• 제목/요약/키워드: Refinement behavior

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Structural Characterization of the (TEX)$Sr_2Co_0.5Nb(Ta)_0.5O_4$(/TEX) and (TEX)$Sr_3CoNb(Ta)O_7$(/TEX)

  • 조한상;;류광현;유철현
    • Bulletin of the Korean Chemical Society
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    • 제21권7호
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    • pp.679-684
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    • 2000
  • The Sr2Co0.5Nb(Ta)0.5O4 and Sr3CoNb(Ta)O7 compounds, both with Ruddlesden-Popper structures, have been synthesized by the ceramic method at $1150^{\circ}C$ under atmospheric pressure. The crystallographic structure of the compounds was assigned to the tetr agonal system with space group 14/mmm by X-ray diffraction(XRD) Rietveld refinement. The reduced lattice volume and lattice parameters increased as the Ta with 5d substitutes for the Nb with 4d in the compounds. The Co/Nb(Ta)O bond length has been determined by X-ray absorption spectroscopic(EXAFS/XANES) analysis and the XRD refinement. The CoO6,octahedra were tetragonally distorted by elongation of Co-O bond along the c-axis. The magnetic measurement shows the compounds Sr2Co0.5Nb(Ta)0.5O4 and Sr3CoNb(Ta)O7 have paramagnetic properties and the Co ions with intermediate spin sates between high and low spins in D4h symmetry. All the compounds showed semiconducting behavior whose electrical conductivity increased with temperature up to 1000 K. The electrical conductiviy increased and the activation energy for the conduction decreased as the number of perovskite layers increased in the compounds with chemical formula An+1BnO3n+1.

2Cr 및 12Cr 크롬강튜브의 고온 장시간 사용에 따른 열화현상 (Material Degradation of 2Cr and 12Cr Tube Steels for High Temperature and Long-Time Exposure)

  • 최병학;이길재;김상호;홍기용;김우식;백운봉;남승훈
    • 한국가스학회지
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    • 제16권5호
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    • pp.28-34
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    • 2012
  • 보일러 튜브용 크롬강의 열화기구에 대해 고찰하였다. 크롬강의 열화는 경도 및 응력-파단 수명의 변화를 동반하는데, 이는 주로 탄화물 분해 거동에 의존한다. 그런데 2Cr강인 T22의 열화는 이러한 탄화물 거동에 따르지만 12Cr강인 X20의 열화는 마르텐사이트 래쓰 성장거동에 따르기도 한다. T22와 X20의 열화에 의한 경도값과 응력-파단수명 변화현상을 미세조직적인 측면에서 고찰하였다.

오스테나이트계 고망간강에서 인장 특성과 피로거동에 미치는 변형유기상의 영향 (The Effect of Deformation Induced Phase on Tensile Properties and Fatigue Behavior of Austenitic High Mn steel)

  • 최상민;권숙인
    • 열처리공학회지
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    • 제7권4호
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    • pp.277-287
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    • 1994
  • The effect of grain size on the tensile properties and fatigue behavior of austenitic high Mn steel has been investigated. The recrystallized austenite grain size of the cold rolled high Mn steel was increased as the annealing temperature increased from $600^{\circ}C$ to $1000^{\circ}C$. Larger austenite grain size decreased the yield strength and the tensile strength, and increased the uniform elongation due to transformation of some austenite into twins or E-martensite phase during deformation. Austenite grain refinement increased the tendency to form dislocation cells, instead. The specimen annealed at $1000^{\circ}C$ with large grain size showed lower fatigue crack propagation rate in low ${\Delta}K$ region due to rougher fracture surface caused by formation of deformation twins during fatigue at the crack tip region.

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Analysis of the dynamical behavior of piezoceramic actuators using piezoelectric isogeometric finite elements

  • Willberg, Christian
    • Advances in Computational Design
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    • 제1권1호
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    • pp.37-60
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    • 2016
  • In this paper an electromechanically coupled isogeometric finite element is utilized to analyse Lamb wave excitation with piezoceramic actuators. An effective actuator design reduces the energy needed for Lamb wave excitation, which is beneficial if a structural health monitoring system should be applied for a structure. For a better understanding of the actuator behavior the piezoeceramics are studied both free and bonded at a structure. The numerical part of the analysis is performed utilizing isogeometric finite elements. To obtain the optimal performance for the numerical analysis the effect of k-refinement of the isogeometric element with respect to the convergence is studied and discussed. The optimal numerical setup with the best convergence rate is proposed and is validated with free piezoeceramic actuators. The validated model is then utilized to study the impact of actuator shape and adhesive bondline effect to the wave amplitude. The study shows that simplified analytical equations do not predict the optimal excitation frequencies for all piezoceramic designs accurately.

풀러렌이 분산된 알루미늄기지 나노복합재의 기계적 거동 (Mechanical Behavior of Al/C60-fullerenes Nanocomposites)

  • 최현주
    • Composites Research
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    • 제26권2호
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    • pp.111-115
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    • 2013
  • $C_{60}$ 풀러렌이 분산된 알루미늄기지 복합재를 볼 밀링법과 열간압연 공정을 이용하여 제조하였다. 볼 밀링이 진행되는 동안, 알루미늄기지는 그 결정립이 100 nm 이하 수준으로 미세화되어 강화되었다. 동시에 $C_{60}$ 풀러렌이 알루미늄기지 내에 균일하게 분산되어, $C_{60}$ 풀러렌의 첨가량이 증가할수록 복합재의 강도가 증가하였으며, 10 vol%의 $C_{60}$ 풀러렌을 포함하는 순 알루미늄기지 복합재는 1 GPa 수준의 압축 강도를 나타내었다.

Sintering Behavior of the Net-shaped Fe-8wt%Ni Nanoalloy Powder and Related Mechanical Property

  • Cha, Berm-Ha;Kang, Yun-Sung;Lee, Sung-Ho;Lee, Jai-Sung
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.501-502
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    • 2006
  • The present investigation has been performed on full densification behavior and mechanical property of the powder injection molded Fe-8wt%Ni nanoalloy powder. The net shaping process of the nanopowder was conducted by powder injection molding (PIM) process. The key-process for fabricating fully densified net-shaped nanopowder by pressureless sintering is an optimal control of agglomerate size of nanopowder. Enhanced mechanical property of PIMed Fe-Ni nanopowder is explained by grain refinement and microstructural uniformity.

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임계상대밀도 모델을 이용한 분말 등통로각압축 공정시 분말 치밀화 거동 (Analysis of Densification Behavior during Powder Equal Channel Angular Pressing using Critical Relative Density Model)

  • 복천희;유지훈;윤승채;김택수;천병선;김형섭
    • 한국분말재료학회지
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    • 제15권5호
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    • pp.365-370
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    • 2008
  • In this study, bottom-up powder processing and top-down severe plastic deformation processing approaches were combined in order to achieve both full density and grain refinement with least grain growth. The numerical modeling of the powder process requires the appropriate constitutive model for densification of the powder materials. The present research investigates the effect of representative powder yield function of the Shima-Oyane model and the critical relative density model. It was found that the critical relative density model is better than the Shima-Oyane model for powder densification behavior, especially for initial stage.

남성 소비자의 소비가치에 따른 신사복 구매행동의 차이 (Differences in Purchase Behavior of Men's Suits among Male Consumption Value Groups)

  • 강유림;박광희
    • 한국의류학회지
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    • 제42권4호
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    • pp.584-598
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    • 2018
  • This study classified respondents by consumption value and analyzed differences in the purchase behavior of men's suits among consumption value groups. Frequency analysis, factor analysis, cluster analysis, and analysis of variance were conducted in order to analyze research problems. Factor analysis results showed that male consumption values included safety-oriented value, individuality-oriented value, others-oriented value, pleasure-oriented value, aesthetic-oriented value, low price-oriented value, community-oriented value, utility-oriented value, innovation-oriented value, and self-expression oriented value. The study divided respondents into personal satisfaction pursuit group, beauty & functionality pursuit group, individuality pursuit group, and others-oriented & low cost preference group according to consumption value. There were significant differences in selection criteria for men's suit (product image, physical properties of product, and brand name), selection reasons of brand (fashion & ostentation, individuality, and refinement), store attributes (store environment/salesperson service, reputation/additional service, and product assortment/shopping convenience).

마그네슘의 등통로각압축 공정 시 변형 및 파괴 거동에 대한 유한요소해석 (Analysis for Deformation and Fracture Behavior of Magnesium during Equal Channel Angular Pressing by the Finite Element Method)

  • 윤승채;팜쾅;김형섭
    • 대한금속재료학회지
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    • 제46권3호
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    • pp.144-149
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    • 2008
  • Equal channel angular pressing (ECAP) has been studied intensively over the decade as a typical top-down process to produce ultrafine/nano structured materials. ECAP has successfully been applied for a processing method of severe plastic deformation to achieve grain refinement of magnesium and to enhance its low ductility. However, difficult-to-work materials such as magnesium and titanium alloys were susceptible to shear localization during ECAP, leading to surface cracking. The front pressure, developed by Australian researchers, can impose hydrostatic pressure and increase the strain level in the material, preventing the surface defect on workpiece. In the present study, we investigated the deformation and fracture behavior of pure magnesium using experimental and numerical methods. The finite element method with different ductile fracture models was employed to simulate plastic deformation and fracture behavior of the workpiece.

노년여성의 화장행동, 심리적 특성과 영정사진 화장이미지 선호의 관계연구 (A Study on the Relationship between Makeup Behavior, Psychological Traits and Preference for the Makeup Images of Funeral portrait in Elderly Women)

  • 최정순;김경희
    • 한국의상디자인학회지
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    • 제18권1호
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    • pp.1-10
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    • 2016
  • The purpose of this study was to examine the influence of elderly women's makeup behavior, psychological traits and demographic variables on their preference for makeup images in daily life(hereinafter called general makeup image) and for the makeup images of their own future funeral portraits. As for the method of research, a research study was implemented by using the questionnaire method. Seven factors were selected for makeup behavior: fashionability, conformity, subjectivity, instrumentality, interpersonal orientation and conspicuousness. The selected psychological traits were personality, death attitude and depression. Preference for general makeup image and for the makeup image of funeral portrait were investigated in terms of four: agreeableness, refinement, individuality and dignity. The subjects in this study were 651 female elderly residents in and around Seoul who were in their 60s to 80s. Concerning data analysis, factor analysis, Cronbach alpha coefficient, Pearson productmoment correlation coefficient, t-test, one-way ANOVA, Duncan's multiple range test and multiple regression analysis were utilized. Concerning the influence of the elderly women's makeup behavior, personality, death attitude, depression and demographic variables on preference for the makeup image of funeral portrait, their preference for an agreeable makeup image was analyzed. Thus, makeup behavior, personality, death attitude and depression were identified as the variables to exert a significant influence on preference for the makeup images of funeral portrait. The findings of the study are expected to help make makeup for funeral portrait entrenched as a part of the beauty industry and to make a contribution to the development of the beauty industry.

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