• Title/Summary/Keyword: fiber analysis

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Fabrication of Lignin Nanofibers Using Electrospinning (전기방사를 이용한 리그닌 나노섬유의 제조)

  • Lee, Eunsil;Lee, Seungsin
    • Journal of the Korean Society of Clothing and Textiles
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    • v.38 no.3
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    • pp.372-385
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    • 2014
  • Lignin is an abundant natural polymer in the biosphere and second only to cellulose; however, it is under-utilized and considered a waste. In this study, lignin was fabricated into nanofibers via electrospinning. The critical parameters that affected the electrospinnability and morphology of the resulting fibers were examined with the aim to utilize lignin as a resource for a new textile material. Poly(vinyl alcohol) (PVA) was added as a carrier polymer to facilitate the fiber formation of lignin, and the electrospun fibers were deposited on polyester (PET) nonwoven substrate. Eleven lignin/PVA hybrid solutions with a different lignin to PVA mass ratio were prepared and then electrospun to find an optimum concentration. Lignin nano-fibers were electrospun under a variety of conditions such as various feed rates, needle gauges, electric voltage, and tip-to-collector distances in order to find an optimum spinning condition. We found that the optimum concentration for electrospinning was a 5wt% PVA precursor solution upon the addition of lignin with the mass ratio of PVA:lignin=1:5.6. The viscosity of the lignin/PVA hybrid solution was determined as an important parameter that affected the electrospinning process; in addition, the interrelation between the viscosity of hybrid solution and the electrospinnability was examined. The solution viscosity increased with lignin loading, but exhibited a shear thinning behavior beyond a certain concentration that resulted in needle clogging. A steep increase in viscosity was also noted when the electrospun system started to form fibers. Consequently, the viscosity range to produce bead-free lignin nanofibers was revealed. The energy dispersive X-ray analysis confirmed that lignin remained after being transformed into nanofibers. The results indicate the possibility of developing a new fiber material that utilizes biomass with resulting fibers that can be applied to various applications such as filtration to wound dressing.

Analysis and Assessment by Thermal Desorption Method of Mixed Organic Solvents Collected on Activated Carbon(AC) and Activated Carbon Fiber(ACF) (AC 및 ACF에 포집된 혼합 유기용제의 열탈착 방법에 따른 분석 및 평가)

  • 원정일;김기환;신창섭
    • Journal of environmental and Sanitary engineering
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    • v.16 no.1
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    • pp.72-90
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    • 2001
  • This study was conducted to evaluate desorption efficiencies accuracy and precision by $CS_2$ and thermal desorption method for polar and non-polar organic solvents collected on activated carbon(AC), activated carbon fiber(ACF), carbosieve SIII, materials tested were Methyl alcohol, n-Hexane, Benzene, Trichloroethylene, Methyl isobutyl ketone and methyl cellosolve acetate and six different concentration levels of samples were made. The results were as follows ; 1. Accuracy on kind adsorbent and desorption method was low. In case of $CS_2$ desorption solvent, Overall B and Overall CV on AC and ACF were 43% and 6.63%, respectively. In case of thermal desorption method, accuracy of thermal desorption method appeared higher than solvent desorption method by AC 18.0%, 3.54%, ACF 2.6%, 2.57%, Carbosieve SIII 13.7% and 1.97%, respectively. 2. In the concentration level III, accuracy of thermal desorption method on adsorbent was in order as follow ; ACF > Carbosieve SIII > AC in the methyl alcohol and Carbosieve SIII > ACF > AC in the rest of them all subject material and Concentration levels showed good precision at EPA recommend standard (${\leq}{\;}30%$) 3. DEs by type of organic solvent adsorbent and desorption method are as follows ; In the case that desorption solvent is $CS_2$, DE of Methyl alcohol is AC 47.5%, DE of all materials is ACF about 50%. In the case of thermal desorption method, DE of Methyl alcohol is AC 82.0%, ACF 97.4%, Carbosieve SIII 86.3%. DE of the later case is prominently improved more than one of former. In particular, Except that DE of EGMEA is ACF 88.5%, DE of the rest of it is more than 95% which is recommend standard MDHS 72. With the result of this study, in order to measure various organic solvent occurring from the working environment, in the case of thermal desorption method, we can get the accurate exposure assessment, reduce the cost, and use ACF as thermal desorption sorbent which available with easy.

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Strength property improvement of OCC-based paper by chemical and mechanical treatments (3 - handsheet physical properties) (골판지 고지의 물리화학적 처리에 의한 강도향상 (제3보 - 수초지의 물리적특성변화))

  • Lee, Jong-Hoon;Seo, Yung B.;Jeon, Yang;Lee, Hak-Lae;Shin, Jong-Ho
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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    • 2000.04a
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    • pp.70-70
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    • 2000
  • This study is a continuation of the previous experimental analysis and is mostly focused on handsheet strength properties. Four completely different fibers, which were Hw-BKP, Sw-BKP, white ledger, and OCC, were selected to investigate the effect of mechanical pre-treatment by Hobart mixer on handsheet strength properties. After equal time mechanical pre-treatment, the fibers were refined with laboratory valley beater for 10, 20 and 30 minutes, and handsheets were prepared from the fibers for physical strength comparison. Handsheets from SW-BKP and OCC showed 5-30% increase of breaking length, burst index, tear index, and compression index while handsheets from HW-BKP and white ledger no Increase except tear index. In Hobart mixer pre-treatment, HW-BKP and white ledger fibers were easily attached to the wall of the mixer bowl and mechanical action was not effectively applied. The fiber length of Hw-BKP and white ledger were 0.837mm and 1.591 mm, respectively, while SW-BKP and OCC were 2.744 mn and 2.033 mm, respectively, in weight weighted length. The effective mechanical pre-treatment seems to be related to the fiber length. Tear indexes of the pre-treated furnish were much higher than no pre-treatment at the same breaking length level.

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Test and Numerical Analysis for Penetration Residual Velocity of Bullet Considering Failure Strain Uncertainty of Composite Plates (복합판재의 파단 변형률 불확실성을 고려한 탄 관통 잔류속도에 대한 시험 및 수치해석)

  • Cha, Myungseok;Lee, Minhyung
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.40 no.3
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    • pp.281-288
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    • 2016
  • The ballistic performance data of composite materials is distributed due to material inhomogeneity. In this paper, the uncertainty in residual velocity is obtained experimentally, and a method of predicting it is established numerically for the high-speed impact of a bullet into laminated composites. First, the failure strain distribution was obtained by conducting a tensile test using 10 specimens. Next, a ballistic impact test was carried out for the impact of a fragment-simulating projectile (FSP) bullet with 4ply ([0/90]s) and 8ply ([0/90/0/90]s) glass fiber reinforced plastic (GFRP) plates. Eighteen shots were made at the same impact velocity and the residual velocities were obtained. Finally, simulations were conducted to predict the residual velocities by using the failure strain distributions that were obtained from the tensile test. For this simulation, two impact velocities were chosen at 411.7m/s (4ply) and 592.5m/s (8ply). The simulation results show that the predicted residual velocities are in close agreement with test results. Additionally, the modeling of a composite plate with layered solid elements requires less calculation time than modeling with solid elements.

Radial Variations in the Lengths of Wood Fibers and Vessel Elements in the Stem of Chestnut (Castanea crenata) Grown in Korea (국내산 밤나무 수간 내 목섬유 및 도관요소 길이의 방사방향 변이성)

  • Lee, Seon-Hwa;Kwon, Sung-Min;Lee, Sung-Jae;Febrianto, Fauzi;Kim, Nam-Hun
    • Journal of the Korean Wood Science and Technology
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    • v.38 no.6
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    • pp.490-497
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    • 2010
  • Radial variations in the lengths of wood fibers and vessel elements in the stem of chestnut (Castanea crenata) grown in Korea were investigated to get some fundamental information for efficient use of wood. Seven chestnut cultivars (Tanzawa, Ibuki, Arima, Ginyose, Tsukuba, Riheiguri, and Mansung) were examined in this study. The lengths of wood fibers and vessel elements were measured and analyzed by an optical microscope and an imaging analysis system. In all chestnut cultivars, the wood fiber length of latewood was longer than that of earlywood, and increased with the increase of growth ring number. Similarly, vessel element length of latewood was longer than that of earlywood, and showed increasing tendency with the increase of growth ring number. Consequently, it was considered that the lengths of wood fibers and vessel elements could be used for separating juvenile wood from adult wood in the chestnut stem.

Development of Modified Printing Hanji Using Alternative Plant Fibers (II) - Printability of Printing Hanji Made of Alternative Plant Fibers - (대체 식물 자원을 이용한 인쇄용 개량한지의 개발 연구(제 2보) - 대체 식물 자원 섬유를 이용한 개량 한지의 인쇄 특성 연구 -)

  • Lee, Ji-Young;Seo, Jeong-Min;Kim, Chul-Hwan;Eom, Tae-Jin;Park, Hyun-Jin;Kim, Sung-Ho;Kim, Gyeong-Chul
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.43 no.2
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    • pp.16-23
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    • 2011
  • This study was carried out to develop the printing Hanji made of mixed raw materials with mulberry bast fibers and alternative plant fibers such as bamboo, soybean stalks, pepper stalk and sea tangle. All alternative plant fibers were produced by the kraft pulping method with 2 stages of bleaching, and used to prepare the modified traditional paper, Hanji for printing purpose. Printing quality of modified Hanji was analyzed by measuring area and Formcircle of halftones and comparing a letter shape printed on paper. The Hanji made of 60% of mulberry bast fibers and 40% of bamboo bleached kraft pulp showed the best printing quality with the smallest area and the largest Formcircle in all modified Hanji. Through the image analysis of form circles of the letters printed on the Hanji, it could also be confirmed that the best printability of the modified Hanji was made using bamboo fibers.

'A Study on Clothing Evaluative Criteria of Various Clothing items(I)' (의류상품 유형별 평가기준에 관한 연구(I))

  • Kim Mi-Young;Rhee Eun-Young
    • Journal of the Korean Society of Clothing and Textiles
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    • v.12 no.2 s.27
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    • pp.249-257
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    • 1988
  • The purposes of the study were to define the clothing evaluative criteria concept as an internal evaluative criteria and buying evaluative criteria based on the Engel-Kollot-Blackwell's consumer behavior model, and to explore the differences between internal evaluative criteria and buying evaluative criteria imprically. The study also aimed to find out the differences between internal evaluative criteria and buying evaluative criteria according to clothing items(underwears, pajama, jeans, blouse, two-pieces, coat) The questionnaires were administered to college female students living in Seoul. Means and Standard Deviations were calculated, and Discriminant Analysis were used for statistical inferences. The results were as follows: In underwears, internal evaluative criteria were comfort and fiber, while toying evaluative criteria was color. In pajama, internal evaluative criteria was comfort and fiber, while buying evaluative criteria was good buy. In jean, internal evaluative criteria was fit and suitability to individual, while buying evaluative criteria was suitability to individual and price. In blouse, internal evaluative criteria was beauty and harmony with other clothing. In two-pieces, internal evaluative criteria was color and beauty, while buying evaluative criteria was suitability to individual. In coat, internal evaluative criteria was textile and color. In conclusion, as shown in the results above, the evident differences between internal evaluative criteria and buying evaluative criteria and buying evaluative criteria were testified, therefore evaluative criteria should he defined as internal evaluative criteria and buying evaluative criteria, and study of evaluative criteria should be explored according to clothing items.

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Analysis of Feed Value and Usability of Soybean Varieties as Livestock Forage

  • Park, Myoung Ryoul;Seo, Min-Jung;Yun, Hong-Tae;Park, Chang-Hwan
    • Journal of The Korean Society of Grassland and Forage Science
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    • v.37 no.2
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    • pp.116-124
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    • 2017
  • This experiment was conducted to evaluate feed value and usability of soybean varieties as livestock forage. In this study, three soybean cultivars, OT93-26, Geomjeongsaeol, and Pungwon, were harvested at R5 (beginning seed development)- and R6 (full seed)-reproductive stages for analyzing feed value of soybean. Days to R5 stage harvest of OT93-26 among the three soybean cultivars was 55 days and the shortest while Pungwon took 103 days to reach at R6 stage. The R6-harvested soybeans had higher dry matter (DM) yields and crude protein (CP) content than the R5-harvested. However, both DM and CP were the highest in the R6-harvested Geomjeongsaeol. Contents of neutral detergent fiber (NDF) and acid detergent fiber (ADF) of Pungwon harvested at R5 were the highest whereas the R6-harvested Geomjeongsaeol had the lowest. Digestible dry matter (DDM), dry matter intake (DMI), and relative feed value (RFV) of the R6-harvested Geomjeongsaeol and Pungwon were higher than those of the R5-harvested, but in case of OT93-26, those at R6 stage were low rather than those at R5 stage. However, soybean could be used as alternative forage with high feed value for livestock. Taken together, Geomjeongsaeol could be used for developing new forage soybean varieties with high feed value, and R6 would be the optimum harvesting stage for yield and quality of forage soybean.

Analysis and fabrication of a wearable antenna using conductive fibers (전도성 실 재질을 이용한 웨어러블 안테나의 제작 및 분석)

  • Nguyen, Tien Manh;Chung, Jae-Young
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.16 no.4
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    • pp.2770-2776
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    • 2015
  • The development of efficient wearable antennas is required to implement short range body-centric wireless communication links for various internet of thing applications. We present simulation and measurement results of conductive-fiber-based wearable antennas which can comfortably fabricated directly on usual clothing materials. The proposed antenna is a form of a rectangular patch antenna designed by weaving conductive fibers on a felt substrate. A full-wave electromagnetic simulation tool is used to investigate the antenna performance such as antenna impedance, resonant frequency, and radiation efficiency. Parametric studies show that the radiation efficiency increases from 67.5% to 70.4% by widening the gap between conductive fibers from 0.25mm to 3mm. This implies a wearable antenna with good radiation efficiency can be designed despite of less portion of conductive fibers on the antenna. The simulation results are also verified by measured results with fabricated antennas.

Dyeability and Functionality of Pine Needles Extract (part I) -Characteristics of Pine Needles Extract and Dyeing Properties of Cellulose Fiber- (솔잎 추출물의 염색성과 기능성 (제1보) -솔잎 추출물의 특성과 셀룰로오스섬유에 대한 염색성-)

  • Woo, Hyo-Jung;Lee, Jung-Soon
    • Journal of the Korean Society of Clothing and Textiles
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    • v.35 no.2
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    • pp.218-229
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    • 2011
  • Dyeing properties of cotton and ramie fabrics with pine needles colorants were studied by investigating the analysis of pine needles colorants, the effect of dyeing conditions (such as dye concentration, dyeing temperatures and times on dye uptakes), effect of mordants, and color change. The various colorfastness of dyed fabrics were evaluated for practical use; in addition, the antimicrobial ability, ultraviolet-cut ability, and deodorant ability were estimated. In the UV-Visible spectrum, the wavelength of the maximum absorption for pine needles extract was 285nm, and pine needles colorants produced a yellow color. From FT-IR and GC-MS results, it was assumed that chromophoric substance from pine needles extracts were mixed with flavonol tannin and flavanol tannin. An increased dyeing concentration resulted in a larger dye uptake and a Freundlich absorption isotherm was obtained. A larger dye uptake occurred as the dyeing time and temperature increased. Post-mordanting was more effective than pre-mordanting and the dye uptake of fabrics improved by mordanting. The colorfastness of dyed fabrics showed a low rating; however, colorfastness to washing and dry cleaning of cotton fabrics mordanted with N.Cu, and friction fastness of ramie fabric mordanted with Cu improved. The dyed fabrics showed very good antimicrobial abilities of 99.9%. In addition, the ultraviolet-cut ability and deodorant ability improved in fabrics dyed with pine needles extracts.