• Title/Summary/Keyword: Vacuum evaporation

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Physical Properties of Thin Metal Films -II (-Effect of Oxygen on Thin Metal Film Formation and Physical Properties- (금속박막의 물리적 성질 -II- -금속박막형성과 물성에 미치는 산소의 영향-=)

  • 이세경;박수현
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.25 no.7
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    • pp.791-798
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    • 1988
  • Films of Cr, Cu, and Al were deposited by the evaporation technique at the high vacuum level-high evaporation rate and the low vacuum level-low evaporation rate. We measured sheet resistance and light transmittance, and observed microstructure and diffraction pattern by TEM, and investigated oxygen content in thin film by AES. We discussed the relations among microstructure, sheet resistance, and light transmittance with AES data. We found that the films deposited at the high vacuum level-high evaporation rate have small oxygen content in thin film comparing to the films deposited at the low vacuum level-low vacuum level-low evaporation rate, and that the films having crystalline structure and larger grain size were formed in the case of the high vacuum level-high evaporation rate and they showed lower sheet resistance and lower light transmittance.

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Study on Optimization of the Vacuum Evaporation Process for OLED (Organic Electro-luminescent Emitting Display) (유기EL 디스플레이의 진공 성막 공정의 최적화에 관한 연구)

  • Lee, Eung-Ki
    • Journal of the Semiconductor & Display Technology
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    • v.7 no.1
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    • pp.35-40
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    • 2008
  • In OLED vacuum evaporation process, the essential requirements include good uniformity of the film thickness over a glass substrate. And, it is commercially significant to improve the consuming efficiency of material of the evaporant which is deposited on the substrate because of high price of organic materials. In this paper, to achieve the better thickness uniformity and the better organic material consuming rate, a process optimization algorithm was developed by understanding vacuum evaporation process parameters that affect the material consuming efficiency and the uniformity of film thickness. Based on the method developed in this study, the vacuum evaporation process of OLED was successfully controlled. The developed method allowed the manufacture of high quality OLED displays with cheaper fabrication cost.

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An Experimental Study on the Dewatering from the Waste Lubrication Oil by Vacuum Evaporation (진공 증발에 의한 폐윤활유 속의 수분 제거에 관한 실험적 연구)

  • 정상현;박성제;홍원석;김용진;구경회
    • Journal of Energy Engineering
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    • v.12 no.3
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    • pp.216-222
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    • 2003
  • An experimental study on the characteristics of a dewatering due to vacuum evaporation in the waste lubrication oil were performed using a lab scale system. Evaporation characteristics were investigated for various performance factors. Results of evaporation characteristics as a function of vacuum pressure, oil temperature, initial water concentration, and nozzle type were obtained. Increasing the oil temperature and altering the nozzle type were found to increase the evaporation rate without increasing vacuum pressure requirement. The best performance is achieved for the nozzle which made porous material.

Study on the deposition rate and vapor distribution of Al films prepared by vacuum evaporation and arc-induced ion plating (증착방법에 따른 Al 피막의 증착율 및 증기분포에 관한 연구)

  • 정재인;정우철;손영호;이득진;박성렬
    • Journal of the Korean Vacuum Society
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    • v.9 no.3
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    • pp.207-215
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    • 2000
  • Al films on cold-rolled steel sheet have been prepared by vacuum evaporation and arc-induced ion plating, respectively, and the evaporation rate and vapor distribution (thickness distribution over the substrate) have been investigated according to deposition conditions. The arc-induced ion plating (AIIP) method have been employed, which makes use of arc-like discharge current induced by ionization electrode located near the evaporation source. The AIIP takes advantage of high ionization rate compared with conventional ion plating, and can be carried out at low pressure of less than $10^{-4}$ torr. Very high evaporation rate of more than 2.0 mu\textrm{m}$/min could be achieved for Al evaporation using alumina liner by electron beam evaporation. The geometry factor n for the $cos^{n/\phi}$ vapor distribution, which affects the thickness distribution of films at the substrate turned out to be around 1 for vacuum evaporation, while it features around 2 or higher for ion plating. For the ion plated films, it has been found that the ionization condition and substrate bias are the main parameters to affect the thickness distribution of the films.

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Perovskite Solar Cells through Application of Hole Transporting Layers based on Vacuum Thermal Evaporation (진공 열 증착 기반의 정공수송층 적용을 통한 페로브스카이트 태양전지)

  • Kim, Hye Seung;Song, Myoung Hoon
    • Current Photovoltaic Research
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    • v.10 no.1
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    • pp.23-27
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    • 2022
  • In this study, we investigate organic-inorganic halide perovskite solar cells with a vacuum thermal evaporated hole transporting layer (NPB/MoO3-x). By replacing solution process based Spiro-MeOTAD with vacuum thermal evaporation based NPB/MoO3-x, a thin hole transporting layer was implemented. In addition, parasitic absorption that may occur during the doping process was eliminated by excluding solution process doping. In a solar cell with a thin vacuum thermal evaporated hole transporting layer, the short-circuit current density (Jsc) increased to 23.93 mA/cm2, resulting in the highest power converstion efficiency (PCE) at 18.76%. Considering these results, it is essential to control the thickness of hole transporting layer located at the top in solar cell configuration.

Study on Cooling Charcteristics of Forced Evaporation by using Steam Ejector (스팀 에젝터에 의한 강제 증발 방식의 냉각 특성에 관한 연구)

  • Son, H.J.;Lee, Y.H.;Kim, Y.G.;Jeong, H.M
    • Journal of Power System Engineering
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    • v.10 no.2
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    • pp.41-46
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    • 2006
  • This study shows a water cooling system by using a steam ejector and jet condenser to drop the temperature of the water by about $5^{\circ}C\;from\;25^{\circ}C$ or higher. In this research, to replace the present water cooling system, we focused on a water cooling system by latent heat of evaporation, thus this system needs a vacuum pressure to evaporate the water in enclosed tank. The water cooling effects are depended on the vacuum pressure in the enclosed tank, and the cooling water is generated by latent head of evaporation. As the experimental results, the absolute vacuum pressure obtained was about $5{\sim}8$ mmHg using a steam driven ejector with jet condenser.

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A Study on the Evaporation Behavior of Magnesium Alloy (AM50) Scrap Melt under Reduced Pressure (감압 하에서 마그네슘 합금(AM50) 스크랩 용탕의 증발 거동에 관한 연구)

  • Wi, Chang-Hyun;Hong, Seong-Hun;You, Byung-Don
    • Korean Journal of Metals and Materials
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    • v.48 no.3
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    • pp.241-247
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    • 2010
  • In order to develop the vacuum distillation process of magnesium alloy scrap, a fundamental study on the evaporation behavior of magnesium alloy (AM50) scrap melt was carried out. Melt temperature, pressure, reaction time, and initial specific surface area of melt were considered as experimental variables. The evaporation rate of magnesium increased with the increase of melt temperature and initial specific surface area of melt, and with the decrease of the pressure. The activation energy of magnesium evaporation reaction calculated by an Arrhenius plot decreased with the decrease of the pressure and with the increase of the initial specific surface area of melt. An empirical equation was derived for the evaporation rate of magnesium from AM50 alloy melt.

Study on the evaporation of high melting temperature metal by using the manufactured electron hem gun system (전자총 시스템 제작과 이를 이용한 고융점 금속 증발에 관한 연구)

  • 정의창;노시표;김철중
    • Journal of the Korean Vacuum Society
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    • v.12 no.1
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    • pp.1-6
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    • 2003
  • An axial electron beam gun system, which emits the electron beam power of 50 kW, has been manufactured. The electron beam gun consists of two parts. One is the electron beam generation part. including the filament, cathode, and anode. The maximum beam current is 2 A and the acceleration voltage is 25 kV. The other part includes the focusing-, deflection-, and scanning coils. The beam diameter and ham trajectory can be controlled by these coils. The characteristic of each part is measured ior the optimum condition of evaporation process. Moreover, Helmholtz coil is installed inside the vacuum chamber to adjust the incident angel of the beam to the melting surface for the maximum evaporation. We report on the evaporation rates for zirconium(Zr) and gadolinium(Gd) metals which have the high melting temperatures.

A Study on the Rapid Cooling Vacuum System for the Storage and Transportation of the Cold Agriculture and Livestock Products (농축산물의 저장 및 유통을 위한 감압증발 급냉각 시스템에 관한 연구)

  • 김성규;김원녕;김경석;최순열;전현필
    • Journal of Advanced Marine Engineering and Technology
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    • v.21 no.1
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    • pp.26-36
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    • 1997
  • Recently, the new refrigerating system, using non - fluorinated hydrocarbon refrigerants has to be developed for the agricultural fields. One of that kinds of systems is the cooling system using the water vapor and vacuum, in which the water evaporate at the low temperature under vacuum and absorb the large amount of the latent heat. If vapor with large amount of latent heat is removed from the system, the system is cooled accordingly. The characteristics of cooling under the vacuum was observed and measured using experimental apparatus, which is consisted of vacuum chamber, the ejectors, the pumps and the measurement apparatus. As the results of experiments, we know that the evaporation in the vacuum occurs vigorously when the materials to be cooled has more amounts of heat before cooling, and by which effects the materials can be cooled. The cooling vacuum system is more efficient than other methods when the agricultural products is chilled or dried.

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Process TAC Time Reduction Technology for Improving the Efficiency and Throughput of the PDP (PDP 효율 및 생산성 향상을 위한 공정단순화 기술)

  • Kwon, Sang Jik
    • Journal of the Semiconductor & Display Technology
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    • v.12 no.2
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    • pp.45-50
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    • 2013
  • This paper focuses on the fundamental issues for improving the efficiency and throughput of the AC PDP (Plasma Display Panel) manufacturing. The properties of the MgO protective layer affect the PDP efficiency. Especially, the secondary electron emission efficiency was affected on the deposition rate of MgO during the evaporation. In this study, the deposition rate of 5 $\AA$/s has given the maximum efficiency value of 0.05 It is demonstrated that the impurity gases such as $H_2O$, $CO_2$, CO or $N_2$, and $O_2$ can be remained inside the PDP panel before sealing and the amount of the impurity gases decreased rapidly as the base vacuum level increased, especially near $10^{-5}$ torr. The fundamental solution in order to overcome these problems is the vacuum in-line sealing process from the MgO evaporation to the final sealing of the panel without breaking the vacuum. We have demonstrated this fundamental process technology and shown the feasibility. The firing voltage was reduced down to 285 V at the base vacuum value of $10^{-6}$ torr, whreras it was about 328 V at the base vacuum value of $10^{-3}$ torr.