• 제목/요약/키워드: pressure DSC

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DSC구성방정식을 이용한 포화사질토의 액상화 거동 예측 (A Study on Prediction of the Liquefaction Behavior of Saturated Sandy Soils Using DSC Constitutive Equation)

  • 박인준;김수일;정철민
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2000년도 가을 학술발표회 논문집
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    • pp.201-208
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    • 2000
  • In this study, the behavior of saturated sandy soils under dynamic loads - pore water pressure and effective stress - was investigated using Disturbed State Concept(DSC) model. The model parameters are evaluated from laboratory test data. During the process of loading and reverse loading, DSC model is utilized to trace strain-hardening and cyclic softening behavior. The procedure of back prediction proposed in this study are verified by comparing with laboratory test results. From the back prediction of pore water pressure and effective mean pressure under cyclic loading, excess pore water pressure increases up to initial effective confining pressure and effective mean pressure decrease close to zero in good greement with laboratory test results. Those results represent the liquefaction of saturated sandy soils under dynamic loads. The number of cycles at initial liquefaction using the model prediction is in good agreement with laboratory test results. Therefore, the results of this study state that the liquefaction of saturated sandy soils can be explained by the effective tress analysis.

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액상화 해석을 위한 수정교란상태개념 모델 개발 (Development of Modified Disturbed State Concept Model for Liquefaction Analysis)

  • 박근보;최재순;박인준;김기풍;김수일
    • 한국지반공학회논문집
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    • 제24권3호
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    • pp.35-51
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    • 2008
  • 본 논문에서는 액상화 해석에 관한 DSC 모델을 실험 및 해석적 관점에서 그 적용성을 평가하였다. 포화 사질토의 동적거동을 보다 정확히 예측하기 위해 DSC 모델을 유효응력 경로와 과잉간극수압 발현에 기초하여 수정하였다. 액상화에 대한 동적거동 및 DSC 모델에 대한 매개변수 산정을 위해 정적배수삼축시험과 반복 비배수삼축시험을 상대밀도와 구속응력에 따라 수행하였다. 유효응력 경로와 과잉간극수압의 항으로 액상화 상태를 분류하고 수정된 DSC 모델을 적용시켜 액상화 해석을 수행하였다. 제안된 방법을 토대로 DSC 모델과 제안된 DSC 모델에 대한 액상화 해석을 상대밀도와 구속응력에 따라 비교하였다. 비교 결과 수정 모델은 액상화 시작점 및 동적 거동을 보다 정밀하게 평가하였고, 입력변수의 수가 감소하고 산정방법이 간편해졌다.

DSC 이론을 기초로 한 액상화 영향인자들에 관한 연구 (A Study on the Influence Factors for Liquefaction Based on the Disturbed State Concept)

  • 박인준
    • 한국지진공학회:학술대회논문집
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    • 한국지진공학회 1998년도 추계 학술발표회 논문집 Proceedings of EESK Conference-Spring 1998
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    • pp.361-368
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    • 1998
  • The purpose of this study is to find out the factors affacting liquefaction potential by using DSC(disturded state concept) method and to verify these results through cyclic shear test (truly triaxial test and cyclic triaxial) on saturated sandy soil. Based on this reserch, the DSC method predictions were found to provide satisfactory correlation with the cyclic shear test. And the relationship between the factors affecting liquefaction characteristics--relative density(Dr0 and initial effective confining pressure and physical properties of the saturated sand --ξD and Dc--is found. If the relative density and the initial effective confining pressure increase, the number of cyclic grows up. This means that Dc is incresed and ξD is decreased. Therefore, the liquefaction potential can be evaluated and the factors affacting liquefaction potential can be investigated by using on DSC method. Finally, it is shown that the DSC method can capture the liquefaction mechanism.

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Oxidation Stability and Antioxidant Capacity of Lubricants Measured by a Pressure DSC

  • Cerny, Jaroslav
    • 한국윤활학회:학술대회논문집
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    • 한국윤활학회 2002년도 proceedings of the second asia international conference on tribology
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    • pp.359-360
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    • 2002
  • A methodology was developed for evaluation of oxidation stability of base stocks and engine oils. Analytical procedures for both classes of lubricants were based on the ASTM standards D 6186 and/or E 2009. The procedures were applied to a set of engine oils of the SAE 5W-30 specification, and to a set of several hydrocracked and solvent neutral base oils, both with and without addition of antioxidant. A potential of a pressure DSC for diagnostic purposed was also demonstrated by monitoring the engine oil ageing during its operation in heavy-duty engine.

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포화사질토의 동적거동규명을 위한 수정 교란상태개념 (Modified Disturbed State Concept for Dynamic Behaviors of Fully Saturated Sands)

  • 최재순;김수일
    • 한국지진공학회:학술대회논문집
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    • 한국지진공학회 2003년도 추계 학술발표회논문집
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    • pp.107-114
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    • 2003
  • There are many problems in the prediction of dynamic behaviors of saturated soils because undrained excess pore water pressure builds up and then the strain softening behavior is occurred simultaneously. A few analytical constitutive models based on the effective stress concept have been proposed but most models hardly predict the excess pore water pressure and strain softening behaviors correctly In this study, the disturbed state concept (DSC) model proposed by Dr, Desai was modified to predict the saturated soil behaviors under the dynamic loads. Also, back-prediction program was developed for verification of modified DSC model. Cyclic triaxial tests were carried out to determine DSC parameters and test result was compared with the result of back-prediction. Through this research, it is proved that the proposed model based on the modified disturbed state concept can predict the realistic soil dynamic characteristics such as stress degradation and strain softening behavior according to dynamic process of excess pore water pressure.

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전기솥과 압력솥을 이용한 기능성 강화쌀과 일반쌀의 취반 특성 연구 (Comparison of Cooking Properties between the Functionally Fortified and Regular Rices using Electric and Pressure Cookers)

  • 김지연;이인선;김혜영
    • 한국식생활문화학회지
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    • 제19권3호
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    • pp.359-368
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    • 2004
  • The Physicochemical, sensory and cooking properties of functionally fortified rice with dietary fiber and chitosan were compared with regular rice when the rices were cooked with pressure and electric cookers. Moisture content of functional rice before cooking was 11.11%, which was lower than 13.72% in regular rice. Accordingly, moisture contents of functional rice samples cooked both with pressure and electric cookers were lower than those of regular rice. L value showing the degree of lightness of cooked rice was significantly higher in rice samples cooked with pressure cookers. The ${\alpha}$ value, the degree of redness and the b value, the degree of yellowness, were the highest in the functional rice cooked with an electric rice cookers. Textural measurement of hardness using a rheometer showed the highest value in functional rice cooked with a pressure cooker. The degree of gelatinization measured using differential scanning calorimetry (DSC) before cooking showed higher onset gelatinization temperature ($T_0$) and peak gelatinization temperature ($T_p$) in functional rice compared with those in regular rice. The gelatinization enthalpy (${\Delta}H$) of functional rice was lower than that of regular rice, showing that functional foe had lower gelatinization energy compared with regular rice. When the samples were stored in a refrigerator for one week, the DSC showed faster retrogradation degrees in samples cooked with electric rice cooker, having significantly higher enthalpies of regular and functional rice cooked with electric cooked compared to those cooked with pressure cookers. The functional rice samples cooked with pressure cooker had higher consumer acceptance test values compared to those cooked with electric cookers.

삭카린 중간체의 열분해 특성에 관한 연구 (A Study on the Thermal Decomposition Characteristics of Intermediate of Saccharin)

  • 김관응;김영수;신창섭
    • 한국안전학회지
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    • 제13권4호
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    • pp.180-185
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    • 1998
  • The evaluation of thermal and pressure hazard of chemicals on the manufacturing, transporting and storaging is important in the chemical industry for safety. In this study, the thermal decomposition characteristics of intermediate of Saccharin were investigated by using Accelerating Rate Calorimeter(ARC) and Differential Scanning Calorimeter(DSC). Experimental results showed that decomposition temperatures in p-TSA were about 280~$318^{\circ}C$ by DSC and $201^{\circ}C$ by ARC. In case of o-TSA were about $336^{\circ}C$~$360.8^{\circ}C$ by DSC and $299^{\circ}C$ by ARC. The decomposition temperature acquired by ARC was about $70^{\circ}C$ lower than that by DSC. The exothermic runaway reaction in case of p-TSA occured in 598 minute and o-TSA in 5 minute. For the safety in the chemical industry, we should consider the ARC data as well as DSC data in the handling and design of process.

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밀가루분진 및 살리실산분진의 폭발하한농도 및 열적특성 비교에 관한 연구 (A Study on the Comparison of Explosive Lower Limit Concentration & Thermal Specific of Wheat Powder Dust & Salicylic Acid Dust)

  • 고재선
    • 한국화재소방학회논문지
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    • 제26권4호
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    • pp.1-9
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    • 2012
  • 본 연구에서는 중소기업형의 밀가루 제조공정 및 각질제거용 기능성 비누를 생산하는 화장품 제조공정에서의 분진들을 채집하여 폭발 및 열적특성을 비교하기 위해 실험을 수행하였다. 폭발실험은 Hartman식 분진폭발장치를 이용하였고, 열적실험은 DSC 및 TGA를 이용하여 활석첨가시 농도의 변화에 따른 폭발압력 및 폭발하한계와 온도에 따른 무게감량과 흡열량을 측정하였다. 폭발실험결과 두 시료 모두 활석분진의 비율이 증가할수록 폭발하한농도가 증가하는 것을 볼 수 있었고, 폭발압력은 감소됨을 확인하였다. 그리고 DSC 실험결과 활석의 첨가량이 증가할수록 열유속은 감소하고 온도 또한 약간의 감소상태인 것으로 분석되었다. 또한 두 시료 모두 승온 속도가 증가 할수록 흡열개시온도가 낮은 온도부분으로 이동하고 있으며, 흡열량도 크게 증가하였다. 아울러 TGA 실험결과 활석의 양이 증가할수록 전체 무게감량이 줄어드는 것으로 나타났다. 향후 분진폭발메커니즘의 지속적 연구와 보완이 효과적인 분진폭발예방 대책수립에 기여할 것으로 기대된다.

포화사질토의 동적거동규명을 위한 교란상태개념의 이용 (Applications of Disturbed State Concept for the dynamic behaviors of fully saturated soils)

  • 최재순;박근보;서경범;김수일
    • 한국지진공학회:학술대회논문집
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    • 한국지진공학회 2003년도 춘계 학술발표회논문집
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    • pp.140-147
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    • 2003
  • There are many problems in the prediction of soil dynamic behaviors because undrained excess pore water pressure builds up and then the strain softening behavior is occurred simultaneously. A few analytical methods based on the dynamic constitutive model have been proposed but the model hardly predict the excess pore water pressure directly. In this study, the verification on the disturbed state concept (DSC) model, proposed by Dr, Desai was performed. Some laboratory tests such as conventional triaxial tests and cyclic triaxial tests were carried out to determine DSC Parameters and then disturbance values are determined by the proposed equation. Through this verification, it is proved that the disturbed state concept can express reliably the soil dynamic characteristics such as excess pore water pressure and strain softening behavior. It is also found that the critical disturbance which is determined at the minimum curvature of disturbance function can be a the specific index.

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DSC, ARC, ISCO를 활용한 다양한 순도를 가진 AP의 장기 열적안정성 연구 (Study on the Long-term Thermal Stability by DSC & ARC and its ISCO behaviors with different AP Quality)

  • 김승희;권국태;이소정
    • 한국추진공학회지
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    • 제22권2호
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    • pp.59-65
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    • 2018
  • AP(Ammonium Perchlorate, $NH_4ClO_4$)를 포함하는 복합화약조성의 등온가열시험시, 일정 순도 이하의 AP를 사용하는 경우 "bulged"현상으로 인해 등온가열시험 결과를 얻을 수 없었다. 본 연구는 품질 혹은 순도에 따른 AP의 열적 안정성 차이에 대해 규명하기 위해 LOT 별 AP에 대해 DSC 결과를 분석하고, 그 분석결과를 등온가열시험 결과 및 ARC결과와 비교분석하였다. 또한 순도가 낮은 AP에 대해서는 재결정을 통해 포함된 불순물을 제거한 후 분석한 결과, 열적 안정성이 높아졌음을 확인하였다. DSC 고압팬을 사용하여 AP 순도를 결정하는 정량적 분석방법을 확립하였다.