• 제목/요약/키워드: three-point flexural test

검색결과 125건 처리시간 0.023초

Fabrication and Strength Properties of LPS-SiC based materials

  • Lee, Sang-Pill;Kohyama, Akira
    • 한국해양공학회:학술대회논문집
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    • 한국해양공학회 2006년 창립20주년기념 정기학술대회 및 국제워크샵
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    • pp.25-28
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    • 2006
  • This paper dealt with the LPS process for the development of high performance SiC materials, based on the detailed analysis of their microstructure and mechanical properties. The submicron SiC powder was used for the fabrication of LPS-SiC materials. A mixture of $Al_2O_3$ and $Y_2O_3$ particles was also used as a sintering additive in the LPS process. LPS-SiC materials were fabricated at different temperatures, using various additive composition ratio ($Al_2O_3/Y_2O_3$). The total amount of additive materials ($Al_2O_3+Y_2O_3$) was fixed as 10 wt%. The characterization Of LPS-SiC materials was investigated by means of SEM, XRD and three point bending test. The LPS-SiC material represented a relative density of about 98 % and a flexural strength of about 800MPa, when it was fabricated at the temperature of $1820^{\circ}C$ and the additive compositional ratio of 1.5.

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Inhibitory effect on Streptococcus mutans and mechanical properties of the chitosan containing composite resin

  • Kim, Ji-Sun;Shin, Dong-Hoon
    • Restorative Dentistry and Endodontics
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    • 제38권1호
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    • pp.36-42
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    • 2013
  • Objectives: This study evaluated the antibacterial effect and mechanical properties of composite resins ($L_{CR}$, $M_{CR}$, $H_{CR}$) incorporating chitosan with three different molecular weights (L, Low; M, Medium; H, High). Materials and Methods: Streptococcus (S). mutans 100 mL and each chitosan powder were inoculated in sterilized 10 mL Brain-Heart Infusion (BHI) solution, and was centrifuged for 12 hr. Absorbance of the supernatent was measured at $OD_{660}$ to estimate the antibacterial activities of chitosan. After S. mutans was inoculated in the disc shaped chitosan-containing composite resins, the disc was cleansed with BHI and diluted with serial dilution method. S. mutans was spread on Mitis-salivarius bacitracin agar. After then, colony forming unit (CFU) was measured to verify the inhibitory effect on S. mutans biofilm. To ascertain the effect on the mechanical properties of composite resin, 3-point bending and Vickers hardness tests were done after 1 and 3 wk water storage, respectively. Using 2-way analysis of variance (ANOVA) and Scheffe test, statistical analysis was done with 95% significance level. Results: All chitosan powder showed inhibition effect against S. mutans. CFU number in chitosan-containing composite resins was smaller than that of control resin without chitosan. The chitosan containing composite resins did not show any significant difference in flexural strength and Vickers hardness in comparison with the control resin. However, the composite resin, $M_{CR}$ showed a slightly decreased flexural strength and the maximum load than those of control and the other composite resins $H_{CR}$ and $L_{CR}$. Conclusions: $L_{CR}$ and $H_{CR}$ would be recommended as a feasible antibacterial restorative due to its antibacterial nature and mechanical properties.

$MoSi_2$ 복합재료의 특성 (Properties of $MoSi_2$ Based Composite Materials)

  • 이상필;조경서;이진경;배동수
    • 한국해양공학회지
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    • 제23권6호
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    • pp.93-98
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    • 2009
  • The mechanical properties of $MoSi_2$ based composites containing various types of reinforcement, such as SiC, $ZrO_2$, and W, were investigated, based on detailed examinations of their microstructures. $MoSi_2$ based composites were fabricated at a temperature of $1350^{\circ}C$ using a hot-press device. The volume fraction of SiC and $ZrO_2$ particles in this composite system was fixed as 20%. The volume fraction of three types of W particles was changed from 10% to 30%. The characteristics of the $MoSi_2$ based composites were determined by means of optical microscopy and a three-point bending test. The addition of W particles to the $MoSi_2$ powders exhibited a sufficient improvement in the microstructure and mechanical property of the sintered $MoSi_2$ materials, compared to those of SiC and $ZrO_2$ particles. In particular, W/$MoSi_2$ composites containing W particles of 20 vol% represented a good flexural strength of about 530MPa at room temperature, accompanying a relative density of about 92%. The flexural strength of the W/$MoSi_2$ composites tended to decrease with an increase in the average size of the W particles.

온성방법과 단면형태가 수종의 의치상 수리레진의 결합강도에 미치는 영향 (THE EFFECT OF PROCESSING METHOD AND SURFACE DESIGN ON THE TRANSVERSE STRENGTH OF REPAIRED DENTURE BASE RESIN)

  • 김강남;배태성;한중석
    • 대한치과보철학회지
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    • 제34권4호
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    • pp.665-674
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    • 1996
  • This study was designed to evaluate the effect of processing method and surface design on the transverse strength of repaired denture base resin. Three heat-cured denture base resins(Vertex, Lucitone, Lang), one cold-cured resin(Lang), and one light-cured resin(Dentacolor gingiva material) were used for repair purpose. The specimens for 3-point flexure test were fabricated by five processing methods such as self-curing, pressure pot, boiling water, processing, and light curing. Finally to evaluate the effect of surface designs for repaired resin, three surface designs(butt, bevel, inverse bevel) were tested. Within the limit of this study, following conclusions were drawn. 1. Lucitone denture base material showed highest flexural strength of $131.37{\pm}2.15MPa$, and there were significant differences in stength between Lucitone and other resins. 2. Between two different self curing methods, self curing repair resin, Lang, cured by pressure pot method showed highest flexural strength, $58.49{\pm}4.89MPa$. 3. Among the heat cured repair resins, maximum transverse strength value of $88.69{\pm}16.60MPa$ was recorded in Lucitone group cured by processing method. 4. Inverse bevel joint design showed significantly higher bond strength than butt joint group, Maximum bond strength was $59.36{\pm}1.33MPa$ in inverse bevel joint design group.

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Assessment of effect of accelerated aging on interim fixed dental materials using digital technologies

  • Omar, Alageel;Omar, Alsadon;Haitham, Almansour;Abdullah, Alshehri;Fares, Alhabbad;Majed, Alsarani
    • The Journal of Advanced Prosthodontics
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    • 제14권6호
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    • pp.360-368
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    • 2022
  • PURPOSE. This study assessed the physical and mechanical properties of interim crown materials fabricated using various digital techniques after accelerated aging. MATERIALS AND METHODS. Three groups of interim dental restorative materials (N = 20) were tested. The first group (CO) was fabricated using a conventional manual method. The second group (ML) was prepared from prefabricated resin blocks for the milling method and cut into specimen sizes using a cutting disc. The third group (3D) was additively manufactured using a digital light-processing (DLP) 3D printer. Aging acceleration treatments using toothbrushing and thermocycling simulators were applied to half of the specimens corresponding to three years of usage in the oral environment (N = 10). Surface roughness (Ra), Vickers microhardness, 3-point bending, sorption, and solubility tests were performed. A 2-way analysis of variance (ANOVA) and Fisher's multiple comparison test were used to compare the results among the groups. RESULTS. The mean surface roughness (Ra) of the resin after accelerated aging was significantly higher in the CO and ML groups than that before aging, but not in the 3D group. All groups showed reduced hardness after accelerated aging. The flexural strength values were highest in the 3D group, followed by the ML and CO groups after accelerated aging. Accelerated aging significantly reduced water sorption in the ML group. CONCLUSION. According to the tested material and 3D printer type, both 3D-printed and milled interim restoration resins showed higher flexural strength and modulus, and lower surface roughness than those prepared by the conventional method after accelerated aging.

노출강연선으로 보강된 하이브리드 건축용 OCB보의 실물모형 재하실험연구 (The Experimental Study of Full-scale Optimized Composite Beam (OCB) Reinforced with Open Strands)

  • 이두성;김태균;채규봉
    • 콘크리트학회논문집
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    • 제27권5호
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    • pp.471-480
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    • 2015
  • 최근 국내의 건축구조는 공간활용을 극대화할 수 있도록 계획되고 있다. 공간활용의 장점을 실현하기 위하여 하이브리드 OCB (Optimized Composite Beam)를 개발하였다. 건축용 OCB는 부모멘트 구간에서는 노출강연선으로 보강된 H형강으로 구성되고 정모멘트 영역에서는 PSC 구조로 구성된다. 본 연구에서는 건축용 OCB의 휨성능을 조사하였다. 15 m 길이의 시험체를 제작하여 3점 휨실험을 실시하였다. 실험을 통해서 다음과 같은 결과를 얻었다. 1) 시험체의 재하실험에서 초기 균열은 설계사용 하중의 171%에서 발생되었다. 2)사용하중에서 처짐은 건축구조설계기준에 제시된 허용처짐량 이내로 만족하였다. 3)균열의 양상, 파괴모드 그리고 극한하중 등의 실험결과는 3D 수치해석결과와 비교검토되었다. 본 실험연구 결과로부터 건축용 OCB보의 구조적인 신뢰성이 입증되었다.

굽힘 하중에 의한 복합재료 파손 예측 연구 (Failure Prediction for Composite Materials under Flexural Loading)

  • 김진성;노진호;이수용
    • 한국항공우주학회지
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    • 제45권12호
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    • pp.1013-1020
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    • 2017
  • 본 연구에서는 굽힘 하중을 받는 복합재료 적층판에 대한 파손 강도를 예측하기 위하여 2D 변형률 기반의 파손 이론을 적용한 유한요소 해석을 수행하였다. 복합재료 적층판 내각 층의 파손 모드에 따른 강성저하를 고려하기 위해 점진적 파손 해석 방법을 적용하였다. 크로스 플라이와 준등방성 복합재 적층판에 대하여 3점 굽힘 시험을 수행하였다. 최대응력 이론, 최대 변형률 이론, 그리고 Tsai-Wu 파손 이론을 적용한 유한요소 해석을 수행하였다. 시험 및 파손 이론에 따른 해석 결과 비교를 통하여 2D 변형률 파손 이론의 정확성을 검증하였다.

Analysis of notch depth and loading rate effects on crack growth in concrete by FE and DIC

  • Zhu, Xiangyi;Chen, Xudong;Lu, Jun;Fan, Xiangqian
    • Computers and Concrete
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    • 제24권6호
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    • pp.527-539
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    • 2019
  • In this paper, the fracture characteristics of concrete specimens with different notch depths under three-point flexural loads are studied by finite element and fracture mechanics methods. Firstly, the concrete beams (the size is 700×100×150 mm) with different notch depths (a=30 mm, 45 mm, 60 mm and 75 mm respectively) are tested to study the influence of notch depths on the mechanical properties of concrete. Subsequently, the concrete beams with notch depth of 60 mm are loaded at different loading rates to study the influence of loading rates on the fracture characteristics, and digital image correlation (DIC) is used to monitor the strain nephogram at different loading rates. The test results show that the flexural characteristics of the beams are influenced by notch depths, and the bearing capacity and ductility of the concrete decrease with the increase of notch depths. Moreover, the peak load of concrete beam gradually increases with the increase of loading rate. Then, the fracture energy of the beams is accurately calculated by tail-modeling method and the bilinear softening constitutive model of fracture behavior is determined by using the modified fracture energy. Finally, the bilinear softening constitutive function is embedded into the finite element (FE) model for numerical simulation. Through the comparison of the test results and finite element analysis, the bilinear softening model determined by the tail-modeling method can be used to predict the fracture behavior of concrete beams under different notch depths and loading rates.

CAD/CAM 전용 금속 합금과 주조용 합금의 세라믹 결합강도에 관한 연구 (A Study on the Metal-Ceramic Bond Strength of CAD/CAM Metal Disk Alloy and Casting Alloy)

  • 정효경;곽동주
    • 대한치과기공학회지
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    • 제35권2호
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    • pp.89-95
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    • 2013
  • Purpose: The purpose of this study was to evaluate bond strength of Metal Disk alloy and casting alloy. Methods: Metal specimens were divided into 4 groups for each alloy. Three point flexural test were used to measure the bond strength of CAD/CAM metal alloy and casting alloy. Statistical analysis was done using the Statistical Package for Social Sciences version 19.0 for Windows. As for the analysis methods, the study used Kruskal-Wallis test. Results: The average bonding strengths of Group 1 to porcelain was $36.7{\pm}9.90$ MPa, Group 2 to porcelain was $37.68{\pm}4.51$ MPa, Group 3 to porcelain was $36.43{\pm}6.57$ MPa, Group 4 to porcelain was $42.88{\pm}6.81$ MPa, Each group was not significantly different. Conclusion: Bond strength of Casting alloy is equal to or higher than bond strength of CAD/CAM Metal Disk alloy. Alloy clinical bond strength is 25 MPa, So CAD/CAM Metal Disk alloy can be used as dental material.

광중합형 레진의 3점 굴곡 강도와 이축 굴곡 강도 측정 방법에 대한 상대적 신뢰도의 비교 (THE COMPARISON OF RELATIVE RELIABILITY ON BIAXIAL AND THREE POINT FLEXURAL STRENGTH TESTING METHODS OF LIGHT CURING COMPOSITE RESIN)

  • 서덕규;노병덕
    • Restorative Dentistry and Endodontics
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    • 제31권1호
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    • pp.58-65
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    • 2006
  • 이번 실험의 목적은 이축 굴곡 강도 시험의 복합레진에서의 적용가능성을 위해 기존의 3점 굴곡 강도 시험과 이축 굴곡 강도 시험을 이용하여 치과용 광중합형 레진의 강도를 측정하고, 이를 Weibull modulus를 이용하여 상대적 신뢰도를 비교하는 것이다. 이번 실험에 사용된 재료는 $MICRONEW^{TM},\;RENEW^{(R)}$ (Bisco, Schaumburg, USA)의 두 가지 광중합형 수복 재료이다. 이축 굴곡 강도 측정에는 International Organization for Standardization (ISO) 6872 규정에 따라 piston-on-3-ball test를 사용하였으며 검사 시편은 직경이 각각 12 mm (지지원의 반지름 3.75 mm), 16 mm (지지원의 반지름 5 mm), 두께가 각각 0.5 mm, 1 mm, 2 mm인 여섯 개의 군으로 나누어 제작하였으며 각 군당 시편을 20개씩 제작하였다. $MICRONEW^{TM}$$RENEW^{(R)}$의 실험 결과, 이축 굴곡 강도가 3점 굴곡 강도보다 높은 평균값을 나타내었고 이축 굴곡 강도의 모든 군이 3점 굴곡 강도보다 높은 Weibull modulus 값을 보여, 이축 굴곡 강도 시험이 상대적으로 실험적 오차의 영향을 적게 받는 방법으로 신뢰 할 수 있었다. 또한 이축 굴곡 강도 시험에서 시편의 두께가 2 mm일 때 가장 높은 Weibull modulus를 나타내었으며 이축 굴곡 강도시험군 중, $MICRONEW^{TM}$의 두께 2 mm군에서는 지지원의 반지름에 따른 굴곡 강도의 통계학적 유의차이가 없었고 (p>0.05), 이를 제외한 모든 군에서 시편의 두께와 지지원의 반지름에 따른 굴곡 강도의 통계학적 유의차이가 있었다 (p<0.05). 위의 결과로 미루어 볼 때 두께 2 mm군에서 이축 굴곡 강도는 기존의 3점 굴곡 강도 시험보다 우수한 것으로 추천할 수 있는 방법이다.