• 제목/요약/키워드: wet strength

검색결과 644건 처리시간 0.025초

타액에 의한 오염이 상아질 접착제의 미세전단결합강도에 미치는 영향 (EFFECT OF SALIVARY CONTAMINATION OF TEETH ON MICROTENSILE BOND STRENGTH OF VAR10US DENTIN BONDING SYSTEMS.)

  • 최경규;류길주
    • Restorative Dentistry and Endodontics
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    • 제28권3호
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    • pp.203-208
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    • 2003
  • The purpose of this study was to evaluate the effect of salivary contamination of teeth on bonding efficacy of self-priming and self-etching DBSs. The materials used were Single Bond(SB, self-priming system, 3M), Unifil Bond(UB, self-etching system, GC), and Scotchbond Multi-Purpose Plus(SM, 3M) as control. Forty five human molars randomly allocated to three groups as dentin bonding systems tested and embedded in epoxy resin. Then the specimens were wet-ground to expose flat buccal enamel surface or flat occlusal dentin surface and cut bucco-lingually to form two halves with slow speed diamond saw. One of them was used under non-contamination, other under contamination with saliva. The bonding procedure was according to the manufacturer's directions and resin composite(Z-100, 3M Dental Products, St. Paul, MN) was built-up on the bonded surface 5mm high. The specimens were ground carefully at the enamel-composite interface with fine finishing round diamond bur to create an hour-glass shape yielding bonded surface areas of $1.5{\pm}0.1\textrm{mm}^2$. The specimens were bonded to the modified microtensile testing apparatus with cyanoacrylate, attached to the universal testing machine and stressed in tension at a CHS of 1mm/min. The tensile force at failure was recorded and converted to a tensile stress(MPa). Mean values and standard deviations of the bond strength are listed in table. One-way ANOVA was used to determine significant difference at the 95% level. The bond strength of SBMP and SB were not affected by salivary contamination, but that of UB was significantly affected by salivary contamination. These results indicate that DBSs with total etch technique seems less likely affected by salivary contamination in bonding procedure.

용융방사에 의한 생분해성 PBS/PBAT 블랜드 모노 필라멘트 제조 및 물리적 특성 (Preparation and physical properties of biodegradable polybutylene succinate/polybutylene adipate-co-terephthalate blend monofilament by melt spinning)

  • 박성욱;김성훈;최혜선;조현혹
    • 수산해양기술연구
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    • 제46권3호
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    • pp.257-264
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    • 2010
  • In order to improve the breaking strength and elongation of Polybutylene succinate (PBS) monofilament, the monofilament was produced by blending PBS and Polybutlyne adipate-co-terephthalate (PBAT). The PBS/PBAT blend monofilament was prepared by the melt spinning system, and the weight ratios of the compositions of PBS/PBAT was 100/0, 95/5, 90/10 and 85/15, respectively. The breaking strength, elongation, softness and crystallization of PBS/PBAT blend monofilament were analyzed by using a tensionmeter, softness measurement, X-ray diffractometer in the both dry and wet conditions. The PBS/PBAT blend monofilaments were spun in the take-up velocity of 1.19m/sec under the drawing ratio of 6.8:1 condition. The production volumes of PBS/PBAT blend monofilaments showed 20% less than that of Nylon. The breaking strength of PBS/PBAT blend monofilaments were decreased as PBAT contents increased, while elongation and softness were increased. In case of PBAT content were over 5%, the breaking strength, elongation and softness of PBS/PBAT blend monofilaments were not shown to increase in spite of increasing in PBAT contents. Based on these results, it was possible to make the monofilaments with the maximized physical properties when the PBAT contents at 5%.

열습환경을 고려한 항공기용 레이돔 볼트 체결부의 베어링 강도에 관한 연구 (A Study on the Bearing Strength of Bolt Jointed Section for Composite Aircraft Radome Under Hygrothermal Environments)

  • 김호일;유구현;김준;김광민;이규송;박영주;박범준;유홍균
    • 대한기계학회논문집A
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    • 제41권8호
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    • pp.759-764
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    • 2017
  • 본 연구에서는 항공기용 레이돔에 적용되는 복합재의 볼트 체결부 강도에 대한 온도 및 습도 환경의 영향을 연구하였으며 열습환경에 노출된 레이돔 체결부에 대해 수분흡수율을 구하고, 온도와 습도환경에 따른 체결부 강도의 물성변화를 확인하였다. 이때 시편은 환경조건을 고려하여 상온건조(RTD), 고온고습(EWT), 저온건조(CTD) 세 가지로 구분하였으며 볼트 체결부의 파손하중 및 파손모드를 결정하기 위한 실험과 유한요소해석을 수행하였다. 유한요소해석의 결과가 체결부 강도와 파손모드에서 실험결과와 잘 일치하였으며 체결부 파손강도 예측이 가능한 효과적인 방법으로 확인하였다.

면직물의 젤라틴 전처리에 의한 소목염색의 염색성 향상 (Improving the Dyeability of Cotton Fabric with Caesalpinia sappan through Pretreatment with Gelatin)

  • 이지연;장정대
    • 한국의류산업학회지
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    • 제21권4호
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    • pp.509-514
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    • 2019
  • Cotton fabrics were treated with gelatin to enhance dyeability and color strength when using Caesalpinia sappan dye. Gelatin was used as the protein and a pad-dry- cure method was used for the treatment process (2, 4, 6, 8, 10, 12, 14g/l concentration). Pretreated fabrics were mordanted with 10% alum. Fabrics were then dyed with freeze-dried sappan wood water extract powder form. Dyed samples were assessed in regards to dyeing behavior and color fastness. Comparing untreated and gelatin treated samples from the SEM images indicated that the Gelatin treatment (10g/l) resulted in an enhanced surface roughness that was relative to that of untreated cotton. Padding cotton with gelatin at 6g/l concentration afforded dyed fabrics with a 2 times increase in the K/S value over that of untreated fabrics. All dyed samples were red color with a significant enhancement in the sample color strength (K/S) being observed for pretreated samples. pH values favor dye absorption with pH 7 yielding the highest color strength. Dyeing at an elevated temperature resulted in a lower color strength and reddish-dull color. Longer dyeing times created greater color strengths for untreated and gelatin treated cotton. Increased dye concentrations resulted in higher K/S values for both gelatin treated and untreated cotton. As for color fastness, gelatin treated and untreated cotton fabrics dyed with sappan wood extract showed a relatively low rating in washing fastness (color change 1 rating), light fastness (1 rating), and rubbing fastness (wet:1-2, dry:3-4 rating).

The push-out bond strength of BIOfactor mineral trioxide aggregate, a novel root repair material

  • Akbulut, Makbule Bilge;Bozkurt, Durmus Alperen;Terlemez, Arslan;Akman, Melek
    • Restorative Dentistry and Endodontics
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    • 제44권1호
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    • pp.5.1-5.9
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    • 2019
  • Objectives: The aim of this in vitro study was to evaluate the push-out bond strength of a novel calcium silicate-based root repair material-BIOfactor MTA to root canal dentin in comparison with white MTA-Angelus (Angelus) and Biodentine (Septodont). Materials and Methods: The coronal parts of 12 central incisors were removed and the roots were embedded in acrylic resin blocks. Midroot dentin of each sample was horizontally sectioned into 1.1 mm slices and 3 slices were obtained from each root. Three canal-like standardized holes having 1 mm in diameter were created parallel to the root canal on each dentin slice with a diamond bur. The holes were filled with MTA-Angelus, Biodentine, or BIOfactor MTA. Wet gauze was placed over the specimens and samples were stored in an incubator at $37^{\circ}C$ for 7 days to allow complete setting. Then samples were subjected to the push-out test method using a universal test machine with the loading speed of 1 mm/min. Data was statistically analyzed using Friedman test and post hoc Wilcoxon signed rank test with Bonferroni correction. Results: There were no significant differences among the push-out bond strength values of MTA-Angelus, Biodentine, and BIOfactor MTA (p > 0.017). Most of the specimens exhibited cohesive failure in all groups, with the highest rate found in Biodentine group. Conclusions: Based on the results of this study, MTA-Angelus, Biodentine, and BIOfactor MTA showed similar resistances to the push-out testing.

지게차용 기계유압식 무단변속기의 기어류에 대한 강도해석 (The Strength Analysis of Gears on Hydro-Mechanical Continuously Variable Transmission for Forklift)

  • 배명호;배태열;최성광
    • 드라이브 ㆍ 컨트롤
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    • 제13권4호
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    • pp.45-51
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    • 2016
  • The power train of a hydro-mechanical, continuously variable transmission for forklifts makes use of hydro-static units, hydraulic multi-wet disc brakes & clutches, and complex helical & planetary gears. The complex helical & planetary gears are very important parts of the transmission because of a strength problem. In the present study, we calculated the specifications of the complex helical & planetary gear train, and analyzed the gear bending and compressive stresses of the gears. It is necessary to analyze the gear bending and compressive stresses thoroughly for optimal design of the complex helical & planetary gears with respect to cost and reliability. In this paper, we analyze the actual gear bending and compressive stresses of complex helical & planetary gears using the Lewes & Hertz equation, and we also verify the calculated specifications of the complex helical & planetary gears by evaluating the results of the data of allowable bending and compressive stress using the Stress vrs Number of Cycles curves of gears.

Desmear 습식 표면 전처리가 무전해 도금된 Cu 박막과 FR-4 기판 사이의 계면 접착 기구에 미치는 영향 (Effect of Desmear Treatment on the Interfacial Bonding Mechanism of Electroless-Plated Cu film on FR-4 Substrate)

  • 민경진;박영배
    • 한국재료학회지
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    • 제19권11호
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    • pp.625-630
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    • 2009
  • Embedding of active devices in a printed circuit board has increasingly been adopted as a future electronic technology due to its promotion of high density, high speed and high performance. One responsible technology is to embedded active device into a dielectric substrate with a build-up process, for example a chipin-substrate (CiS) structure. In this study, desmear treatment was performed before Cu metallization on an FR-4 surface in order to improve interfacial adhesion between electroless-plated Cu and FR-4 substrate in Cu via structures in CiS systems. Surface analyses using atomic force microscopy and x-ray photoemission spectroscopy were systematically performed to understand the fundamental adhesion mechanism; results were correlated with peel strength measured by a 90o peel test. Interfacial bonding mechanism between electrolessplated Cu and FR-4 substrate seems to be dominated by a chemical bonding effect resulting from the selective activation of chemical bonding between carbon and oxygen through a rearrangement of C-C bonding rather than from a mechanical interlocking effect. In fact, desmear wet treatment could result in extensive degradation of FR-4 cohesive strength when compared to dry surface-treated Cu/FR-4 structures.

실리콘 직접 접합을 위한 선형가열법의 개발 및 SOI 기판에의 적용 (Development of Linear Annealing Method for Silicon Direct Bonding and Application to SOI structure)

  • 이진우;강춘식;송오성;양철웅
    • 한국표면공학회지
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    • 제33권2호
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    • pp.101-106
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    • 2000
  • SOI (Silicon-On-Insulator) substrates were fabricated with varying annealing temperature of $25-660^{\circ}C$ by a linear annealing method, which was modified RTA process using a linear shape heat source. The annealing method was applied to Si ∥ $SiO_2$/Si pair pre-contacted at room temperature after wet cleaning process. The bonding strength of SOI substrates was measured by two methods of Razor-blade crack opening and direct tensile test. The fractured surfaces after direct tensile test were also investigated by the optical microscope as well as $\alpha$-STEP gauge. The interface bonding energy was 1140mJ/m$^2$ at the annealing temperature of $430^{\circ}C$. The fracture strength was about 21MPa at the temperature of $430^{\circ}C$. These mechanical properties were not reported with the conventional furnace annealing or rapid thermal annealing method at the temperature below $500^{\circ}C$. Our results imply that the bonded wafer pair could endure CMP (Chemo-Mechanical Polishing) or Lapping process without debonding, fracture or dopant redistribution.

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수입 NYLON망사의 장력시험과 염색후의 변화 (Strength Tests of Imported NYLON 6 and its Variation after Dying)

  • 고관서;김병태;강건희
    • 수산해양기술연구
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    • 제6권1호
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    • pp.14-22
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    • 1970
  • 국내에서 생산하고 있는 Nylon 6 망사의 원사는 대부분 일본에서 수입하여 제망해서 수출하고 있다. 그러나 우리가 수입하고 있는 원사중 어느 회사의 원사가 우수한지 또한 염색 가공후의 망사의 성질변화에 대하여서는 그다지 알려져 있지 않으며 그뿐만 아니라 같은 Nylon 6 망사라 할지라도 제조 공정에 따라 망사의 성질이 달라질 수 있으므로 저자들은 일산 Nylon6 망사를 가지고 염색전과 후의 강신도와 염색후의 수축등을 시험 비교해 보았다. 특히 망사는 수중에서 사용되기 때문에 습윤시의 인장 강도와 신장이 겁습에 비해 어떻게 변화하는가를 관찰하였다.

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건식벽체에서 접착제 종류에 따른 타일부착 안전성 평가에 관한 연구 (A Study of the appraisal for adhesive stability classified by tile bond agent on the dry wall surface)

  • 엄찬용;선윤숙;권시원;오상근
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2005년도 춘계 학술기술논문발표대회 논문집
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    • pp.173-178
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    • 2005
  • The tile construction methods for existing have been used materials within limit which adhesion by wet method in masonry wall and concrete structure. These existing adhesive tech can caused many problems in construction of large and reform tile, after that it can be happened loose scale, peel off, falling off tile by heat and vibration or impact. In according to, this study is to test tile for bond stability, adhesive property by impact, vibration. low property by heat and then, we have the results as below; (1) The tile adhesive stability can be effected as adhesive area between bond agent and tile, adhesive area can more wide and press enough to ensure property. (2) Existing adhesive strength and standard relative tile construction is limited to adjust performance tile on the concrete and masonry wall. In summary, It is necessary to establish standard of performance and test method to ensure tile adhesive salability in dry wall.

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