• Title/Summary/Keyword: Standard method

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Accurate Measurement of Arsenic in Laver by Gravimetric Standard Addition Method Combined with High Resolution Inductively Coupled Plasma Mass Spectrometry

  • Lee, Kyoung-Seok;Kim, Hyeon-Ji;Yim, Yong-Hyeon;Kim, Jeongkwon;Hwang, Euijin
    • Mass Spectrometry Letters
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    • v.5 no.2
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    • pp.57-61
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    • 2014
  • A gravimetric standard addition method combined with internal standard calibration has been successfully developed for the accurate analysis of total arsenic in a laver candidate reference material. A model equation for the gravimetric standard addition approach using an internal standard was derived to determine arsenic content in samples. Handlings of samples, As standard and internal standard were carried out gravimetrically to avoid larger uncertainty and variability involved in the volumetric preparation. Germanium was selected as the internal standard because of its close mass to the arsenic to minimize mass-dependent bias in mass spectrometer. The ion signal ratios of $^{75}As^+$ to $^{72}Ge^+$ (or $^{73}Ge^+$) were measured in high resolution mode ($R{\geq}10,000$) to separate potential isobaric interferences by high resolution ICP/MS. For method validation, the developed method was applied to the analysis of arsenic content in the NMIJ 7402-a codfish certified reference material (CRM) and the result was $37.07mg{\cdot}kg^{-1}{\pm}0.45mg{\cdot}kg^{-1}$ which is in good agreement with the certified value, $36.7mg{\cdot}kg^{-1}{\pm}1.8mg{\cdot}kg^{-1}$. Finally, the certified value of the total arsenic in the candidate laver CRM was determined to be $47.15mg{\cdot}kg^{-1}{\pm}1.32mg{\cdot}kg^{-1}$ (k = 2.8 for 95% confidence level) which is an excellent result for arsenic measurement with only 2.8 % of relative expanded uncertainty.

Construction of Korean Korea CALS Standardization (한국적 CALS 표준화 구축방안)

  • 김철환;김규수;신영인
    • The Journal of Society for e-Business Studies
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    • v.1 no.1
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    • pp.117-140
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    • 1996
  • CALS is recognized as a national response to the new chapter of information society. It is essential that the standardization in Korea should be constructed compatible with not only domestic but also international standardization trend. This study aims to propose a proper direction of CALS standardization in Korea, based on the international CALS standardization movement. This paper classifies standard into five types and provides a proper direction and guidance far each standard. As a trend of CALS standard, all ten data files are converted using SGML standard far the interchangeability of data among heterogenous systems. CAD and Graphic data arc also moving toward to the STEP as their standard. In this regard, this paper discusses how to implement SGML and STEP Model. Finally, this paper proposes a method how to construct an EDI system with CALS standard and how to establish a standard authorization institute which will be responsible far the standard authorization. Furthermore, this paper also proposes the CALS Test Network (CTN) as its experimental method.

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The controversial points for the assessment of soil contamination related to the change of pH of extraction solution in using partial extraction in standard method in Korea (국내 토양오염 공정시험방법의 용출법 사용시 용출액의 pH의 변화가 토양 오염 평가에 미치는 문제점)

  • 오창환;유연희;이평구;이영엽
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2000.11a
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    • pp.294-297
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    • 2000
  • Heavy metals are extracted from Chonju stream sediment, roadside soils and sediments along Honam expressway, soils and tailings from mining area using partial ectraction in Standard Method, partial ectraction method with maintaining 0.1N of extraction solution and acid digestion. In samples having buffer capacity against acid, 0.1N of extraction solution can not be maintained and pH of extraction solution increases up to 8.0 when partial extraction in Standard Method is used. The averages and ranges of (heavy metals extracted using partial extraction in standard method, HPE)/(heavy metals extracted using partial extraction method with maintaining 0.1N of extraction solution, HPEM) values are 0.506 and 0.145~1.126 in Cd, 0.534~ and 0.078~0.928 in Zn, 0.461 and 0.041~1.715 in Mn, 0.359 and 0.011~0.874 in Cu, 0.195 and 0.018~1.785 in Cr, 0.710 and 0.003~3.075 in Pb, and 0.088 and 1.73$\times$10$^{-5}$ ~0.303 in Fe. These data indicate that the difference between HPE and HPEM is big in the order of Fe, Cr, Cu, Mn, Cd, Zn and Pb. It is quite possible that the partial extraction method in Standard Method of soil in Korea is not adequate for an assessment of contamination in area where buffer capacity of soil will be decreased or lost after a long term exposure of soils to environmental damage.

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Comparison of the Total Nitrogen Determination Methods by UV spectrophotometric method and Standard method (수질공정시험법과 Standard Method의 총질소 분석방법비교)

  • Park, Sang-Chan;Park, Jong-Ho;Kang, Byung-Wook;Lee, Sung-Hee;Chang, In-Soo;Cho, Jung-Sik
    • Proceedings of the KAIS Fall Conference
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    • 2010.11a
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    • pp.291-293
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    • 2010
  • 알카리성 과황산칼륨을 이용한 자외선 흡광광도법은 수중의 총질소를 간편하면서도 신속하고 정확하게 분석할 수 있는 방법으로 각각의 질소성분을 standard method에 의해 분석한 후 이들을 합산하는 방법보다 회수율이 좋게 나타났다. 자외선 흡광광도법을 이용할 경우 Cr(VI)이온과 Br이온에 의해 방해를 받으므로, Br이온을 다량 함유하는 해수의 총질소 분석방법으로는 적합하지 않은 것으로 관찰되었다. 전처리를 한 후 220 nm에서 흡광도를 측정하기 위해서는 탄산염의 방해를 방지하기 위해 pH를 2~3으로 조절한 후 분석해야만 하고, 알카리성 과황산칼륨을 이용한 자외선 흡광광도법은 총질소를 분석하는 방법으로 우수성이 입증되었으나 각 형태별 질소의 농도를 측정할 수 없는 단점이 있으므로 각 형태별 질소의 농도를 측정하기 위해서는 standard method를 이용해야 된다. 본 연구에서 알카리성 과황산칼륨을 이용한 자외선 흡광광도법은 총질소를 분석하는데 있어서 standard method에 의한 합산법보다 시간과 노력을 절약할 수 있는 것으로 검토되었다.

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DEVELOPMENT OF A NON-STANDARD FINITE DIFFERENCE METHOD FOR SOLVING A FRACTIONAL DECAY MODEL

  • SAID AL KATHIRI;EIHAB BASHIER;NUR NADIAH ABD HAMID;NORSHAFIRA RAMLI
    • Journal of applied mathematics & informatics
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    • v.42 no.3
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    • pp.695-708
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    • 2024
  • In this paper we present a non-standard finite difference method for solving a fractional decay model. The proposed NSFDM is constructed by incorporating a non-standard denominator function, resulting in an explicit numerical scheme as easy as the conventional Euler method, but it provides very accurate solutions and has unconditional stability. Two examples from the literature are presented to demonstrate the performance of the proposed numerical scheme, which is compared to three methods from the literature. It is found that the method's estimated errors are extremely minimal, such as within the machine precision.

Design standard for fairway in next generation

  • Ohtsu, Kohei;Yoshimura, Yasuo;Hirano, Masayoshi;Takahashi, Hironao;Tsugane, Masanori;Ohtsu, Kohei
    • Proceedings of the Korean Institute of Navigation and Port Research Conference
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    • 2006.10a
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    • pp.230-239
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    • 2006
  • The depth, width and alignment of fairway that are main port water facilities should be designed considering the various elements including particulars of design ships, weather and sea conditions around fairway and method of ship-handling. However not only the existing Japanese design standard for fairway and also those of other countries do not take into consideration of such kind of elements and no design standard is made by quantitative analysis. In this circumstance the new design standard (Approach Channels, A Guide for Design) depending on classified various elements and quantitative analysis was proposed in 1997 by PIANC and IAPH. But it was proved that calculated values according to this standard were unfounded and had some problems to output the discontinuous value by small difference of calculation condition because the each value fur each element was simply added. And also it is hard to apply this standard to the design of port water facilities in Japan because this [A Guide for Design] is the design standard for long channels in European port. The proposal of more reasonable Japanese standard will be expected by applying the study result of naval architecture and navigation and by the cooperation of ship operators to use fairway, naval architects to built ships and civil engineers to dredge fairway. The concept of a fairway in 'Design standard fur fairway in next generation' is defined as passage for approach channel) and traffic lane designated by light buoys as navigable water for safe navigation. In 'Design standard for fairway in next generation' depth, width and alignment are picked up among many design elements of a fairway. Design method for those elements is shown based on design ships and navigational environments. This standard shows the method of design for each dimension depending on characteristic on design ship and weather and sea condition. On the other hand, in case of existing fairway, it is possible to decide the size of ship and navigation criteria by opposite analysis.

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A Study for GASP(GIS Audit Standard Procedure) methodology to set up the GIS Audit process (GIS감리절차 확립을 위한 감리방법론(GASP)엔 관한 연구)

  • 신동빈;맹홍주;전성자
    • Spatial Information Research
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    • v.10 no.1
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    • pp.29-43
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    • 2002
  • The purpose of this study is to set up the GIS Audit methodology through the definition of standard procedure ailed GIS Audit criteria and the result of preliminary study about the GIS Audit. the frame of GIS Audit criteria and the result of preliminary study about the GIS Project and check the GIS Audit methodology is to define a standard process of GIS Project and check the GIS Project according to the standard process. We named the method as CASP(GIS Audit Standard Procedure). GASP method means doing Pilot Project for setting the sample standard procedure(named Prototype) of total GIS Project process, and checking the activity to fulfill the prototype. GASP method is advanced method for GIS Audit to analyze the full range of GIS Project and characteristics of GIS contents.

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A W-Band Millimeter-Wave Power Standard Transfer System Using the Direct Comparison Method (직접 비교법을 이용한 W-Band 밀리미터파 전력 표준 전달 시스템)

  • Kwon, Jae-Yong;Kang, Tae-Weon;Kang, Jin-Seob;Lee, Dong-Joon
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.24 no.1
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    • pp.47-54
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    • 2013
  • This paper introduces a W-band millimeter-wave power standard transfer system using the direct comparison method. The transfer system was developed to evaluate the effective efficiency and calibration factor of a W-band waveguide power sensor. The evaluation method and the measured results of the directional coupler that characterizes the calibration system are studied. The uncertainties of the standard transfer system are investigated, and the major uncertainty contributors are discussed as well. The performance of the realized W-band power standard transfer system was verified by comparing results with reference values.

A Study on the Standard Method of Measurement Information Communication Field Contractors (정보통신시설공사 수량산출기준에 관한 연구)

  • Seol, Dong-Hwa;Lee, Kwang-Hee
    • Journal of The Institute of Information and Telecommunication Facilities Engineering
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    • v.2 no.4
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    • pp.52-63
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    • 2003
  • This study proposes a change from the currentexpected price integrated system, which is based on the standard of estimated unit manpower and material, to a new actual construction cost integrated system. In order to implement it, the standard method of measurement organization system as well as the communication area standard of estimated unit manpower and material should be changed Moreover, the work breakdown structure and itemized structure should be assorted.

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