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A STUDY ON THE HARDNESS IN VISIBLE LIGHT COMPOSITE RESIN (광중합(光重合) 레진의 경도측정(硬度測定)에 관(關)한 연구(硏究))

  • Lee, Myung-Jong
    • Restorative Dentistry and Endodontics
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    • v.14 no.1
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    • pp.179-188
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    • 1989
  • The purpose of this study was to measure Micro vicker's hardness of 4 kinds of anterior Composite resins (Pyrofil light bond anterior, Lite-fil anterior, Photo clear fil anterior, Silux) and 6 kinds of posterior Composite resin (Pyrofil light bond posterior. Lite-fil posterior, Photo clear fil posterior, Occlusin posterior, Palfique light posterior, P-30, posterior) according to deference of depth and distance of light tip from surface of composite resin. Each composite resin was filled into Teflon tube of 5mm in diameter and 5mm in depth, celluloid matrix was covered and the light in accordance with each composite resin was irradiated in distance of zero millimeter and 1 cm from light tip to surface of composite resin for 30 seconds. Specimens were sectioned longitudinally with cutting device. Microvicker's hardness measurements ware made at the depth of surface, 1mm, 2mm, 3mm, 4mm and 5mm from the surface to deep portion. Vicker's hardness numbers were taken on each depth under 200gm load for 30 seconds with MVK-E. The following results were: 1. The highest hardness value was measured at 1 mm depth. Then the deeper the depth, the lesser the hardness was observed. 2. The hardness value of anterior composite resins is lower than one of posterior composite resins. 3. Hardness number of composite resin irradiated in distance of zero millimeter from surface of composite resin was higher than one of 1 cm from surface of composite resin. 4. The pattern of hardness change at varying depth was similar to all the experimental material with no relation to distance of light from specimen.

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A Study for Improving Direction of Legal Regime and Policy for Protecting our Underwater Cultural Heritages (수중문화유산 보호를 위한 법제도 정비 및 효율적 관리방안)

  • Park, Seong-Wook
    • Ocean and Polar Research
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    • v.27 no.2
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    • pp.171-179
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    • 2005
  • Korea has many underwater cultural heritages within the east, west and south seas surrounding the Peninsula that indicate historically important sealanes for trade and transportation. As these underwater cultural heritages are the objects of despoilment because of their relatively easy access through modern technology, their often high historical and priceless value demands strong protection similar to or better than the land cultural properties. Currently, Korea does not have any concrete laws or regulations for the protection of underwater cultural heritages. Thus, these heritages iu, somewhat temporary and inappropriately subjected to laws and regulations relating to provisions of individual Laws concerning protection of cultural properties act, and statute of excavation of material fir buried national property, lost articles act etc.. Internationally, the UNESCO Convention on the Protection of the Underwater Cultural Heritage was adopted but not yet entered into force. Therefore, the protection of underwater cultural heritage has become an urgent matter. In this regard, this article's main purpose is to provide recommendations for improving direction of legal regime and policy for protecting our underwater cultural heritages. These legal regimes need provisions for definition of the underwater cultural heritage, scope of application, ownerships, jurisdictions and protection measures. And suggestions are provided in regard to policies for the protection of underwater cultural heritages that may improve organization and cooperation among concerned ministries and agencies, compensation system, restrictions for excavation of underwater relics, efficiency of survey of underwater surface and information system.

A Study on the Properties of Mortar with Recycled Fine Aggregate (순환잔골재를 사용한 모르타르의 제물성에 관한 실험적 연구)

  • Moon, Dae-Joong;Choi, Jae Jin
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.4 no.1
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    • pp.96-100
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    • 2009
  • The properties of recycled fine aggregates which had different source concrete were examined by mortar test. With higher strength of source concrete, specific gravity of recycled fine aggregate was higher and absorption of recycled fine aggregate was lower due to reduction of the volume of adhered cement paste. The compressive strength and flexible strength of mortar with recycled fine aggregate were affected by the interface boundary of new mortar and the strength of adhered mortar. Strength development of mortar with recycled fine aggregate reduced because recycled fine aggregate become a porous material with the smaller strength of source concrete. The drying shrinkage of mortar was about$800{\sim}2000{\mu}m/m$. It was about 1.5 times than that of mortar with natural fine aggregate. Relative dynamic modulus of elasticity was a similar level with that of mortar with natural fine aggregate.

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Manufacturing and Properties of Low Vacuum Plasma Sprayed W-Carbide Hybrid Coating Layer (진공 플라즈마 스프레이 공정을 이용한 W계 복합 코팅층의 제조 및 특성 연구)

  • Cho, Jin-Hyeon;Jin, Young-Min;Ahn, Jee-Hoon;Lee, Kee-Ahn
    • Journal of Powder Materials
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    • v.18 no.3
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    • pp.226-237
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    • 2011
  • W-ZrC and W-HfC composite powders were fabricated by the Plasma Alloying & Spheroidization (PAS) method and the powders were sprayed into hybrid coating layers by using Low Vacuum Plasma Spray (LVPS) process, respectively. Microstructure, mechanical properties, and ablation characteristics of the fabricated coating layers were investigated. The LVPS process led to successful production of W-Carbide hybrid coatings, approximately 400 ${\mu}M$ or above in thickness. As the substrate preheating temperature increased from $870^{\circ}C$ to $917^{\circ}C$, the hardness of the W-ZrC coating layer increased due to decreased porosity. Vickers hardness showed higher value (about 108.4 HV) in W-ZrC hybrid coating material compared to that of W-HfC while adhesive strength was found to be similar in both coating layers. The plasma torch test revealed good ablation resistance of the W-Carbide hybrid coating layers. The relatively high performance W-ZrC coating layer at the elevated temperature is thought to be attributed to both the strengthening effect of ZrC particle remained in the layer and the formation of ZrO2 phase with high temperature stability.

Tensile Strength Variation of Binary Tablets Produced by Planetary Ball Milling (유성볼밀링으로 제조한 2성분 정제의 인장강도 변화)

  • Sim, Chol-Ho
    • Journal of Pharmaceutical Investigation
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    • v.38 no.1
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    • pp.1-8
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    • 2008
  • Planetary ball mill was used to decrease and control the particle size of excipients. The effects of the weight of sample and the revolution number of mill, and grinding time on the particle size of the ground sample were analyzed by response surface methodology. The optimum conditions for the milling of microcrystalline cellulose were 38.82 g of the weight of sample and 259 rpm of the revolution number of mill, and 45 minutes of grinding time. The predicted value of the particle size at the these conditions was $19.02{\mu}m$, of which the experimental value at the similar conditions was $18.68{\mu}m$. The tensile strength of tablets of single-component powders, such as microcrystalline cellulose, hydroxypropylmethyl cellulose and starch, binary mixtures and ground binary mixtures of these powder were measured at various relative densities. It was found that the logarithm of the tensile strength of the tablets was proportional to the relative density. A simple model, based upon Ryshkewitch-Duckworth equation that was originally proposed for porous materials, has been developed in order to predict the relationship between the tensile strength and relative density of ground binary tablets based on the properties of the constituent single-component powders. The validity of the model has been verified with experimental results for ground binary mixtures. It has demonstrated that this model can well predict the tensile strength of ground binary mixtures based upon the properties of single-component powders, such as true density, and the compositions. When the tensile strength of the mixture of microcrystalline cellulose hydroxypropylmethyl cellulose (90:10) and the ground mixture of them were compared, the tensile strength of the ground mixture decreased widely from 45.3 to 5.6% compared to the mixture in case the relative density of tablets was in the range of $0.7{\sim}0.9$. When the tensile strength of the mixture of microcrystalline cellulose starch (80:20) and the ground mixture of them were compared, the tensile strength of the ground mixture decreased widely from 31.0 to 11.6% compared to the mixture in case the relative density of tablets was in the range of $0.7{\sim}0.9$.

Physical Properties of Sulfur Concrete with Modified Sulfur Binder (유황개질 바인더를 사용한 유황 콘크리트의 물리적 특성)

  • Bae, Sung Geun;Gwon, Seong Woo;Kim, Se Won;Cha, Soo Won
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.34 no.3
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    • pp.763-771
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    • 2014
  • Recently, a huge amount of sulfur has been produced as a byproduct of petroleum refining processes in Korea. Sulfur concrete is made of modified sulfur binder instead of cement paste, which has advantages of reducing $CO_2$ emission from cement industry as well as utilizing surplus sulfur. Also, sulfur concrete is a sustainable material that can be repetitively recycled. In this study, the physical properties of sulfur concrete are experimentally investigated. From the test results, sulfur concrete showed compressive strengths higher than at least 50MPa. Also, the unit weight, modulus of elasticity and splitting tensile strength of sulfur concrete was similar to that of Portland cement concrete (PCC). The coefficient of thermal expansion of sulfur concrete was a little larger than that of Portland cement concrete and sulfur concrete with mineral filler is helpful to lower the coefficient of thermal expansion. recycled aggregate sulfur concrete resulted in a slight reduction in the compressive strength, but sulfur concrete with recycled aggregate can achieve the high strength characteristics.

Manufacture of $BaTiO_3$ Powders by Gel-hydrothermal Method (겔의 수열합성법에 의한 다공성 구형 $BaTiO_3$ 미분체의 제조)

  • Kim, Yong-Ryul
    • Journal of the Korean Applied Science and Technology
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    • v.22 no.4
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    • pp.306-314
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    • 2005
  • In this study, spherical $pre-BaTiO_3$ particles are prepared by gelation and aging process in autoclave without catalysts. The (Ba-Ti) gel used as a starting material was prepared by aging mixtures of titanyl acylate with barium acetate aqueous solution([glacial acetic acid (AcOH)]/[titanium isopropoxide (TIP)] 4, [barium acetate]/[TIP] 1) at $45^{\circ}C$ for 48hrs. XRD and SEM results for the (Ba-Ti) gel sample at aging process showed that the gel was formed via aggregation of the fine particles. It seems to be the primary particles of bulk (Ba-Ti) gel amorphous, but the spatial arrangement of barium and titanium in the (Ba-Ti) gel is similar to that in crystalline $BaTiO_3$ particles. From XRD and FT-IR. spectroscopy analysis it was found that the crystal structure of the prepared particles continuously transformed from amorphous to tetragonal as the calcination temperature increased, and crystallized spherical cubic and tetragonal $BaTiO_3$ powder obtained at the very low calcination temperature between $500^{\circ}C$ and $900^{\circ}C$ after 1hrs of heat treatment respectively. According to BET analysis result, final particle have pore structure of ink bottle shape which is produced by aggregation of fine spherical particles with surface area of $280m^2/g$ and average pore size of 130nm.

Electrochemical Behavior of Si/Cu/Graphite Composite Anode for Lithium Secondary Battery (리튬이차전지용 Si/Cu/Graphite 복합체 음극의 전기화학적 거동)

  • Kim, Hyung-Sun;Chung, Kyung-Yoon;Cho, Won-Il;Cho, Byung-Won
    • Journal of the Korean Electrochemical Society
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    • v.12 no.2
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    • pp.162-166
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    • 2009
  • The carbon-coated Si/Cu powders were synthesized by mechanical ball-milling and hydrocarbon gas decomposition methods at high temperature. The carbon-coated Si/Cu powder was used as anode for lithium secondary battery and its electrochemical behavior was investigated. In addition, the carbon-coated Si/Cu/graphite composite anode material was prepared using natural graphite powder and their electrochemical characteristics were compared with natural graphite anode. The specific capacity of carbon-coated Si/Cu anode increased to the initial 10 cycles. The carbon-coated Si/Cu/graphite composite anode exhibited the reversible specific capacity of 450mAh/g and the first cycle efficiency of 81.3% at $0.25mA/cm^2$. The cycling performance of the composite anode was similar to that of pure graphite anode except the reversible specific capacity value.

GEOMETRICAL ANALYSIS ON THE DENTOFACIAL COMPOSITION OF KOREAN BEAUTIFUL WOMAN (한국 미인의 치아안면구도에 대한 기하학적 분석)

  • Shin Young-Ho;Oh Sang-Chun
    • The Journal of Korean Academy of Prosthodontics
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    • v.42 no.5
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    • pp.524-534
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    • 2004
  • Statement of problem: The meaning of the beauty has a little different nature according to a time, culture, and nation. Purpose : This study was undertaken to estimate the geometric esthetic criteria for Korean woman by analysis of facial photograph in a smiling. Material and methods: The facial photographs of 678 Korean beautiful woman were collected from Miss Korea candidates(from 1971 to 2003 year). The dento-facial composition was measured and analyzed geometrically on computer monitor using $Adobe^{(R)}$ $Photoshop^{(R)}$ 7.0. The statistical significance of the differences among the 4 decade groups was estimated by a $x^2$ test. Result : The Korean beautiful woman skewed the geometric characteristics such as the 'coincidence' (83.0%) between facial midline and dental midline, the 'normal' (96.9%) alignment and arrangement of upper anterior teeth. the 'average' (79.1%) position and 'upward' (53.4%) curvature of upper lip, the 'parallel' (85.7%) relationship between the lower lip and upper anterior incisal curvature, the 'touching' (49.9%) and 'not-touching' (44.8%) relationship between upper anterior incisor and towel lip, the 'first premolar' (54.1%) and 'second premolar' (38.9%) displayed in a smile, and the 'symmetry' (89.4%) of smile. There was statistical significance among the 4 decades in the respect of the upper lip curvature, the relationship between upper anterior incisor and lower lip, and the most posterior teeth displayed in a smile (p<0.05). Conclusion : The Korean beautiful woman showed similar results to the western esthetic criteria in the some respects and the tendency that the Korean woman had more active smiling recently.

Removal Characteristics of Mixed Heavy Metals from Aqueous Solution by Recycled Aggregate as Construction Waste (건설폐기물인 순환골재를 이용한 수용액상에서의 혼합 중금속 제거 특성)

  • Shin, Woo-Seok;Kim, Young-Kee
    • Journal of the Korean Society for Marine Environment & Energy
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    • v.16 no.2
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    • pp.115-120
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    • 2013
  • This study examined the removal rate of mixed heavy metals from aqueous solution using recycled aggregate. The recycled aggregate is favorable for the absorbent because it contains about 95% (CaO, $SiO_2$, $Al_2O_3$ and $Fe_2O_3$), which are major ingredient of adsorbent for heavy metal. The kinetic data presented that the slow course of adsorption follows the Pseudo first and second order models. The equilibrium data were well fitted by the Langmuir model and showed the affinity order: $Cu^{2+}$ > $Pb^{2+}$ > $$Zn^{2+}{\simeq_-}Ni^{2+}$$ > $Cd^{2+}$. The results also showed that adsorption rate slightly increased with increasing pH from 6 to 10. Moreover, this trend is similar to results obtained as function of loading amount of recycled aggregate. Meanwhile, an unit adsorption rate was slightly decreased. From these results, it was concluded that the absorbents can be successfully used the removal of the heavy metals from the aqueous solutions.