• Title/Summary/Keyword: coating solutions

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Syntheses of Cu-In-Ga-Se/S nano particles and inks for solar cell applications

  • Jung, Duk-Young
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.08a
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    • pp.295-295
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    • 2010
  • Nanoparticles of the compound semiconductor, Cu(In, Ga)Se2 (CIGS), were synthesized in solution under ambient pressure below $100^{\circ}C$ and characterized by powder X-ray diffraction (XRD), scanning electron microscopy (SEM), optical absorption spectroscopy and energy-dispersive X-ray (EDX) analyses. These materials have chalcopyrite crystal structures and the particle sizes less than 100 nm. Synthetic conditions were studied for the crystallized CIGS nanoparticles formation to prevent from side products of Cu2Se, Cu2-xSe, and CuSe etc. The single phase CIGS nanoparticles were applied to coating of thin films photovoltaic cells. The electro deposition of CIGS thin films is also a good non-vacuum technology and under investigation. In aqueous solutions, the different chemical compositions of CIGS thin films were obtained, depending on pH, concentration of starting materials and deposition potentials. The surface morphology of the prepared CIGS thin films depends on the complexing ligands to the solutions during the electrochemical deposition.

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A Study on the Electrical Characteristics of Optical Memory PLZT Thin Films (Sol-Gel법으로 제작된 광메모리영역 PLZT박막의 전기적 특성)

  • 최형욱;장낙원;백동수;박정흠;박창엽
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.11 no.1
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    • pp.57-61
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    • 1998
  • In this study, PLZT stock solutions were prepared by Sol-Gel processing after the compositions were selected in the memory region of PLZT bulk phase diagram. PLZT solutions were deposited on the ITO glass substrate by spin-coating method. The thin films were annealed by rapid thermal processing. The electric characteristics, hysteresis loop, C-V characteristics of thin films in the memory region were measured in order to investigate the electrical characteristics of PLZT thin films. In selected compositions the decrease in Zr/Ti ratio led to an increase in dielectric constant and the decrease in remanent polarization and coercieve field which brought about slim hysteresis loop.

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Electrical Properties of Coatings of Polyaniline (Polyaniline을 이용한 코팅막의 전기적 특성)

  • 김언령;김종은;서광석
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.11a
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    • pp.310-313
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    • 2000
  • Polyaniline Emeraldine Base (PANI EB) polymerized by chemical oxidative polymerization was doped with Camphorsulfonic Acid(CSA). Polyaniline-Camphorsulfonic Acid Emeraldine Salt(PANI-CSA ES) solutions were solved in organic solvents and sonificated at the room temperature for different solvents in PANI-CSA ES solution and sonification time. PANI-CSA ES solutions was coated on PET films using bar coater. 1-Step oxidatively-polymerized Polyaniline-Camphorsulfonic Acid Emeraldine Salt(PANI-CSA ES) was solved in m-cresol:chloroform 1:1 co-solvents and their solution was bar-coated on PET film. The surface resistivities of these coated films were measured, The surface resistivity of PANI-CSA ES solution in m-cresol:chloroform 1:1 co-solvent system was 5${\times}$10$^2$$\Omega$/$\square$.

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Flow Characteristics of Photo Resist in a Slit-Coater Nozzle (Slit-Coater 노즐에서 Photo Resist의 유동 특성)

  • 김장우
    • Journal of the Semiconductor & Display Technology
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    • v.3 no.3
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    • pp.37-40
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    • 2004
  • This study presents numerical solutions of three-dimensional laminar flow-field formed by photo resist flow in a slit-coater model. We discuss on the governing equations, laminar viscosities and the computational model applied in our numerical calculation and some results. We prove that the structure of tapered-cavity aid to make uniform pressure-field and boundary effect is an important problem to improve coating uniformity. In view of uniformity improvement, it is necessary to study for the structure of cavity and flow path.

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A Study on High Temperature Particles-Erosion of Hard Coatings (경질 코팅의 고온 입자침식 현상 연구)

  • 이의열;김종하
    • Journal of the Korean institute of surface engineering
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    • v.36 no.4
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    • pp.291-295
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    • 2003
  • Many steam turbine components encounter solid particle erosion damage. It has been reported that particle erosion damage is caused by oxide scale exfoliation from boiler tubes. One of the most effective solutions to combat the erosion damage is the application of erosion resistant coatings on the turbine components. In this study, particle erosion resistance for various hard coatings such as nitride, Cr carbide and boride coatings was evaluated under the simulated erosion conditions of steam turbines. Based on the particle erosion tests, the boride coating was found to be more superior to others.

Gold Recovery Using Inherently Conducting Polymer Coated Textiles

  • Tsekouras, George;Ralph, Stephen F.;Price, William E.;Wallace, Gordon G.
    • Fibers and Polymers
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    • v.5 no.1
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    • pp.1-5
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    • 2004
  • The ability of inherently conducting polymer (ICP) coated textiles to recover gold metal from aqueous solutions containing $[AuCl_4]^-$ was investigated. Nylon-lycra, nylon, acrylic, polyester and cotton were coated with a layer of polypyrrole (PPy) doped with 1,5-naphthalenedisulfonic acid (NDSA), 2-anthraquinonesulfonic acid (AQSA) or p-toluenesulfonic acid (pTS). Textiles coated with polyaniline (PAn) doped with chloride were also used. The highest gold capacity was displayed by PPy/NDSA/nylon-lycra, which exhibited a capacity of 115 mgAu/g coated textile, or 9700 mgAu/g polymer. Varying the underlying textile substrate or the ICP coating had a major effect on the gold capacity of the composites. Several ICP coated textiles recovered more than 90 % of the gold initially present in solutions containing 10 ppm $[AuCl_4]^-$ and 0.1 M HCl in less than 1 min. Both PPy/NDSA/nylon-lycra and PAn/Cl/nylon-lycra recovered approximately 60 % of the gold and none of the iron present in a solution containing 1 ppm $[AuCl_4]^-$, 1000 ppm $Fe^{3+}$ and 0.1 M HCl. The spontaneous and sustained recovery of gold metal from aqueous solutions containing $[AuCl_4]^-$ using ICP coated textiles has good prospects as a potential future technology.

Development of Evaluation Method for Drug Release Propreties in Drug Eluting Stent (약물방출스텐트의 약물 방출 특성 평가 방법 개발)

  • Song, J.M.;Baek, H.;Lee, S.Y.;Jang, D.H.;Seo, M.Y.;Park, G.J.;Maeng, Eun-Ho
    • Journal of Biomedical Engineering Research
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    • v.34 no.2
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    • pp.69-72
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    • 2013
  • The goal of this study is to develop test method for evaluating the drug eluting properties of drug eluting stents (DES). PBS and the detergent solutions, presented by each DES manufacturer, were used for drug release of DES coated with paclitaxel, zotarolimus and everolimus. The drugs which are coating DES were not released by PBS but released by the detergent solutions, finally paclitaxel 83.38%, zotarolimus 103.85% and everolimus 115.78%. It seems that the use of the detergents is necessary in order to release the drugs because those drugs are extremely hydrophobic. In conclusion, using of detergent solutions presented by each manufacturer were suitable for evaluating the drug eluting property of drug eluting stent.

Change of Dispersibility and Refractive Index of Zirconia Suspension Depending on Alkali Treatment Time (염기처리시간에 따른 지르코니아 현탁액의 분산성과 굴절율 변화)

  • Jo, Choong Hee;Ham, Dong Seok;Lee, Jae Heung;Ryu, Juwhan;Lee, Kee-Yoon;Cho, Seong Keun
    • Korean Journal of Materials Research
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    • v.27 no.1
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    • pp.1-7
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    • 2017
  • Zirconia nanoparticles were widely used as filler in order to get high refractive index layer. However, dispersion of nanoparticles is difficult due to their agglomeration in solvent. In this study, the dispersibility of the zirconia suspension is promoted by controlling the steric hindrance and electrostatic interactions through the adsorption of PEI according to alkali treatment time. Also, to induce improved dispersibility on suspension, we changed the dispersion conditions variously and fabricated an ink formulation method for the coating layer. Zirconia suspension was characterized by dynamic light scattering (DLS), Zeta potential measurement, Transmission Electron Microscope (TEM) and FT-IR. We were able to confirm that good dispersion of zirconia suspension by alkali treatment and PEI led to high refractive index.

Comparative study on fretting wear of aerospace, biomedical, and nuclear components (항공, 바이오, 원자력 부품의 프레팅 마모 현상 비교 연구)

  • Jun, Tea-Sung;Kim, Kyungmok
    • Journal of Aerospace System Engineering
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    • v.11 no.2
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    • pp.16-22
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    • 2017
  • This paper investigates fretting wear damage in aerospace, biomedical, and nuclear components. Experimental parameters are identified that affect fretting wear damage. The parameters observed in industries are directly compared. The magnitudes of frequency, relative displacement, and normal force are found to differ depending on the contacting components where fretting wear occurs. In addition, recent solutions to minimize fretting wear damage are reviewed. The solutions include depositing of a low-friction coating, surface treatment, selection of substrate material, and optimal design of contact geometries. This comparative study suggests useful methods and solutions for analyzing fretting wear damage and for designing tribo-components.

Effect of Solvent on the Dispersion Stability of CaCO3 Pigment (CaCO3 안료의 분산 안정성에 대한 용제의 영향)

  • Lee, Gun Dae;Ryu, Young Cheal;Suh, Cha Soo;Hong, Seong Soo;Ahn, Byung Hyun;Moon, Myung Jun
    • Applied Chemistry for Engineering
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    • v.8 no.2
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    • pp.252-261
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    • 1997
  • The effect of solvent on the dispersion stability of $CaCO_3$ pigment in various solvents and resin solutions has been studied using Dynometer. Dispersion stability can be estimated in a relatively short time by means of Dynometer and the solubility parameter, ${\delta}$, of $CaCO_3$ determined from dispersion stability was 11.62(${\delta}_d=8.04$, ${\delta}_p=5.05$, ${\delta}_h=6.70$). The solvent showing weaker interaction with pigment increased the adsorption of resin on to the pigment, resulting in higher dispersion stability in resin solution. It was found that the rheological properties and dispersion stability of pigmented resin solution were depending strongly on the solvent added in small amount in the formulation.

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