• Title/Summary/Keyword: wax removal

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Removal of Organic Wax and Particles on Final Polished Wafer by Ozonated DI Water

  • Yi, Jae-Hwan;Lee, Seung-Ho;Kim, Tae-Gon;Lee, Gun-Ho;Choi, Eun-Suck;Park, Jin-Goo
    • Korean Journal of Materials Research
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    • v.18 no.6
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    • pp.307-312
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    • 2008
  • In this study, a new cleaning process with a low cost of ownership (CoO) was developed with ozonated DI water ($DIO_3$). An ozone concentration of 40 ppm at room temperature was used to remove organic wax film and particles. Wax residues thicker than $200\;{\AA}$ remained after only a commercial dewaxer treatment. A $DIO_3$ treatment in place of a dewaxer showed a low removal rate on a thick wax layer of $8000\;{\AA}$ due to the diffusion-limited reaction of ozone. A dewaxer was combined with a $DIO_3$ rinse to reduce the wax removal time and remove wax residue completely. Replacing DI rinse with the $DIO_3$ rinse resulted in a surface with a contact angle of less than $5^{\circ}$, which indicates no further cleaning steps would be required. The particle removal efficiency (PRE) was further improved by combining a SC-1 cleaning step with the $DIO_3$ rinsing process. A reduction in the process time was obtained by introducing $DIO_3$ cleaning with a dewaxing process.

Removal of Paraffin Wax from Ceramic Injection Mold Using Supercritical Carbon Dioxide (세라믹 사출성형체로부터 초임계이산화탄소를 이용한 파라핀왁스의 제거)

  • Kim, Dong-Hyun;Hong, Seung-Tae;Yoo, Ki-Pung;Lim, Jong-Sung
    • Clean Technology
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    • v.14 no.1
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    • pp.1-6
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    • 2008
  • Removal of paraffin wax from a ceramic injection mold using supercritical $CO_2$ has been studied. The paraffin wax is used as a binder in the ceramic injection molding process. The effects of pressure, temperature and flow rate of supercritical $CO_2$ on the removal of the paraffin wax were investigated. The removal rates were measured with various flow rates of $CO_2$ in the range of 328.15 - 348.15 K and 15 - 30 MPa. The removal rate of paraffin wax increased as the pressure increased. In the effect of temperature, the paraffin wax was effectively removed over 329.15K (melting point of paraffin wax), however, the efffct of temperature was not significant when the temperature was further increased. The increase of $CO_2$ flow rate also affected the removal of paraffin wax. However, the effect of flow rate was not observed when the flow rate reached a certain value. Propane was used as a co solvent in order to remove the paraffin wax effectively. When the propane was added to the $CO_2$, the removal efficiency was improved. The paraffin wax was completely removed from the ceramic injection mold without any change in their shape and the structure.

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Effect of Organic wax residues and particles removal by DIO3 (ozonated DI water) after Silicon Wafer batch Polishing Process (오존수를 이용한 실리콘 웨이퍼 연마 후 지용성 왁스 및 오염입자 제거의 영향)

  • Yi, Jae-Hwan;Lee, Seung-Ho;Kim, Tae-Gon;Park, Jin-Goo;Lee, Gun-Ho;Bae, So-Ik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.06a
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    • pp.558-559
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    • 2007
  • A commercially de-waxer which kinds of solvent after was used to remove a thick organic wax film after polishing process and several steps of SC-1 cleanings were followed for the removal of organic wax residues and particles which requires long process time and high cost of ownership (COO). DIO3 was used to remove organic wax residues too achieve low COO. In this study, 0103 rinsing could use instead of 01 water rinsing. The process time and chemical consumption were reduced by using DIO3.

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The Impact of the Morphological Characteristics of Leaves on Particulate Matter Removal Efficiency of Plants

  • Son, Deokjoo;Kim, Kwang Jin;Jeong, Na Ra;Yun, Hyung Gewon;Han, Seung Won;Kim, Jeongho;Do, Gyung-Ran;Lee, Seon Hwa;Shagol, Charlotte C.
    • Journal of People, Plants, and Environment
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    • v.22 no.6
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    • pp.551-561
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    • 2019
  • This study was conducted to find out differences in the removal efficiency of particulate matter (PM) depending on the type of plants and the morphological characteristics of leaves. A total of 12 plants were used, with three plants selected for each type of leaves (big leaf, small leaf, compound leaf, needle leaf). We measured the removed amount of PM10 and PM2.5, the structure of the abaxial leaf surface, and the weight of the wax layer of each plant. Plants with the high removal efficiency of PM included Pachira aquatica Aubl., Ardisia crenata, and Dieffenbachia 'Marianne', and plants with the low removal efficiency included Nandina domestica Thunb, Schefflera arboricola, and Quercus dentata. The abaxial leaf surface having a high removal efficiency of PM had many large wrinkles, and the abaxial leaf surface having a medium removal efficiency was flat and smooth. On the other hand, there were many fine hairs on the abaxial leaf surface with a low removal efficiency. According to the plant leaf type, the PM10 removal efficiency of plants with needle leaves was about three times higher than that of other plants. In particular, the wax layer of conifers weighed 6-24 times higher than those of other plants. The stomata of conifers were evenly distributed on the adaxial and abaxial leaf surfaces; however, the stomata of Sciadopitys verticillata appeared in the form of papillae unlike general stomata. Therefore, the removal efficiency of PM varied depending on the macro-, and micro-morphological characteristics of plant leaves such as the structure of the abaxial leaf surface, and the weight of the wax layer. Based on this research, selecting plants that are effective in reducing PM in consideration of the plant type and leaf characteristics will improve indoor air quality and decrease exposure of PM to human body.

Development of the ultra/nano filtration system for textile industry wastewater treatment

  • Rashidi, Hamidreza;Sulaiman, Nik Meriam Nik;Hashim, Nur Awanis;Bradford, Lori;Asgharnejad, Hashem;Larijani, Maryam Madani
    • Membrane and Water Treatment
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    • v.11 no.5
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    • pp.333-344
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    • 2020
  • Advances in industrial development and waste management over several decades have reduced many of the impacts that previously affected ecosystems, however, there are still processes which discharge hazardous materials into environments. Among industries that produce industrial wastewaters, textile manufacturing processes play a noticeable role. This study was conducted to test a novel continuous combined commercial membrane treatment using polyvinylidene fluoride (PVDF), ultrafiltration (UF), and polyamide (PA) nanofiltration (NF) membranes for textile wastewater treatment. The synthetic textile wastewater used in this study contained sodium silicate, wax, and five various reactive dyes. The results indicate that the removal efficiency for physical particles (wax and resin) was 95% through the UF membrane under optimum conditions. Applying UF and NF hybrid treatment resulted in total effective removal of dye from all synthetic samples. The efficiency of sodium silicate removal was measured to be between 2.5 to 4.5% and 13 to 16% for UF and NF, respectively. The chemical oxygen demand in all samples was reduced by more than 85% after treatment by NF.

Binder Removal by Supercritical $CO_2$ in Powder Injection Molded WC-Co (WC-Co계 분말사출성형에서 초임계$CO_2$에 의한 결합제 제거)

  • 김용호;임종성;이윤우;김소나;박종구
    • Journal of Powder Materials
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    • v.8 no.2
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    • pp.91-97
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    • 2001
  • The conventional debinding process in metal injection molding is very long time-consuming and unfriendly environmental method. Especially, in such a case of injection molded parts from hard and fine metal powder, such as WC-Co, an extremely long period of time is necessary in the conventional slow binder removal process. On the other hand, supercritical debinding is thought to be the effective method which is appropriate to eliminate the aforementioned inconvenience in the prior art. The supercritical fluid has high diffusivity and density, it can penetrate quickly into the inside of the green metal bodies, and extract the binder. In this paper, super-critical debinding is compared with wicking debinding process. Wax-based binder system is used in this study. The binder removal rate in supercritical $CO_2$ have been measured at $65^{\circ}C$, 75$^{\circ}C$ in the pressure range from 20 MPa to 28 MPa. Pores and cracks in silver bodies after sintering were observed using SEM When the super-critical $CO_2$ debinding was carried out at 75$^{\circ}C$, almost all the wax (about 70 wt% of binder) was removed in 2 hours under 28 MPa and 2.5 hours under 25 MPa.

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Multi-pole anisotropic Sr-ferrite sintered magnets fabricated by powder injection molding (분말사출성형으로 제조된 다극 이방성 Sr-페라이트 소결자석)

  • Cho, Tae-Sik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11b
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    • pp.284-287
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    • 2001
  • Multi-pole anisotropic Sr-ferrite sintered magnets has been studied by powder injection molding under applied magnetic field. The orientation of anisotropic Sr-ferrite powders higher than 80% during injection molding is achieved at the following conditions; apparent viscosity lower then 2500 poise in 1000 $sec^{-1}$ shear rate and applied magnetic field higher then 4 kOe. For the high fluidity and strength of injection molded compact, and the effective binder removal without defects during solvent extraction and thermal debinding, the optimum multi-binder composition is paraffin wax(PW)/carnauba wax(CW)/HDPE = 50/25/25 wt%. The rate of binder removal is proportional to the mean particle size of Sr-ferrite powders whereas it is inversely proportional to the content of Sr-ferrite powders and the sample thickness. The high magnetic properties of Sr-ferrite sintered magnets are; 3.8 kG of remanent flux density, 3.4 kOe of intrinsic coercivity, and 1.2 kG of surface flux density (l-mm-thick) in the direction of applied magnetic field.

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Mu7i-pole anisotropic Sr-ferrite sintered magnets fabricated by powder injection molding (분말사출성형으로 제조된 다극 이방성 SF-폐라이트 소결자석)

  • 조태식
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11a
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    • pp.284-287
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    • 2001
  • Multi-pole anisotropic Sr-fertile sintered magnets has been studied by powder injection molding under applied magnetic field. The orientation of anisotropic Sr-ferrite powders higher than 80% during injection molding is achieved at the following conditions; apparent viscosity lower then 2500 poise in 1000 sec$\^$-1/ shear rate and applied magnetic field higher then 4 kOe. For the high fluidity and strength of injection molded compact, and the effective binder removal without defects during solvent extraction and thermal debinding, the optimum multi-binder composition is paraffin wax(PW)/carnauba wax(CW)/HDPE = 50/25/25 wt%. The rate of binder removal is proportional to the mean particle size of Sr-ferrite powders whereas it is inversely proportional to the content of Sr-ferrite powders and the sample thickness. The high magnetic properties of Sr-ferrite sintered magnets are; 3.8 kG of remanent flux density, 3.4 kOe of intrinsic coercivity, and 1.2 kG of surface flux density (1-mm-thick) in the direction of applied magnetic field.

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A Study of Simple Hinge Articulator Mounting Method (단순접번 교합기의 모형부착 방법에 관한 연구)

  • Cho, Hong-Kyu
    • Journal of Technologic Dentistry
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    • v.25 no.1
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    • pp.95-102
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    • 2003
  • The purpose of this study was to show occlusion on the simple hinge articulator optionally mounted. Modelling of upper-lower jaw and simple hinge articulator were developed. This modelling of upper-lower jaw inserting wax bite was mounted imaginary on the modelling of simple hinge articulator by use of the computer simulation. From changes of THA(transverse horizontal axis)-incisor distance, Balkwill angle and THA deviation, eight types were mounted respectively. After removal of wax bite, upper-lower jaw position changing were compared with centric jaw relation. The results were as follows: 1. The change of THA-incisor distance had influence on mostly a vertical shift of upper jaw. 2. The change of Balkwill angle had influence on mostly a horizontal shift of upper jaw. 3. Inferior type in the THA deviations was the least shift of upper jaw. The above results suggest that the simple hinge articulator optionally mounted effect a shift of upper jaw.

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Epidermal Features of the Nelumbo nucifera Tissues and Lotus Effect (연꽃식물 조직의 표피 특성과 연잎효과)

  • Kim, In-Sun
    • Applied Microscopy
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    • v.42 no.2
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    • pp.95-103
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    • 2012
  • The cell surface sculpture of the plant epidermis has received great interest recently. It has also been an active area of research, as the biological microstructures of the surface, such as papillae and waxes, exhibit several unique properties, including self-cleaning character; namely the "Lotus effect" first described in the leaves of the lotus, Nelumbo nucifera. The Lotus effect is the phenomenon in which the super-hydrophobic and water-repellent nature of lotus leaves allow water drops to run off easily on the surface in a rolling and sliding motion thereby facilitating the removal of dirt particles. It is well-known that surface roughness on the micro- and nanoscale is a primary characteristic allowing for the Lotus effect. This effect is common among plants and is of great technological importance, since it can be applied industrially in numerous fields. In the present study, Nelumbo nucifera leaf and stem epidermal surfaces have been examined with a focus on the features of papillae and wax crystalloids. Both young and mature Nelumbo nucifera leaf epidermis demonstrated the Lotus effect on their entire epidermal surface. The central area of the upper epidermis, in particular, formed extremely papillose surfaces, with an additional wax layer, enabling greater water repellency. Despite the presence of wax crystalloids, epidermal surfaces of the lower leaf and stem lacking papillae, were much more easily wetted.