• Title/Summary/Keyword: solution mixing

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A Study on the reparation of Cobalt Oxide Powders by the Emulsion Evaporation Technique (에멀젼 증발법에 의한 산화코발트 분말의 제조에 관한 연구)

  • 손성호;안재우;이응조
    • Journal of the Korean Ceramic Society
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    • v.30 no.5
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    • pp.411-419
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    • 1993
  • A process for the preparation of cobalt oxide powders was developed by the evaporaton of emulsion containing cobalt. The characteristics of powders were examined by means of DTA, X-ray diffracton, SEM, PSA. Cobalt oxide powders were produced by evaporating the emulsion prepared by mixing cobalt sulfate solution and organic phase consisted of kerosene, Span 80 and D2EHPA in the kerosene bath at 16$0^{\circ}C$, then the precursor obtained was calcined at 100$0^{\circ}C$. As the concentration of cobalt ions in the aqueous solution, Span 80 and the stirring speed increased, the mean size of cobalt oxide powders decreased and the size distribution was improved. At the volume ratio of one of the aqueous to organic phase, the finest mean size and the optimum size distribution was obtained. On the other hand the concentration of D2EHPA and liquid paraffin had little effect on the mean size as well as on the size distribution of powders.

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Electrochemical Characteristics of Silicon-carbon Composite Anodes for Lithium Rechargeable Batteries

  • Lee, Jaeho;Won, Sora;Shim, Joongpyo;Park, Gyungse;Sun, Ho-Jung;Lee, Hong-Ki
    • Transactions on Electrical and Electronic Materials
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    • v.15 no.4
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    • pp.193-197
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    • 2014
  • Si-carbon composites as anode materials for lithium rechargeable batteries were prepared simply by mixing Si nanoparticles with carbon black and/or graphite through a solution process. Si nanoparticles were well dispersed and deposited on the surface of the carbon in a tetrahydrofuran solution. Si-carbon composites showed more than 700 mAh/g of initial capacity under less than 20% loading of Si nanoparticle in the composites. While the electrode with only Si nanoparticles showed fast capacity fading during continuous cycling, Si-carbon composite electrodes showed higher capacities. The cycle performances of Si nanoparticles in composites containing graphite were improved due to the role of the graphite as a matrix.

Influence of In/Sn Ratio and Precursor on the Electrical Properties of Solution-processed Indium-Tin-Oxide Electrodes (용액공정 Indium-Tin-Oxide 전극에서 In/Sn Ratio 및 Precursor가 전기적 특성에 미치는 영향)

  • Kim, Na-Young;Kim, Yong-Hoon;Han, Jeong-In
    • Proceedings of the KIEE Conference
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    • 2011.07a
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    • pp.2013-2014
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    • 2011
  • Indium tin oxide (ITO) thin films have been deposited onto bare glass substrates by sol-gel process. The solution was prepared by mixing indium precursor and tin precursor dissolved in 2-methoxyethanol at $75^{\circ}C$ for 12 hours. Indium tin oxide films were prepared by slowly heat up to $200^{\circ}C$ for 10 minutes and annealed at $350^{\circ}C$ for 1 hour. In this paper, we researched simple and inexpensive sol-gel process. To find the optimal ratio of In/Sn to reduce electric resistance in ITO made by sol-gel process, we assessed electric properties varying the ratio of In and Sn precursor.

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An Efficient Algorithm for a Block Angular Linear Program with the Same Blocks (부분문제가 같은 블록대각형 선형계획문제의 효율적인 방볍)

  • 양병학;박순달
    • Journal of the Korean Operations Research and Management Science Society
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    • v.12 no.2
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    • pp.42-50
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    • 1987
  • This objective of this paper is to develop an efficient method with small memory requirement for a feed-mixing problem on a micro computer. First this method uses the decomposition principle to reduce the memory requirement. Next, the decomposition principle is modified to fit the problem. Further four different variations in solving subproblems are designed in order to improve efficiency of the principle. According to the test with respect to the processing time, the best variation is such that the dual simplex method is used, and the optimal basis of a previous subproblem is used as an initial basis, and the master problem is (M +1) dimensional. In general, the convergence of solution becomes slower near the optimal value. This paper introduces a termination criterion for a sufficiently good solution. According to the test, 5%-tolerence is acceptable with respect to the relation between the processing time and optimal value.

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Bifidobacterium Fermentation of Rice and Apple Pomace Mixture (쌀과 사과박 혼합물을 이용한 Bifidobacterium발효제품의 개발)

  • 이주연;박종현;장학길;목철균
    • Microbiology and Biotechnology Letters
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    • v.27 no.4
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    • pp.333-338
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    • 1999
  • This study was aimed to develop a value-added fermented products from rice and apple pomace using Bifidobacterium fermentation. The Bifidobacterium fermentation system of the mixture of rice and apple pomace was developed, and the physicochemical properties of the products were investigated. After 4 different bifidobacteria were compared for their fermentation capability and sensory properties of the fermented product, Bifidobacterium FBD-13 and FBD-22 were selected as appropriate strains for the fermentation of saccharified rice solution(SRS). The optimum inoculation level was 2% and the optimum fermentation time was 42 hrs. When wet apple pomace(WAP) was added to SRS, it contributed to the improvement of sensory properties of the fermented products and the optimum mixing ratio was 40% WAP and 60% SRS in weight. For the fermentation of the mixture of WAP and SRS, Bifidobacterium FBD-27 and FBD-22 were selected as suitable strains.

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Studies on the Structure of Transparent Glass Ceramics (투명 결정화유리의 구조에 관한 연구)

  • 박용완;박원규;김대혁
    • Journal of the Korean Ceramic Society
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    • v.27 no.2
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    • pp.288-296
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    • 1990
  • Parent glasses for the experiments were prepared to be ratio of Li2O : Al2O3 : SiO2=4.5 : 25 : 70.5 as basic components, and TiO2 and ZrO2 in the mixing ratio of 1 : 1 were added as the nucleating agents, whose contents were increased in each sample. DTA, XRD, SEM, IR were observed, and thermal expansion and transmissivities were measured for the crystallized samples under the controlled heat-treatments. The transformation temperatures and the dilatometric softening temperatures in thermal expansion curves, and also the exothermic peaks in differential thermo-analytical curves were shifted to lower temperature. The crystal phase deposited through the heat-treatment was identified as ${\beta}$-quartz solid solution with XRD and IR analysis. The crystalline phases in oopactified samples were ${\beta}$-spodumene coexiting with ${\beta}$-quartz solid solution. The samples having more than 3% nucleating agents were transparent. The crystallized grain sizes were ranged 0.05 to 0.1$\mu\textrm{m}$. The crystallized transparent samples were exceeded 85% in the transmissivity.

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The Enhancement of Corrosion Resistance for WC-Co by Ion Beam Mixed Silicon Carbide Coating

  • Yeo, Sun-Mok;Kim, Dong-Jin;Park, Jae-Won
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.08a
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    • pp.101-101
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    • 2010
  • A strong adhesion of a silicon carbide (SiC) coating on a WC-Co substrate was achieved through an ion beam mixing technique and the corrosion resistance of the SiC coated WC-Co was investigated by means of a potentiodynamic electrochemical test. In the case of 1 M NaOH solution, a corrosion current density for a SiC coated WC-Co with a heat treatment at $500^{\circ}C$ displays about 50 times lower than that for the as-received WC-Co. However, in the case of 0.5 M H2SO4 solution, a corrosion current density for a SiC coated WC-Co displays about 3 times lower than that for as-received WC-Co. We discussed the physical reasons for the changes of the corrosion current densities at the different electrolytes.

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Selection and Bacterialization into Rootzone of the Various Plant Growth Promoting Rhizobacteria in Peatmoss Compost on the Early Growth of Cucumber and Tomato Plug Seedlings (수종의 식물생장촉진 근권미생물의 분리 및 근권처리가 오이와 토마토 플러그묘의 초기생장에 미치는 영향)

  • 조자용;김광수;정순주
    • Korean Journal of Organic Agriculture
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    • v.6 no.1
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    • pp.151-160
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    • 1997
  • Azospirillum sp., photosynthetic bacteria(Rhodopseudomonas sp.) and Pseudomonas sp. were separated and screened from soil and soilless culture, and identificated. The antifungal activities against root-infected pathogens and plant growth promoting effects of the cultured solution of the starins(5.0$\times$105 cells/$m\ell$) in the peatmoss compost on the early growth of cucumber and tomato seedling were investigated. Azospirillum sp. and Pseudomonas sp. showed a antifungal activities against Fusarium sp., Pythium sp. and Rhizoctonia sp in thed ranges of 51.0% to 72.0% on potato dextrose agar medium, however photosynthetic bacteria had not antifungal activities. When cultured solution of Azospirillum sp., photosynthetic bacterial and Pseudomonas sp. were bacterialized by mixing with peatmoss compost, early growth of cucumber and tomato in terms of plant height, number of leaves, leaf area, root length, fresh anf dry weight of leaf, stem and root were promoted, especially photosynthetic bacteria had a the best plant growth promting activities.

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A Study on Pattern Formation of Ultra Definition Display Panel Applying Phosphoric Acid (인산을 적용한 Ultra Definition 디스플레이 패널의 패턴 형성에 관한 연구)

  • Kim, Min-Su;Cho, Ur Ryong
    • Journal of the Semiconductor & Display Technology
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    • v.13 no.3
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    • pp.13-19
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    • 2014
  • Phosphoric acid was used as etching agent instead of conventional peroxide - based chemicals for forming pattern of ultra definition display. Etchant was synthesized by mixing etching agent, oxidation agent, buffer solution, and additive into solvent, deionized water. Thicknesses of copper, main metal of ultra definition display, for etching, were 10,000 and $30,000{{\AA}}$. Etch stop of good low skew for proper pattern formation has been occurred at the content ratio of phosphoric acid 60 - 64%, nitric acid 4 - 5%, additive(potassium acetate) 1 - 3%. Buffer solution(acetic acid) decreased the metal contact angle $63.07^{\circ}$ to $42.49^{\circ}$ for benefiting pattern formation. Content variations on four components (phosphoric acid, nitric acid, acetic acid, potassium acetic acid) of the etchant with storage time were within 3 wt% after 24 hrs of etching work.

Microencapsulation of Anchovy Oil by Sodium Alginate (알긴산소다를 이용한 멸치어유의 미세캡슐화)

  • 임상빈;좌미경
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.28 no.4
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    • pp.890-894
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    • 1999
  • Microencapsulation of anchovy oil as a core material in sodium alginate as a wall material was inves tigated. Microencapsulation was accomplished by injecting an oil/water emulsion, consisting of a mixture of liquefied sodium alginate and emulsifier, under high pressure through an orifice submerged in a calcium lactate solution. Microcapsules suspended in a dispersion fluid were observed under a fluorescence mi croscope to verify the presence of the capsules and to note coalescence or degradation of the capsules. Optimum conditions for microencapsulation of anchovy oil were obtained when 1.0% aqueous solution of sodium alginate contained 3% of a 1:1 ratio of ESPR 25(polyglycerine+polylinoleate) and TW 20(sorbitan laurate+ethylene oxide) as an emulsifier in terms of capsule size and size distribution, and emulsion stability. The airless sprayer produced microcapsules with a diameter between 15.9 and 73.9 m with different concentration of a wall material. The optimum mixing ratio of wall material to core material was 90:10(wt/wt). 0.2% calcium lactate was appropriate as a dispersion fluid.

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