• Title/Summary/Keyword: coating properties

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Properties Evaluation of $SnO_2$ : Sb transparent conductive films by $SiO_2$ barrier ($SiO_2$ barrier에 따른 $SnO_2$ : Sb 투명전도막의 특성고찰)

  • 김범석;김창열;임태영;오근호
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2003.03a
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    • pp.190-190
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    • 2003
  • 여러원소 (Sb, F 등)를 도핑한 SnO$_2$ 투명전도막은 여러 가지 훌륭한 특성으로 Solar cell, heat mirrors, gas sensors, liquid crystal displays, thick film resistor 등과 같이 넓은 범위에서 응용되고 있다. 본 연구에서는 Sb 도핑된 Tin Oxide films이 Sol-gel dip coating법에 의해 준비되었다. SnO$_2$:Sb 용액은 SnC1$_2$ 와 SbC1$_3$ Power를 알코올에 용해하여 Ethylene glycol 와 Citric acid를 첨가하여 합성하였다. 막의 상형성은 XRD와 SEM(Scanning electron microscope)에 의해서 분석되었으며, 특성분석은 투과율(UV/VIS Spectrophotometer)과 표면전기저항(four point probe)으로 분석되었다. SiO$_2$ barrier이 SnO$_2$:Sb 막의 특성에 미치는 영향을 확인하기 위하여 XPS(X-ray photoelectron spectroscopy) 분석이 적용되었다.

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Analysis of Characteristics of DLC Coating Thin Film in Tungsten Carbide for Production of Medical Thermal-Infrared Lenses

  • Park, Yong-Pil;Kim, Tae-Gon;Cheon, Min-Woo
    • Transactions on Electrical and Electronic Materials
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    • v.15 no.6
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    • pp.344-347
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    • 2014
  • This study was carried out on DLC thin film deposition technology used in infrared optical system production as a method of reducing the shape changes of the molding core and the consequent loss of life. Experiments on the deposition on silicon wafer and tungsten carbide used as a substrate for molding core were conducted at each processing condition using a filtered arc system, and it was found that the surface and mechanical properties were of the greatest quality when the substrate bias voltage of -150 V was used. In addition, it was confirmed that the PV and Ra characteristics were improved by the deposition of the DLC thin film.

Study on the Splat Formation of Ni-based Thermal Sprayed Coatings (니켈기 용사코팅의 스플랫 형성에 관한 연구)

  • Kim, K.T.;Lee, S.S.;Lee, D.H.;Kim, Y.S.
    • Journal of Power System Engineering
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    • v.16 no.2
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    • pp.49-53
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    • 2012
  • Thermal spray coatings developed by deposition of splats, it formed by impacting molten droplets on substrates during thermal spray process. In this study, the Ni-based coatings were fabricated by thermal spray process with two different process parameters, oxygen gas flow and acetylene gas flow, with three different levels of each parameters. The morphology of splats and microstructure were observed by optical microscope. Hardness test were performed on the Ni-based coatings. It was confirmed that process parameters of thermal spray process have effect in morphology of splats. These effects also have important implications on the deposit microstructure and properties of Ni-based coatings.

Tribological Behavior of the Plasma Sprayed Fe$_2$O$_3$Added Zirconia Based Coatings ($Fe_2{O_3}$가 첨가된 지르코니아계 용사코팅층의 마모마찰 특성)

  • 신종한;임대순;안효석
    • Tribology and Lubricants
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    • v.16 no.2
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    • pp.84-90
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    • 2000
  • High Temperature wear behavior of plasma sprayed zirconia coatings containing up to 10 mol% of Fe$_2$O$_3$ were investigated. The wear test results showed that the addition of Fe$_2$O$_3$ particles to zirconia improved the wear resistance and lowered the coefficient of friction. Optimum concentration of Fe$_2$O$_3$ was about 5 mol%. Similar degradation behavior was observed at about 40$0^{\circ}C$ for both zirconia and Fe$_2$O$_3$ added zirconia coatings. The results indicated that stabilization of tetragonal phase and changes in mechanical properties such as hardness and toughness were responsible for tribological behavior of plasma sprayed zirconia contain Fe$_2$O$_3$.

Plasma-immersion ion Deposition of Hydrogenated Diamond-like Carbon Films on Dielectric Substrates

  • Kon;Chun, Hui-Gon;Cho, Tong-Yul;Nikolay S. Sochugov;You, Yong-Zoo
    • Journal of Korean Vacuum Science & Technology
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    • v.6 no.4
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    • pp.143-148
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    • 2002
  • Method of plasma-immersion ion deposition of hydrogenated DLC films on relatively thick flat dielectric substrates from plasma of not-self-sustained low-pressure gas arc discharge is suggested. Coating properties have been investigated experimentally, average energy Per a deposited carbon atom depending on discharge current has been calculated. Optimum deposition parameters lot obtaining sufficiently hard and transparent high-adhesive a-C:H films on a 4-mm thick glass substrates have been determined. Possibility to use these coatings for photo-tools protection from abrasion wear at low operating loads is shown in general.

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Preparation of Cu-Al$_2$O$_3$ Composite Powder in the Aqueous Solution by Ha Gas Reduction (수소환원법에 의한 수용액 중 Cu-Al$_2$O$_3$ 복합분말제조)

  • 이종현
    • Journal of Powder Materials
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    • v.4 no.2
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    • pp.106-112
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    • 1997
  • $Cu-Al_20_3 $ composite powders were prepared by hydrogen reduction of $Cu^{2+}$ from ammoniacal copper sulfate solution on alumina core using autoclave. The copper reduction rate and the properties of copper layer were investigated using Scanning Electron Microscope(SEM), X-ray diffractometer, size and chemical analyzers. The reduction rate of $Cu^{2+}$ showed the maximum value when the molar ratio of [$NH_3$]/[$Cu^{2+}$] was 2. In order to prevent the agglomeration of Cu powder and ethane reduction rate, $Fe^{2+}$ and anthraquinone which act as catalysis were added in the solution. Catalysis was effectively chanced with the addition of two elemerts at a time. Optimum conditions obtained in this study were hydrogen reduction temperature of 205$^{\cire}C$, stirring speed of 500 rpm and hydrogen partial pressure of 300 psi. Obtained $Cu-Al_20_3 $ composite Powders were found to have the uniform and continuous copper coating layer of nodule shape with 3~5 $\mu$m thickness.

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Printability of an Aqueous Gravure Ink for Polyolefin (Polyolefin용 수성 Gravure Ink의 인쇄작성)

  • 김종원
    • Journal of the Korean Graphic Arts Communication Society
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    • v.12 no.1
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    • pp.1.1-11
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    • 1994
  • The photosensitive properties and carrier transport in the organic photoconductor with the carrier transport layers(CTL) of polymer matrix doped with two carrier transport materials above carrier generation layer(CGL) containing oxotitanium phthalocyanine (TiOPc) were investigated. The CGL of TiOPc dispersed in poly(vinylbutyral) was formed as thickness of 0.1${\mu}{\textrm}{m}$and the carrier transport layer was prepared by coating polycarbonate and polyester doped with oxadiazoly(OXD), polyvinylcarbazole (PVK), trinitro fluorenone(TNF) as thickness of 10~15${\mu}{\textrm}{m}$, respectively. We have measured half decay exposure,sensitivity and xerographic gain from the photo-induced discharge curve(PIDC). In this work, it was found that the characteristics of carrier transport were mainly caused by the ionization potential difference of constitutive materials in molecularly doped polymer.

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Humidity Sensitive Properties of $V_2O_5$-added $TiO_2$ Ceramics ($V_2O_5$ 첨가에 따른 $TiO_2$ 세라믹스의 감습특성)

  • Hyun, You-Do
    • Proceedings of the KIEE Conference
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    • 2008.05a
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    • pp.161-163
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    • 2008
  • $TiO_2-V_2O_5$ sol was fabricated using sol-gel method and $TiO_2-V_2O_5$, thin films were fabricated using dip-coating method. $V_2O_5$ sol was added 0.01mole, 0.03mole, 0.05mole into $TiO_2$ sol. Capacitance of thin films decreased with increasing $V_2O_5$ additive and it increased largest at 0.01mole. Because adsorption time and desorption time of thin films was about 2 minutes 40 seconds and about 3 minutes 40 seconds respectively, adsorption time was faster about 1 minutes than desorption time.

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Weatherability Comparison with Changing Mixing Ratios of Mill-Base and Let-Down Silicone/Acrylic Resins (안료분산 및 희석용 실리콘/아크릴수지의 배합비에 따른 고내후성 물성비교)

  • Park, Hong-Soo;Kim, Song-Hyoung;Hahm, Hyun-Sik
    • Journal of the Korean Applied Science and Technology
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    • v.24 no.3
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    • pp.253-263
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    • 2007
  • Three different weather-resistant coatings were fabricated with the various weight ratios of a mill-base silicone/acrylic resin to let-down silicone /acrylic resin at 2:8, 3:7, and 4:6 respectively. The prepared coatings were tested to investigate the effect of composition of weather-resistant coatings on the physical properties. The thermal stability, salt spray exposure, and weather-resistance were improved with the increased silicone content. It was concluded that the optimum retio of mill-base silicone/acrylic resin to let-down silicone/acrylic resin would be 2:8 and the coating with 30 wt% of silicone content would have high weather-resistance.

$Sr_2(Nb,Ta)_2O_7$ Thin Films for Ferroelectric Gate Field Effect Transistor. (Ferroelectric Gate Field Effect Transistor용 $Sr_2(Nb,Ta)_2O_7$박막)

  • 김창영;우동찬;이희영;이원재
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1998.11a
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    • pp.335-338
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    • 1998
  • Ferroelectric Sr$_2$(Nb,Ta)$_2$O$_{7}$ (SNTO) thin films were prepared by chemical solution deposition processes. SNTO thin films were spin-coated on Pt/Ti/SiO$_2$/(100)Si substrates. After multiple coating, dried thin films were heat-treated for decomposition of residual organics and crystallization. B site-rich impurity phase, i.e. [Sr(Nb,Ta)$_2$O$_{6}$], was found after annealing, where its appearance was dependent on process temperature indicating the possible reaction with substrate. Dielectric and other relevant electrical properties were measured and the results showed a little possibility in ferroelectric gate random access memory devices.s.s.

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