• Title/Summary/Keyword: Wet/Dry Oxide

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Development of Pre-treatment for Tin Recovery from Waste Resources (주석 함유 폐자원의 공정부산물 전처리 기술)

  • Jin, Y.H.;Jang, D.H.;Jung, H.C.;Lee, K.W.
    • Journal of Powder Materials
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    • v.21 no.2
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    • pp.142-146
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    • 2014
  • Fundamental experiences have been studied for development of pre-treatment process of Sn by-products such as solders. Dry and wet separation/recovery processes were considered by the differences of physical properties. The by-products, which are analyzed by solder metal and oxides. The metal and oxide were simply separated by dry ball-milling process for 12 hours, after that recovery metal powder might be reusable as lead or lead-free solders. In terms of wet separation process, samples were dissolved in $HNO_3+H_2O_2$ and the precipitation were analyzed by $SnO_2$. Overall efficiency of recovery might be increasing via developing simple pre-treatment process.

Durability of Photocatalytic Cement after Nitric Oxide-Wet-Dry Cycling

  • Lee, Bo Yeon;Kurtis, Kimberly E.
    • Journal of the Korea Institute of Building Construction
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    • v.14 no.4
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    • pp.359-368
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    • 2014
  • Photocatalytic cement has been receiving attention due to its high oxidation power that reduces nitrogen oxide, thus contributing to a clean atmospheric environment. However, there has not yet been a thorough investigation on the effect of photocatalytic reactions on the durability of cementitious material, the parent material. In this study, photocatalytic cement samples were exposed to nitric oxide gas and UV along with cycles of wetting and drying to simulate environmental conditions. The surface of samples was characterized mechanically, chemically, and visually during the cycling. The results indicate that that the photocatalytic efficiency decreased with continued NO oxidation. The pits found from SEM indicated that chemical deterioration, such as acid attack or leaching, did occur. However, this was not confirmed by X-ray diffraction. The hardness was not affected, probably due to the formation of CSH as evidenced by the XRD pattern. In conclusion, it was found that photocatalysis could alter cementitious materials both chemically and mechanically, which could further affect long-term durability.

A selective formation of high-quality fully recessed oxide (양질의 FRO(fully recessed oxide)의 선택적 형성)

  • 류창우;심준환;이준희;이종현
    • Journal of the Korean Institute of Telematics and Electronics A
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    • v.33A no.7
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    • pp.149-155
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    • 1996
  • A new technique wasdeveloped which obtains selectively the htick fully recessed oxidized porous silicon layer (OPSL) with good dielectric property. The porous silicon layer was ocnverted to thick fully recessed oxide (FRO) with 3-step (1${\mu}$m, 1.5${\mu}$m, 1.8${\mu}$m) by multi-step thermal oxidation (after 400$^{\circ}$C, 1 hour by dry oxidation, 700$^{\circ}$C, 1 hour and then 1100$^{\circ}$C, 1 hour by wet oxidation). The breakdwon field of the FRO was about 2.5MV/cm and the leakage current was several pA ~ 100 pA in the range of 0 of 90 pF. The progress of oxidation of a porous silicon layer was studied by examining the infrared abosrption spectra. The refractive index (1.51) of the fRO, which was measured by ellipsometer, was comparable to that of the thermally grown silicon dioxide (1.46). The etching rate (1600${\AA}$/min) of the FRO was also almost equal to that of the thermal oxide.

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Investigation on the Stability Enhancement of Oxide Thin Film Transistor (산화물반도체 트랜지스터 안정성 향상 연구)

  • Lee, Sang Yeol
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.26 no.5
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    • pp.351-354
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    • 2013
  • Thin-film transistors(TFTs) with silicon-zinc-tin-oxide(SiZnSnO, SZTO) channel layer are fabricated by rf sputtering method. Electrical properties were changed by different annealing treatment of dry annealing and wet annealing. This procedure improves electrical property especially, stability of oxide TFT. Improved electrical properties are ascribed to desorption of the negatively charged oxygen species from the surfaces by annealing treatment. The threshold voltage ($V_{th}$) shifted toward positive as increasing Si contents in SZTO system. Because the Si has a lower standard electrode potential (SEP) than that that of Sn, Zn, resulting in the degeneration of the oxygen vacancy ($V_O$). As a result, the Si acts as carrier suppressor and oxygen binder in the SZTO as well as a $V_{th}$ controller, resulting in the enhancement of stability of TFTs.

A Study on the Removal of Native Oxide on a Silicon Surface Using UV-Excited $F_2/H_2$ (UV-excited $F_2/H_2$를 이용한 실리콘 자연산화막 제거에 관한 연구)

  • Choi, S.H.;Choi, J.S.;Kim, S.I.;Koo, K.W.;Chun, H.G.
    • Proceedings of the KIEE Conference
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    • 1997.07d
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    • pp.1528-1530
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    • 1997
  • As device size shrinks, contamination will increasingly affect the reliability and yield of device. Therefore, contaminants must be removed from the surfaces of Si wafers prior to each process. But it becomes out increasingly difficult to clean silicon surfaces with finer patterns by the conventional wet treatment because of the viscosity and surface tension of solutions. Hence, a damage less dry cleaning process is needed for the silicon surfaces. For the removal of Si native oxide by UV-enhanced dry cleaning. $F_2$ gas and $F_2/H_2$ mixed gas were applied. As a result of analysis, UV-enhnaced $F_2/H_2$ treatment is more suitable than UV-enhanced $F_2$ treatment for removal of native oxide on the surfaces of Si wafers.

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A Study on the Preparation and Properties of Cellulose-EVOH Fibers (Cellulose-EVOH 섬유의 제조와 물성에 관한 연구)

  • 문병화;임상규;손태원;김삼수
    • Textile Coloration and Finishing
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    • v.10 no.5
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    • pp.19-23
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    • 1998
  • In this study, Cellulose-Poly(Ethylene-Co-Vinyl Alcohol) (EVOH) fibers from MMNO(N-me-thylmorpholine-N-oxide) /water/cellulose/EVOH were prepared according to changes of EVOH content(wt%), which is main factors to dry-jet wet spinning. The mechanical properties and morphology of produced fibers were investigated. The resultant fibers had tensile strength of 3.7∼4.5g/d, elongation of 3.3∼7.5% and exhibited lower density than the density of pure cellulose fiber.

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Age-related digestibility of nutrients depending on the moisture content in aged dogs

  • Kim, Ki Hyun;Seo, Kangmin;Cho, Hyun-Woo;Jeon, Jung-Hwan;Kim, Chan Ho;Jung, Jiyeon;Chun, Ju Lan
    • Journal of Animal Science and Technology
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    • v.63 no.6
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    • pp.1355-1361
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    • 2021
  • Digestibility of pet food can affect the health of dog, especially of aged animals. To maintain the health of dogs in an overall good status it is necessary to provide nutritionally balanced food. For example, the digestibility of dogs was known to be decreased along aging. In addition, losing teethes is an often event in aged dogs that could induce a problem to eat a large size dry pet food. Nonetheless, few detailed information is available on the most suited feeding for aged dogs. As part of the nutritional study of food for aged dogs, in this study, we tested whether food type impacts on digestibility on adult versus senior dogs. The methodology to measure the digestibility of nutrients was chosen the index method using chromium oxide. Dogs were fed the same commercial dry or wet diets, which were supplemented with 0.5% chromium oxide. The wet food was prepared by adding twice volume of water in the dry food prior to incubated overnight (14-16 hours) at room temperature. After five days, their feces were collected up to a total weight of > 200 g which was the amount to analyze undigested nutrients in feces as 3 repeats. In the apparent total tract digestibility analysis of the experimental breed, no difference in the digestibility of crude protein, crude fat, crude fiber, ash, and energy was observed regarding the moisture content of the food. Noteworthy, the digestibility of nitrogen free extract was significantly increased in senior dogs fed dry dog food compared with adult dogs fed the same diet, whereas no difference was observed between senior and adult dogs fed wet food. The small breed dogs showed similar results to the experimental breed dogs. However, the digestibility of crude fat was additionally affected by age and food type unlike the experimental breed dogs. This finding suggests that the food moisture content affects the digestibility of nutrients in dogs with aging. Hence, it may be helpful to determine the nutrient contents in foods for senior dogs depending on the food type.

Effect of Relative Humidity on the Atmospheric Corrosion of Mild Steel Using the Electrochemical Wet/Dry Method (전기화학적 wet/dry 법을 이용한 탄소강의 대기부식에 미치는 상대습도의 영향에 관한 연구)

  • Yeon Jei-Won;Pyun Su-Il;Lee Woo-Jin;Choi In-Kyu;Chun Kwan-Sik
    • Journal of the Korean Electrochemical Society
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    • v.3 no.1
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    • pp.5-10
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    • 2000
  • In the present work, corrosion rate W and corrosion potential tow were simultaneously measured as a function of relative humidity RH employing the electrochemical wet and dry method as an accelelated atmospheric corrosion method. The W versus (vs.) RH curve is classified into .three regions, namely, the first W plateau region, the second region of the linear relationship between logarithmic W and RH, finally, followed by an abrupt decay region. Based upon the atmospheric corrosion mechanism of mild steel, we introduced another diagram of $\varepsilon_{corr}$ vs. RH which is divided into three regions. In the first region, the corrosion scales are composed of single lepidocrocite-phase $(\gamma-FeOOH)$; in the second region, $\gamma-FeOOH$-phase coexists with magnetite-phase $(Fe_3O_4)$ in the scales and finally the oxide scales change into a single Fe304-phase in the third region. The three distinct regions of both representations share almost each other, which is validated by FT-IR (Fourier transform infra-red) analysis and surface observation. Both representations prove to be convenient and complementary for surveying the spectrum of the atmospheric corrosion of mild steel.

A study on the Dislocation-Free Shallow Trench Isolation (STI) Process (Dislocation-Free Shallow Trench Isolation 공정 연구)

  • Yoo, Hae-Young;Kim, Nam-Hoon;Kim, Sang-Yong;Lee, Woo-Sun;Chang, Eui-Goo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.11a
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    • pp.84-85
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    • 2005
  • Dislocations are often found at Shallow Trench Isolation (STI) process after repeated thermal cycles. The residual stress after STI process often leads defect like dislocation by post STI thermo-mechanical stress. Thermo-mechanical stress induced by STI process is difficult to remove perfectly by plastic deformation at previous thermal cycles. Embedded flash memory process is very weak in terms of post STI thermo-mechanical stress, because it requires more oxidation steps than other devices. Therefore, dislocation-free flash process should be optimized.

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Fabrication of Depth-probe type Silicon Microelectrode array for Neural signal Recording (신경신호기록용 탐침형 반도체 미세전극 어레이의 제작)

  • Yoon, T.H.;Hwang, E.J.;Shin, D.Y.;Kim, S.J.
    • Proceedings of the KOSOMBE Conference
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    • v.1998 no.11
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    • pp.147-148
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    • 1998
  • In this paper, we developed the process for depth-probe type silicon microelectrode arrays. The process consists of four mask steps only. The steps are for defining sites, windows, and for shaping probe using plasma etch from above, and for shaping using wet etch from below, respectively. The probe thickness is controlled by dry etching, not by impurity diffusion. We used gold electrodes with a triple dielectric system consisting of oxide/nitride/oxide. The shank of the probe taper from 200um to tens of urn tip and has 30 um thickness.

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