• Title/Summary/Keyword: Sintering rate

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A Quantitative Evaluation of Combustion Characteristics of Coke/Anthracite in an Iron Ore Sintering Bed (소결층 내 코크스/무연탄 연소 특성의 정량적 평가)

  • Yang, Won;Yang, Gwang-Hyeok;Choi, Sang-Min;Choe, Eung-Su;Lee, Deok-Won;Kim, Seong-Man
    • 한국연소학회:학술대회논문집
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    • 2004.11a
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    • pp.33-40
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    • 2004
  • Combustion of coke/anthracite in an iron ore sintering bed is characterized quantitatively by introducing newly defined parameters related to propagation and thickness of combustion zone and maximum temperature. The parameters are obtained by sintering pot experiment and I-D, unsteady numerical model which treats solid material as multiple solid phases. Experiments and calculations are performed for various major operating parameters: air inlet velocity, different type of fuels which have different reactivity and diameter of the solid fuel. Effects of the operating parameters on the productivity and quality of the sintering process are investigated and evaluated quantitatively and the results show that optimized air supply rate and diameter of anthracite for replacement of coke can be obtained. This approach can be applied to other kinds of combustors for characterization of the combustion in the solid fuel beds.

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Effects of Sintering Atmosphere and Dopant Addition on the Densifcation of $SnO_2$ Ceramics (첨가제와 소결분위기가 $SnO_2$ 요업체의 치밀화에 미치는 영향)

  • 정재일;김봉철;장세홍;김정주
    • Journal of the Korean Ceramic Society
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    • v.34 no.12
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    • pp.1221-1226
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    • 1997
  • The effects of sintering atmosphere and dopant addition on the behavior of densification and grain growth of SnO2 ceramics were investigated with consideration of defect chemistry. CoO and Nb2O5 were chosen as dopants, and oxygen and nitrogen were used for controlling of sintering atmospheres. With the decrease of oxygen partial pressure, densification was depressed due to evaporation of SnO2 ceramics. In the case of SnO2 sintering, the addition of CoO, which produced oxygen vacancy in SnO2 ceramics, led to acceleration of densification and grain growth. On the contrary, when Nb2O5 as a dopant producing Sn vacancy was added to SnO2 ceramics, densification and grain growth were simultaneously retarded. As results, it was conformed that diffusion of oxygen ions was rate determinant in densification and grain growth of SnO2 ceramics.

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Effects of Sintering Conditions on the Properties of Sintered Molybdenum

  • Kadokura, Takanori;Hiraoka, Yutaka;Nakabayashi, Seiji;Yamamoto, Yoshiharu
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1153-1154
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    • 2006
  • Effects of sintering conditions such as sintering temperature and heating rate on oxygen content, density, microstructure and toughness of sintered Mo were investigated. The oxygen content of the sintered Mo significantly depended on the sintering conditions. The oxygen content of the primary sintered(below 1673 K) Mo influenced the densifications. The number of pores at grain boundaries of the secondary sintered(at 2073 K)Mo depended on the oxygen content of the primary sintered Mo. Grain growth of the secondary sintered Mo was inhibited by the existence of pores at the grain boundaries. The secondary sintered Mo having larger number of pore and smaller grain size demonstrated higher strength.

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The Characteristic of Agglomerate and Sintering of Y-PSZ Powders Prepared by Different Processes (제조방법에 따른 Y-PSZ 분말의 응집 및 소결특성)

  • Lee, Jong-Kook;Kim, Hwan;Hwang, Kyu-Hong
    • Journal of the Korean Ceramic Society
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    • v.22 no.5
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    • pp.9-16
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    • 1985
  • Agglomeration of Y-PSZ and its related properties were studied. The ultrafine $ZrO_2$ powder containg 3 mol% $Y_2O_3$ was prepared by 1) coprecipitation method b) hot petroleum drying method c) sol-gel method and the characteristics of calcined powders and the microstructures of sintered body were observed. Powder prepared by the coprecipitation method was about 125$\AA$ in crystallite size and 0.1~1.0${\mu}{\textrm}{m}$ of intra-agglomerate pore size when calcined at $600^{\circ}C$ for 1 hour. because of small crystallite size and weak agglo merate strength resultant densification of sintered body was high. But above the temperature of 130$0^{\circ}C$ efflorescent phenomena due to anions attached to powder surface was observed. Powder prepared by hot petroleum drying method was 65$\AA$ in crystallite size and 1~10${\mu}{\textrm}{m}$ of intraagglome-rate pore size and it was observed that the agglemerates were formed during the calcining process. In this case despite of small crystallite size the rate of sintering was slow and the existing lenticular interagglomerate pore was not eliminated to the final stage of sintering. Powder prepared by sol-gel method showed solid agglomertes due to rapi dhydrolysis reaction. In this powder which involves strong solid agglomerates overall sintering rate was determined by the sintering between the agglomerates and therefore sinterability of powders made by sol-gel method was very poor.

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A Study on the Fluidity Properties and Strength Properties of Non-sintered Hwangtoh mixed with PVA Fiber (PVA섬유를 혼입한 비소성 황토 콘크리트의 유동특성 및 강도특성에 관한 연구)

  • Lee, Sang-Soo
    • Journal of the Korea Institute of Building Construction
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    • v.10 no.3
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    • pp.49-56
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    • 2010
  • The purpose of this study is to examine the effect of variations in the mix rate of PVA fiber and the replacement ratio of non-sintering Hwangtoh on non-sintering Hwangtoh mortar and concrete mixed with PVA fiber. For water to binder ratio, mortar and concrete were both 50%, and PVA fiber mix rate was 0% and 0.3%. The replacement ratio of non-sintering Hwangtoh was 0, 25, 50 and 75(%) for mortar, and 0, 15, 30 and 50(%) for concrete. The properties of the mortar and concrete were compared and analyzed in 4 different levels, and the results can be summarized as follows. The replacement ratio of 30% of the non-sintering Hwangtoh, and the PVA fiber mix rate of 0.3% is determined to result in concrete of high quality, including strength and fluidity, and crack control by plastic shrinkage.

Evaluation of Mechanical Properties and Microstructure Depending on Sintering Heating Rate of IN 939 W Alloy (IN 939 W 합금의 소결 승온 속도에 따른 물리적 특성과 미세조직 분석)

  • Jeon, Junhyub;Lee, Junho;Seo, Namhyuk;Son, Seung Bae;Jung, Jae-Gil;Lee, Seok-Jae
    • Journal of Powder Materials
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    • v.29 no.5
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    • pp.399-410
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    • 2022
  • Changes in the mechanical properties and microstructure of an IN 939 W alloy according to the sintering heating rate were evaluated. IN 939 W alloy samples were fabricated by spark plasma sintering. The phase fraction, number density, and mean radius of the IN 939 W alloy were calculated using a thermodynamic calculation. A universal testing machine and micro-Vickers hardness tester were employed to confirm the mechanical properties of the IN 939 W alloy. X-ray diffraction, optical microscopy, field-emission scanning electron microscopy, Cs-corrected-field emission transmission electron microscopy, and energy dispersive X-ray spectrometry were used to evaluate the microstructure of the alloy. The rapid sintering heating rate resulted in a slightly dispersed γ' phase and chromium oxide. It also suppressed the precipitation of the η phase. These helped to reinforce the mechanical properties.

Process Modeling of an Iron Ore Sintering Bed for Flue Gas Recirculation (배가스 재순환 적용을 위한 제철 소결 베드 프로세스 모델링)

  • Ahn, Hyung-Jun;Choi, Sang-Min;Cho, Byung-Kook
    • Journal of the Korean Society of Combustion
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    • v.16 no.4
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    • pp.23-30
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    • 2011
  • In the iron and steel manufacturing, sintering process precedes blast furnace to prepare feed materials by agglomerating powdered iron ore to form larger particles. There are several techniques which have devised to improve sintering production and productivity including flue gas recirculation(FGR) and additive gas enriched operation. The application of those techniques incurs variations of process configurations as well as inlet and outlet gas conditions such as temperature, composition, and flow rate which exert direct influence on reactions in the bed or the operation of the entire plant. In this study, an approach of sintering bed modeling using flowsheet process simulator was devised in consideration of FGR and the change of incoming and outgoing gas conditions. Results of modeling for both normal and FGR sintering process were compared in terms of outgoing gas temperature, concentration, and moisture distribution pattern as well as incoming gas conditions. It is expected to expand the model for various process configurations with FGR, which may provide the usefulness for design and operation of sintering plant with FGR.

Microstructural evolution in liquid-phase sintered $\alpha$-silicon carbide (액상소결 $\alpha$형 탄화규소의 미세구조 변화)

  • 이종국;강현희;박종곤;이은구
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.2
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    • pp.324-331
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    • 1998
  • After the addition of yttrium aluminum garnet of 2, 5, 10 mol% as a sintering aid, $\alpha$-silicon carbides were prepared by a liquid-phase sintering at $1850^{\circ}C$, and the microstructural evolution was investigated during sintering as functions of liquid-phase amount and sintering time. The highest apparent density in each compositions was obtained in specimens sintered for 2 h, and the percentage of weight loss increased with sintering time. By increasing the amount of sintering aid (yttrium aluminum garnet), the rate of grain growth during sintering decreased, but the apparent density of sintered body increased. The phase transformation from 6H-SiC to 4H-SiC was partially observed in specimens sintered for a long time, and so, a few rod-like grains were observed.

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Microwave Sintering Behavior and Electrical Properties of BaTiO$_3$ Ceramics (BaTiO$_3$ 세라믹의 마이크로파 소성 및 전기적 특성)

  • Bai, Kang;Kim, Ho-Gi
    • Journal of the Korean Ceramic Society
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    • v.35 no.11
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    • pp.1203-1211
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    • 1998
  • The microwave sintered BaTiO3 samples were obtained by using the microwave sintering device which can precisely control the sintering temperature and the sinter time by using IR optical thermometer and PID temperature controller. During microwave sintering the internal temperature of samples were mesur-ed by the optical fiber thermometer to compare the sintering behaviors between microwave- and con-ventionally sintered ones. The former showed the faster rate of grain growth with sintering time and the larger grain size than the latter. Also they showed the similar pattern of dielectric properties with tem-perature changes from 2$0^{\circ}C$ to 16$0^{\circ}C$.

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