• 제목/요약/키워드: Pre-calibration

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200 N급 GCH4/LOx 소형로켓엔진의 형상설계와 성능시험평가 (Part I: 예비설계와 시험장치) (Configuration Design, Hot-firing Test and Performance Evaluation of 200 N-Class GCH4/LOx Small Rocket Engine (Part I: A Preliminary Design and Test Apparatus))

  • 김영진;김민철;김정수
    • 한국추진공학회지
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    • 제24권1호
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    • pp.1-8
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    • 2020
  • 메탄/산소 이원추진제 소형로켓엔진의 성능평가를 위한 형상설계 및 시험평가시스템을 구축하였다. 인젝터는 추진제 미립화 성능이 우수하고, 연소불안정성이 적은 스월 동축형(swirl-coaxial) 방식을 채택하였다. 연소효율 비교를 위해 연소실의 종횡비는 1.5, 1.8, 2.1로 각각 설정하였다. 그리고 정밀추력측정장치의 측정 신뢰성을 높이기 위해 pre/post calibration을 실시하였다. 그 결과, 예비 지상연소시험에서 추력과 비추력은 89.2 N, 181.8 s로 78.4%의 효율을 가지고, 특성속도는 84.2%의 효율을 갖는 것이 확인되었다.

표준 요 시료 중 Oxalate의 측정을 위한 FT-NIR 분광기의 유용성 검정 (Evaluation of Fourier Transform Near-infrared Spectrometer for Determination of Oxalate in Standard Urinary Solution)

  • 김영은;홍수형;김정완;이종영
    • Journal of Preventive Medicine and Public Health
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    • 제39권2호
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    • pp.165-170
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    • 2006
  • Objectives : The determination of oxalate in urine is required for the diagnosis and treatment of primary hyperoxaluria, idiopathic stone disease and various intestinal diseases. We examined the possibility of using Fourier transform near-infrared (FT-NIR) spectroscopy analysis to quantitate urinary oxalate. The practical advantages of this method include ease of the sample preparation and operation technique, the absence of sample pre-treatments, rapid determination and noninvasiveness. Methods : The range of oxalate concentration in standard urine solutions was $0-221mg/{\ell}$. These 80 different samples were scanned in the region of 780-1,300 nm with a 0.5 nm data interval by a Spectrum One NTS FT-NIR spectrometer. PCR, PLSR and MLR regression models were used to calculate and evaluate the calibration equation. Results : The PCR and PLSR calibration models were obtained from the spectral data and they are exactly same. The standard error of estimation (SEE) and the % variance were $10.34mg/{\ell}$ and 97.86%, respectively. After full cross validation of this model, the standard error of estimation was $5,287mg/{\ell}$, which was much smaller than that of the pre-validation. Furthermore, the MCC (multiple correlation coefficient) was 0.998, which was compatible with the 0.923 or 0.999 obtained from the previous enzymatic methods. Conclusions : These results showed that FT-NIR spectroscopy can be used for rapid determination of the concentration of oxalate in human urine samples.

USE OF NEAR-INFRARED SPECTROSCOPY TO PREDICT OIL CONTENT COMPONENTS AND FATTY ACID COMPOSITION IN OLIVE FRUIT

  • Lorenzo, Leon-Moreno;Ana, Garrido-Varo;Luis, Rallo-Romero
    • 한국근적외분광분석학회:학술대회논문집
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    • 한국근적외분광분석학회 2001년도 NIR-2001
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    • pp.1512-1512
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    • 2001
  • The University of Cordoba conducts since 1991 a breeding program to obtain new olive cultivars from intraspecific crosses. The objective is to obtain new early bearing and high-quality cultivars. In plant breeding, many seedlings must be tested to increased the chance of getting desirable genotypes. Therefore, fast, cheap and accurate methods of analysis are necessary. The conventional laboratory techniques are costly and time-consuming. Near Infrared Spectroscopy (NIRS) can satisfy the characteristics requested by plant breeders and offers many advantages such as the simultaneous analysis of many traits and cheap cost. The objective of this work was to asses the performance of NIRS to estimate oil fruit components (fruit weight, flesh moisture, flesh/stone ratio and oil flesh content in dry weight basis) and fatty acid composition in olive fruit. Genotypes from reciprocal crosses between ‘Arbequina’, ‘Frantoio’ and ‘Picual’ cultivars have been used in this study. A total of 287 samples, each from a single plant, were scanned using a DA-7000 Diode Array VIS/NIR Analysis System (Perten Instruments), which covers the visible and NIR range from 400-1700 nm. All samples were analysed for fatty acid composition (gas chromatography) and 220 for oil fruit components (oil content by nuclear magnetic resonance), 70% and 30% of samples were randomly assign for the calibration and validation sets respectively. The preliminary results shows that calibration for palmitic, oleic and linoleic acids were highly accurate with calibration and validation values of $r^2$ from 0.85 to 0.95 and 0.76 to 0.91 respectively. Calibration for palmitoleic and estearic acids were less accurate, probably because of the narrow range of variability available for these fatty acids. For the oil fruit components, calibration were high accurate for flesh moisture and oil flesh content in dry weight basis ($r^2$ higher than 0.90 in both calibration and validation sets) and less accurate for the other characteristics evaluated. The first results obtained indicate that NIRS analysis could be an ideal technique to reduce the cost, time and chemical wasted necessary to evaluate a large number of genotypes and it is accurate enough to use for pre-selecting genotypes in a breeding program.

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PHASE-B PRE-SIMULATION USING BORON AND GADOLINIUM AS POISON IN THE MODERATOR SYSTEM FOR WOLSONG-1

  • Kim, Sung-Min;Kim, Hyeong-Taek;Donnelly, Jim;Marleau, Guy
    • Nuclear Engineering and Technology
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    • 제44권5호
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    • pp.551-560
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    • 2012
  • The Wolsong-1 (W-1) Phase-B pre-simulations were carried out in preparation for tests to be conducted for the restart of the reactor after a major refurbishment project that included replacement of the pressure tube. These pre-simulations for Wolsong-1 Phase-B differ from those in the past that were performed for the Wolsong-1,2,3,4 tests in that these tests use the WIMS/DRAGON/RFSP-IST code suite for verification of the tests and gadolinium instead of the traditional PPV/MULTICELL/RFSP code system and boron as poison in the moderator system. The use of gadolinium is deemed not to have domestically accumulated experience gained from the previous Phase-B tests. Thus, it is appropriate to conduct a study in order to gain a correct understanding and interpretation of potential differences in test results stemming from using gadolinium rather than boron. Although the calibration of the reactivity device will not be noticeably different using boron and gadolinium at a constant moderator temperature, the temperature dependency of the neutronic behavior due to the presence of gadolinium in the moderator system might be pronounced. The results of the pre-simulations using gadolinium revealed that the moderator temperature reactivity coefficients indeed showed significant differences in comparison with those with boron. In order to secure the validity of the analysis results, the newly acquired WIMS/DRAGON/RFSP-IST code suite was verified against the W-2,3,4 Phase-B test results. The results of the new code suite verifications revealed some overall improvements in accuracy; justification of the use of the code can be claimed for the validation of the W-1 Phase-B test results.

HPLC를 이용한 잎담배 중 유기산 함량 분석 (Determination of Organic Acids in Tobacco Leaves by HPLC)

  • 민혜정;장석수;김익중;신준원;김용하;민영근
    • 한국연초학회지
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    • 제28권2호
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    • pp.130-135
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    • 2006
  • This study was carried out to improve the analytical methods for determination of organic acids in tobacco leaf by HPLC. The samples for HPLC analysis were pre-treated by means of SPE. The calibration curve for each acid was linear and $R^2$ values ranged from 0.9990 to 1.0000. The limit of detection were obtained from the calibration curves and their values were between 1.39 to $4.87{\mu}g/mL$. Recovery rates of organic acids were between 88.6 % to 98.5 %. The concentrations of organic acids among the various tobacco leaves were compared to the concentration of organic acids, were in the order oriental, burley, flue-cured tobacco. In the case of flue-cured and oriental tobacco leaves, the order of concentration of organic acids was malic acid, oxalic acid, citric acid. But in the case of burley tobacco leaves, the order of concentration of organic acids was citric acid, oxalic acid, malic acid.

공간주파수대역에서 기저대역 확장을 통한 원전 대비시험편과 대비 보정 시험편의 초음파 영상 개선 (Ultrasonic Images Enhancement of the SS Reference Specimen and the Reference Calibration Block for NPPs by the Combining Bases of Support for Spatial Frequency)

  • 박치승;김선진
    • 한국재료학회지
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    • 제13권10호
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    • pp.651-657
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    • 2003
  • Ultrasonic microscope has been used to detect the defects on surface or inner solid. Conventionally, it has used at a single operating frequency. The resolution and quality of the measured images are determined by a characteristic of the transducer of the ultrasonic microscope. The conventional ultrasonic microscope has been used envelope detector to detect the amplitude of reflected signal, but the changes in amplitude is not sensitive enough for specimen with microstructure that in phase. In this paper, we have studied multi-frequency depth resolution enhancement with ultrasonic reflection microscope for the reflectors of a stainless steel reference specimen and a reference calibration block to be used as the material in nuclear power plants for ISI, PSI. Increased depth resolution can be obtained by taking two, three-dimensional images at more that one frequency and numerically combining the results. As results of the experiment, we could get enhanced images with the rate of contrast in proportion and high quality signal distribution for the image to the changing rate of depth for the reflectors of the two kinds of specimens.

영상처리를 이용한 Mark 판독 기법에 관한 연구 (A Study on the Mark Reader Using the Image Processing)

  • 김승호;김범진;이용구;노도환
    • 제어로봇시스템학회:학술대회논문집
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    • 제어로봇시스템학회 2000년도 제15차 학술회의논문집
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    • pp.83-83
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    • 2000
  • Recently, Vision system has being used all around industry. Sensor systems are used for Mark Reader, for example, optical scanning is proximity sensor system, have many disadvantages, such as, lacking user interface and difficulty to store original specimens. In contrast with this, Vision systems for Mark Reader has many advantages, including function conversion to achieve other work, high accuracy, high speed, etc. In this thesis, we have researched the development of Mark Reader by using a Vision system. The processing course of this s)'stem is consist to Image Pre-Processing such as noise reduction, edge detection, threshold processing. And then, we have carried out camera calibration to calibrate images which are acquired from camera. After searching for reference point within scanning area(60pixe1${\times}$30pixe1), we have calculated points crossing by using line equations. And then, we decide to each ROI(region of interest) which are expressed by four points. Next we have converted absolute coordinate into relative coordinate for analysis a translation component. Finally we carry out Mark Reading with images classified by six patterns. As a result of experiment which follows the algorithm has proposed, we have get error within 0.5% from total image.

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On the Optical Characteristics of Solar X-Ray Telescopes: Possible Relation between Vignetting Effect and Mirror Scattering

  • Shin, Jun-Ho;Sakurai, Takashi
    • 천문학회보
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    • 제36권2호
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    • pp.87.1-87.1
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    • 2011
  • Since early 90's, the solar X-ray telescopes such as Yohkoh SXT and Hinode XRT have observed coronal magnetic structures on the Sun's surface in the range of about $40'{\times}40'$ field-of-view (FOV) covering the full solar disk. Thus it has been stressed by the scientists that the optical structure of solar telescopes should be designed with care for improving the uniformity over a wide FOV. There would be, however, no unique solution in designing the optical system of a telescope for overcoming perfectly the problem of off-axis response variation. As a consequence, the correction of optical imperfectness of telescopes has become an important calibration step that should be performed beforehand when the observed images are to be used for photometric purposes. In particular, a special care should be taken when performing the temperature analysis with thin and thick filters for flaring activities observed at the periphery of the full FOV. From the analyses of both pre-launch calibration and in-flight observation data, the optical characteristics for describing the performance of solar X-ray telescopes, especially in view of their energy dependence, will be introduced and discussed in our presentation.

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마른김 품질 평가를 위한 FT-NIR 분광기 활용 연구 (A study on the use of FT-NIR spectophotometer for dried laver quality evaluation)

  • 이경인;이근직;윤영승
    • 한국해양바이오학회지
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    • 제14권2호
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    • pp.69-75
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    • 2022
  • The micro-Kjeldahl method, a common technique for analyzing crude proteins, is time-consuming and dangerous due to the employment of reagents such as sulfuric acid and sodium hydroxide. However, a Fourier transform near-infrared (FT-NIR) spectrophotometer analysis can be completed in under a minute after simple pre-processing if data has been gathered using sufficient reference material in advance. Furthermore, the use of safe reagents in this technique ensures the safety of the experimenter and the environment. In addition, a portable FT-NIR spectrophotometer enables real-time measurement at processing or distribution sites and has recently gained popularity. The standard errors of calibration and regression (r2) for the calibration result for estimating the crude protein content of dried laver were 0.9775 and 1.2526, respectively. The standard error of prediction was 1.1814, and the r2 was 0.9303 in the validation results, which was a good level. In the present study, a method for predicting the crude protein content of dried laver using an FT-NIR spectrophotometer in the range of 29%-40% crude protein content has been reported.

Offset 개선을 위해 Auto Zero Calibration 기법을 적용한 8-bit / 49.98dB-SNDR SAR ADC 설계 (ENOB 8-bit / 49.98dB-SNDR SAR ADC with Auto Zero Calibration Technique for Offset Improvement)

  • 정채은;오주원;부영건;이강윤
    • 반도체공학회 논문지
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    • 제2권3호
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    • pp.13-18
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    • 2024
  • 본 논문은 Reference generator 와 Comparator 에서 발생하는 offset 을 최소화하고 정확도를 향상시키기 위해 Auto zero 기술을 활용한 회로를 제안한다. 이에 대한 근거로 Auto zero 사용 전/후를 비교했을 때 약 90% 표준 편차가 줄어드는 결과를 얻을 수 있었다. 제안하는 회로는 55nm CMOS 공정을 사용하였으며, input frequency 는 781.2 Hz, Effective Number of Bits(ENOB) 8.01bit, Signal-to-Noise Distortion Ratio(SNDR)이 49.98dB 을 보여준다.