared with Zygo measurement system. With the proposed method, the surface flatness of $3.45{\mu}m$ resolution could be obtained.

Formation of Incommensurate Phase in TiNiFe Processed by Self-propagating High Temperature Synthesis Method (고온자전 합성법에 의해 제조된 TiNiFe합금에서 Incommensurate 상의 형성)

  • Cho, Jae-Seob;Kim, Do-Hyang;Kim, Yong-Seog
    • Applied Microscopy
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    • v.26 no.3
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    • pp.379-388
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    • 1996
  • Structure of premartensite in $Ti_{50}Ni_{49}Fe_1\;and\;Ti_{50}Ni_{50}$ prepared by self-propagating high temperature synthesis (SHS) method has been investigated by a detailed transmission electron microscopy. $Ti_{50}Ni_{49}Fe_1$ consists of microdomain area and needle type domain area. On the other hand, $Ti_{50}Ni_{50}$ consists of microdomain-free and microdomain area, and needle type domain area. Various types of extra superreflections, such as 1/2<100>, 1/2<110> and 1/4<210> type superreflection have been observed in the selected area electron diffractions from microdomain area. Such extra superreflections are due to transformation from B2 structure to distorted B2 structure or premartensite. The present study shows that incommensurate phase forms as an intermediate phase during martensitic transformation. Particularly, in Fe-free $Ti_{50}Ni_{50}$, two types of matrix phases have been observed, microdomain and microdomain-free area. Types of extra superreflections in $Ti_{50}Ni_{50}$ are different from those in $Ti_{50}Ni_{49}Fe_1$, i.e. 1/7<321> type superreflections have been observed, instead of 1/2<110>, 1/2<100>, 1/4<210> types in $Ti_{50}Ni_{49}Fe_1$.

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Investigation of Demixing Phenomena of a Polymer Solution During the Phase Inversion Process

  • Han, Myeong-Jin;D. Bhattacharyya
    • Proceedings of the Membrane Society of Korea Conference
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    • 1995.04a
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    • pp.11-15
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    • 1995
  • Polysulfone (PS) membranes were prepared by the phase inversion process using water or isopropanol as nonsolvent. The Flory-Huggins theory for a ternary system nonsolvent/solvent/polymer is applied to describe the thermodynamic equilibria of the components. The calculated ternary phase equilibria show that demixing of a PS binary solution with n-methylpyrrolidone (NMP) will be fast in a water coagulation bath and will be delayed in an isopropanol bath. The prepared membranes were characterized by SEM, gas adsorption-desorption measurement, and permeability test. The membrane, which is precipitated by fast demixing in a water bath, has nodular structures in the skin region and includes finger-like cavities in the sublayer. The membrane coagulated by isopropanol has a very dense and thick skin structure, which is formed by delayed demixing. The membrane coagulated by isopropanol showed considerably lower pore volume and surface area compared to that observed with water coagulation method. With dimethylformamide (DMF) as solvent and 2-3 wt% of water, the solution can show the liquid-liquid phase separation due to agglomation of the polymer-lean phase from the homogeneous solution. The membranes, which were coagulated near an equilibrium state, show the large (micron size) round pores in the whole membranes. The pores do not contribute the permeation characteristics.

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HRT에 따른 혐기-호기-무산소 공정의 BNR 특성

  • 김홍태;김은경
    • Proceedings of the Korean Environmental Sciences Society Conference
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    • 2003.11b
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    • pp.47-48
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    • 2003
  • 무산소조의 HRT가 3.5시간에서는 탈질이 일어날 수 있는 조건을 이루지 못하였다. Phase 4에는 무산소조를 3.7시간으로 고정하고 호기조와 혐기조의 HRT를 조절하여도 전체적인 효율에는 큰 영향을 미치지 않았다. 또한 슬러지 반송만으로 높아질수 있는 NO3-N 농도를 무산소조의 HRT로 조절함과 동시에 호기조에서의 DO농도를 1.5로 주입함으로써 높은 질산화로 인해 발생되는 낮은 탈질률을 막아줌으로써 인제거율에도 효과를 나타냄을 알 수 있다.

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Stress-Bias Effect on Poly-Si TFT's on Glass Substrate

  • Baek, Do-Hyun;Yong Jae lee
    • Proceedings of the IEEK Conference
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    • 2000.07b
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    • pp.933-936
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    • 2000
  • N-channel poly-Si TFT, processed by Solid Phase Crystalline(SPC) on a glass substrate, has been investigated by measuring its electrical properties before and after stressing. It is observed that the threshold voltage shift due to electrical stress varies with various stress conditions. Threshold voltages measured in 1.5um and 3um poly-Si TFT’s are 3.3V, 37V respectively. With the threshold voltage shift, the degradation of transconductance and subthreshold swing is also observed.

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Synthesis and Mesomorphic Properties of Palladium(II) Complexes Based on 3,4,5-Trialkoxy Benzonitrile Ligands

  • 이명수;유용식;최문근
    • Bulletin of the Korean Chemical Society
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    • v.18 no.10
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    • pp.1067-1070
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    • 1997
  • The synthesis and characterization of the nitrile ligands 3,4,5-tridodecyloxy benzonitrile (7) and 3,4,5-trioctadecyloxy benzonitrile (8), and their corresponding palladium(Ⅱ) complexes are described. The nitrile ligands display only a crystalline phase and do not show liquid crystalline behavior, while their corresponding palladium(Ⅱ) complexes dispaly an enantiotropic columnar mesophase. The induction of the columnar mesophase is mainly due to dimerization through the palladium complexation of the half disk-like nitrile ligands giving rise to a trans square planar geometry.

Two-Dimensional Behavior and J-Aggregate Formation of Merocyanine Dye Monolayers in Mutual Mixing (상호혼합에 의한 메로시아닌 색소 단분자막의 2차원 거동 및 J-회합체 형성)

  • Sin, Hun-Gyu;Kwon, Young-Soo
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.51 no.3
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    • pp.105-110
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    • 2002
  • J-aggregates in the mutual mixing LB films of [6Me-DS]$_{1-x}$ [DO]$_{x}$,[DS]$_{1-x}$ [DO]$_{x}$ and [DSe]$_{1-x}$ [DO]$_{x}$ have been studied by optical absorption, fluorescence and surface pressure-area isotherms. In [6Me-DS]$_{1-x}$ [DO]$_{x}$ films, sharp J-band absorption and fluorescence of [6Me-DS] are linearly shifted to the longer wavelength for the replacement of [6Me-DS] by [DO]. According to the x, a smooth shift of the limited area has been cleared. In the [DS]-[DO] system, the J-band is enhanced at 1:1 composition and strong fluorescence is also observed. Also, the presence of phase separation was suggested in the [DSe]-[DO] system, because the absorption spectra were decomposed into [DSe] and [DO] spectra. On the other hand, in the pressure-area isothermal study, reduction in the molecular occupying area of monolayers has been clarified. This could be ascribed to the enhancement of molecular ordering in J-aggregates. These facts are also believed to reflect the most closely packed arrangement of chromophores in the merocyanine dye monolayers. Thus, it was confirmed that the interaction between mixed dye molecules and the CdC1$_2$+KHCO$_3$subphases affected the J-aggregates of the LB films. Also. it is thought that the J-aggregates are formed non-dimensionally in LB films, such as solution synthesized [DX:DO] assemblies on mixing.s on mixing.