• 제목/요약/키워드: transmission electron microscope

검색결과 830건 처리시간 0.026초

Elevated Temperature Strength and Microstructure of Atomized and Ball-milled Al-xFe-yCr Alloys

  • Kim, Kyeong-Hwan;Chun, Byong-Sun
    • 한국분말재료학회지
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    • 제7권4호
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    • pp.197-204
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    • 2000
  • Gas atomization mechanical alloying and hot pressing have successfully made high temperature Al-9.45Fe-4.45Cr alloy. The microstructure and mechanical properties of this alloy has been studied by using optical microscope, scanning electron microscope, transmission electron microscope, X-ray diffractometer and compressive tester. It contains high concentration of transition elements of Fe and Cr, which form thermally stable dispersoids in the aluminum matrix. Proper oxidation of powders during ball milling strengthens the bulk extrudates by providing the obstacle particles. The oxide particles are very chemically and thermally stable and prevent the coarsening of the intermediate compounds.

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배추흰나비 복안의 각막 형성 (Corneal Formation of the Compound Eye in Pieris rapae L.)

  • 김창식;김우갑;김창환
    • Applied Microscopy
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    • 제24권4호
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    • pp.98-106
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    • 1994
  • The corneal formation of compound eye of Pieris rapae L., which was mostly made during pupal stage, was morphologically investigated with light microscope, scanning electron microscope and transmission electron microscope. The regeneration of the microvilli were found on the surface membranes of corneagen cells and retinular pigment cells of preommatidium after apolysis pupal cuticle. The microvilli were finally differentiated to corneal nipples of the ommatidium. The corneal cuticle was generated on the superficial layer of the preommatidium from corneagen cells and retinular pigment cells. The corneal process was also formed under the cuticular layer from the corneagen cells. The pore canal was appeared within the cuticular layer and connected with the retinular pigment cell as if the root of interommatidial hair was connected. The interommatidial hair was projected randomly among the ommatidial facets and cornal nipple was arrayed regular on the ommatidial facets. The cornea was convex lens and the refracting power by its convex shape was 4 diopter.

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Self-Organized Synthesis and Mechanism of SnO2@Carbon Tube-Core Nanowire

  • Luo, Minting;Ma, Yong-Jun;Pei, Chonghua;Xing, Yujing;Wen, Lixia;Zhang, Li
    • Bulletin of the Korean Chemical Society
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    • 제33권8호
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    • pp.2535-2538
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    • 2012
  • $SnO_2@carbon$ tube-core nanowire was synthesized via a facile self-organized method, which was in situ by one step via Chemical Vapor Deposition. The resulting composite was characterized by scanning electron microscopy, X-ray diffraction and transmission electron microscope. The diameter of the single nanowire is between 5 nm and 60 nm, while the length would be several tens to hundreds of micrometers. Then X-ray diffraction pattern shows that the composition is amorphous carbon and tin dioxide. Transmission electron microscope images indicate that the nanowire consists of two parts, the outer carbon tube and the inner tin dioxide core. Meanwhile, the possible growth mechanism of $SnO_2@carbon$ tube-core nanowire is also discussed.

Morphological Study of the Digestive Tract of the Mud Crab (Hemigrapsus Penicillatus De Haan) and the Symbiotic Crab (Pinnotheres cyclinus Shen)

  • Moon, Young-Wha;Kim, Han-Hwa
    • Animal cells and systems
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    • 제3권4호
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    • pp.407-412
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    • 1999
  • The influence of eating habits and food type on the ultrastructural characteristics of the digestive tracts was studied under the scanning and transmission electron microscopes in two crustacean decapods (Hemigrapsus penicillatus De Haan; mud crab, Pinnotheres cyclinus Shen; symbiotic crab). The relative ratio of the length of midgut versus hindgut was 1:1 in the mud crab, but 4:1 in the symbiotic crab. Observation through the scanning electron microscope revealed that the midguts of both species have densely-arranged longitudinal mucosal folds with a smooth surface. In the hindgut of the mud crab, mucosal folds were longitudinally oriented, clusters of two to five spines were observed on the cuticular surface, and the length of the spine in the distal hindgut was longer than that in the proximal portion. In the symbiotic crab, the mucosal folds were irregulary arranged, and numerous rudimentary spinal structures were noted on the cuticular surface. Through observation of a transmission electron microscope, the epithelial cells of the midgut in both species had numerous microvilli, but the length of the microvilli was slightly longer in the mud crab than in the symbiotic crab. The central layer of the basement membrane and the muscular layer of the midgut were more developed in the mud crab than in the symbiotic crab. The thickness of the cuticular layer over the hindgut surface in the mud crab was about 4 times than that of the symbiotic crab.

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Empirical relationship between band gap and synthesis parameters of chemical vapor deposition-synthesized multiwalled carbon nanotubes

  • Obasogie, Oyema E.;Abdulkareem, Ambali S.;Mohammed, Is'haq A.;Bankole, Mercy T.;Tijani, Jimoh. O.;Abubakre, Oladiran K.
    • Carbon letters
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    • 제28권
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    • pp.72-80
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    • 2018
  • In this study, an empirical relationship between the energy band gap of multi-walled carbon nanotubes (MWCNTs) and synthesis parameters in a chemical vapor deposition (CVD) reactor using factorial design of experiment was established. A bimetallic (Fe-Ni) catalyst supported on $CaCO_3$ was synthesized via wet impregnation technique and used for MWCNT growth. The effects of synthesis parameters such as temperature, time, acetylene flow rate, and argon carrier gas flow rate on the MWCNTs energy gap, yield, and aspect ratio were investigated. The as-prepared supported bimetallic catalyst and the MWCNTs were characterized for their morphologies, microstructures, elemental composition, thermal profiles and surface areas by high-resolution scanning electron microscope, high resolution transmission electron microscope, energy dispersive X-ray spectroscopy, thermal gravimetry analysis and Brunauer-Emmett-Teller. A regression model was developed to establish the relationship between band gap energy, MWCNTs yield and aspect ratio. The results revealed that the optimum conditions to obtain high yield and quality MWCNTs of 159.9% were: temperature ($700^{\circ}C$), time (55 min), argon flow rate ($230.37mL\;min^{-1}$) and acetylene flow rate ($150mL\;min^{-1}$) respectively. The developed regression models demonstrated that the estimated values for the three response variables; energy gap, yield and aspect ratio, were 0.246 eV, 557.64 and 0.82. The regression models showed that the energy band gap, yield, and aspect ratio of the MWCNTs were largely influenced by the synthesis parameters and can be controlled in a CVD reactor.

Metallurgical Failure Analysis on a Suspension Clamp in 154kV Electric Power Transmission Tower

  • 이재홍;정남근
    • KEPCO Journal on Electric Power and Energy
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    • 제7권2호
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    • pp.237-240
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    • 2021
  • Failure of a suspension clamp made of hot dip galvanized cast iron in 154kV transmission tower was investigated. Metallurgical analysis of a crack of the clamp was performed using a digital microscope, an optical microscope, and a scanning electron microscope. It was revealed that the crack surface was covered by continuous zinc layer. Distinctive casting skin was found underneath both the outer surface and crack surface. The result showed that pre-existing crack had been formed in the fabrication, and liquid metal embrittlement during hot dip galvanization may assist crack propagation.

성대용종에서 부착섬유의 형태학적 변화 (Morphologic Changes of Anchoring Fibers in Vocal Polyps)

  • 정광윤;최종욱
    • 대한기관식도과학회지
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    • 제1권1호
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    • pp.64-68
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    • 1995
  • Vocal folds injury from vocal abuse is important topics of phonosurgery. Recent advances in diagnostic equipment, phonosurgery and speech analysis equipment have provided a lot of Information about fine movement of the vocal folds. However, predicting the reaction of the vocal folds to phonatory trauma remains difficult. The vocal folds need to withstand great vibratory and shearing stress and anchoring fibers of basement membrane Bone play a role in maintaining structural integrity of histologically different epidermis and superficial layer of lamina propria(cover of vocal folds). The purpose of this study is to demonstrate the changes of anchoring fibers in vocal polyp using transmission electron microscope. Various defects were observed : a irregular thickening of basement membrane, a near absence of normal anchoring fiber, a lot of electron dense material in superficial layer of lamina propria, a destruction of hemidesmosome and many vesicles carrying electron dense material In basal keratinocyte. These observations were suggestive of a hyperactivity of basal keratinocyte of vocal folds epithelium in response to vibratory stress.

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Poxvirus under the eyes of electron microscope

  • Jaekyung Hyun
    • Applied Microscopy
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    • 제52권
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    • pp.11.1-11.9
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    • 2022
  • Zoonotic poxvirus infections pose significant threat to human health as we have witnessed recent spread of monkeypox. Therefore, insights into molecular mechanism behind poxvirus replication cycle are needed for the development of efficient antiviral strategies. Virion assembly is one of the key steps that determine the fate of replicating poxviruses. However, in-depth understanding of poxvirus assembly is challenging due to the complex nature of multi-step morphogenesis and heterogeneous virion structures. Despite these challenges, decades of research have revealed virion morphologies at various maturation stages, critical protein components and interactions with host cell compartments. Transmission electron microscopy has been employed as an indispensable tool for the examination of virion morphology, and more recently for the structure determination of protein complexes. In this review, we describe some of the major findings in poxvirus morphogenesis and the contributions of continuously advancing electron microscopy techniques.

포유류 조직비만세포의 주사전자현미경적 연구 (Scanning Electron Microscopic Study on the Tissue Mast Cells of Mammals)

  • 강호석;유기수
    • Applied Microscopy
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    • 제13권1호
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    • pp.41-47
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    • 1983
  • A Scanning electron microscope which can obtain additional information not readily available with either the light or transmission electron microscope was used to study the mast cell shape and its granules in normal mammal tissue(rat mesentery, stomach and mouse stomach) by fretting cut using liquid nitrogen. The results showed that rat mesentery and mouse stomach mast cell surfaces had no ridges and microvilli, but revealed several microvilli projecting into the surrounding connective tissue in the rat stomach mast cell. The shape of the mast cell varied from discoid(in the rat mesenteric mast cell) to ellipsoid (rat and mouse stomach), ranging from 7.5 to $10{\mu}m$ in diameter. The shape of the nucleus was ellipsoid and nucleic membrane was adherent to the outer surface of the granules. The granules, approximately 0.2 to $0.9{\mu}m$ in diameter, were various shapes. Frequently, rounded protrusions of cytoplasmic granules could be discerned under the cell membrane. Many small granules were seen in the cytoplasm.

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TEM 관련 이론해설 (6): 투과전자현미경의 고분해능 영상이론: 결맞음 (1) (Theory of High Resolution TEM Image Formation: Coherence (1))

  • 이확주
    • Applied Microscopy
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    • 제35권3호
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    • pp.105-112
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    • 2005
  • 고분해능 TEM 영상 이론의 결맞음 조사에서의 결맞음에 관한 개념을 소개하였다. 현미경에서 부분 결맞음 파동으로 인한 transfer function과 envelope의 발생을 설명하고 현미경의 분해능과 관련된 passband와 Scherzer 초점 조건을 소개하였다.