• Journal of the Korean Applied Science and Technology
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• v.30 no.4
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• pp.602-611
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• 2013

We have investigated the influence of system composition and preparation conditions on the particle size of vitamin E acetate (VE)-loaded nanoemulsions prepared by PIC(phase inversion composition) emulsification. This method relies on the formation of very fine oil droplets when water is added to oil/surfactant mixture. The oil-to-emulsion ratio content was kept constant (5 wt.%) while the surfactant-to-oil ratio (%SOR) was varied from 50 to 200 %. Oil phase composition (vitamin E to medium chain ester ratio, %VOR) had an effect on particle size, with the smallest droplets being formed below 60 % of VOR. Food-grade non-ionic surfactants (Tween 80 and Span 80) were used as an emulsifier. The effect of f on the droplet size distribution has been studied. In our system, the droplet volume fraction, given by the oil volume fraction plus the surfactant volume fraction, was varied from 0.1 to 0.3. The droplet diameter remains less than 350 nm when O/S is fixed at 1:1. The droplet size increases gradually as the increasing the volume fraction. Particle size could also be reduced by increasing the temperature when water was added to oil/surfactant mixture. By optimizing system composition and homogenization conditions we were able to form VE-loaded nanoemulsions with small mean droplet diameters (d < 50 nm). The PIC emulsification method therefore has great potential for forming nanoemulsion-based delivery systems for food, personal care, and pharmaceutical applications.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.28 no.5
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• pp.587-593
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• 2004

In this paper, flow characteristics of plasma flow in a micro-tube were investigated experimentally using micro particle image velocimetry(micro-PIV). For comparison, the experiments were repeated for deionized(DI) wale. instead of plasma. Both velocity profiles of plasma and do-ionized water are well agreed with the theoretical velocity distribution of newtonian fluid. We also carried out generating plasma-in-oil droplet formation at a Y-junction microchannel. In order to clarify the hydrodynamic aspects involved in plasma droplet formation, Rhodamine-B were mixed with plasma only for visualization of plasma droplet. With oil as the continuous phase and plasma as the dispersed phase, plasma droplet can be generated in a continuous phase flow at a Y-junction. For given experimental parameters, regular-sized droplets are reproducibly formed at a uniform flow conditions.

• Particle and aerosol research
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• v.17 no.3
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• pp.43-54
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• 2021

Size distributions of atmospheric particulate matter (PM) and its water-soluble organic and inorganic components were measured between January and February 2021 at an urban site in Gwangju in order to identify the major factors that determine their size distributions. Their size distributions during the study period were mainly divided into two groups. In the first group, PM, NO₃^-, SO₄^2-, NH₄⁺ and water-soluble organic carbon (WSOC) exhibited bi-modal size distributions with a dominant condensation mode at a particle size of 0.32 ㎛. This group was dominated by local production of secondary water-soluble components under atmospheric stagnation and low relative humidity (RH) conditions, rather than long-range transportation of aerosol particles from China. On the other hand, in the second group, they showed tri-modal size distributions with a very pronounced droplet mode at a diameter of 1.0 ㎛. These size distributions were attributable to the local generation and accumulation of secondary aerosol particles under atmospheric conditions such as atmospheric stagnation and high RH, and an increase in the influx of atmospheric aerosol particles by long-distance transportation abroad. Contributions of droplet mode NO₃^-, SO₄^2-, NH₄⁺ and WSOC to fine particles in the second group were significantly higher than those in the first group period. However, their condensation mode contributions were about two-fold higher in the first group than in the second group. The significant difference in the size distribution of the accumulation mode of the WSOC and secondary ionic components between the two groups was due to the influx of aerosol particles with a long residence time by long-distance transport from China and local weather conditions (e.g., RH).

• Particle and aerosol research
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• v.9 no.1
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• pp.23-29
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• 2013

Inertial impaction type mist eliminators are the most effective instruments to separate mist from the gas. In this work, the effect of the horizontal chevron type mist eliminators is characterized experimentally. Droplet size distribution and evaluation of removal efficiency of the chevron type mist eliminators at different gas flows were investigated using an aerosol particle size analyzer and a portable aerosol spectrometer, respectively. The experimental investigations showed that the mist removal efficiency in these instruments is dependent in the droplet size, and the pressure drop is nil.

• Food Science and Biotechnology
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• v.16 no.6
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• pp.999-1005
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• 2007

An oil-in-water (O/W) emulsion [20 wt% com oil, 0.5-6.0 wt% fish gelatin (FG), pH 3.0] was produced by high pressure homogenization, and the influence of pH, protein concentration, and homogenization condition on the formation of FG-stabilized emulsions was assessed by measuring particle size distribution, electrical charge, creaming stability, microstructure, and free FG concentration in the emulsions. Optical microscopy indicated that there were some large droplets ($d>10\;{\mu}m$) in all FG-emulsions, nevertheless, the amount of large droplets tended to decrease with increasing FG concentration. More than 90% of FG was present free in the continuous phase of the emulsions. To facilitate droplet disruption and prevent droplet coalescence within the homogenizer, homogenization time was adjusted in O/W emulsions stabilized by 2.0 or 4.0 wt% FG. However, the increase in the number of pass rather promoted droplet coalescence. This study has shown that the FG may have some limited use as a protein emulsifier in O/W emulsions.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2007.04a
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• pp.106-109
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• 2007

The spray plume characteristics of liquid water jet injected into subsonic cross-flow at 42 m/s were experimentally investigated. Nozzle has a 1.0 m diameter and L/D=5. Droplet sizes, velocities, volume flux were measured at each downstream area of the injector exit using phase Doppler particle anemometry. Measuring probe position is moved with 3-way transversing machine. Experimental results indicate that SMD is varied from 75 to $120{\mu}m$ distribution and it is uncertain layer structure. SMD peaks at the top of the spray plume. This phenomenon is related to the momentum exchange between column waves and cross-flow stream. Droplet vector velocities were varied from 11.5 to 33 m/s. A higher-velocity region can be identified in down edge region at Z/D : 40, 70 and 100. Lower-velocity region were observed on bottom position of the spray plume. Volume flux is a criterion to the droplet concentration. All volume flux distribution has a same structure that continuously decreases from the center region to the edge of the plume. Z/D : 20 is spatially less concentrated than in Z/D : 100.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.13 no.9
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• pp.4334-4340
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• 2012

In this work, we developed and evaluated the Liquid Particle Generator for generating fine particles in the air. The Liquid Particle Generator, which was based on the spray-evaporation method, had two kinds of orifices: 0.3 mm and 0.5 mm. The Liquid Particle Generator was operated at different pressure between 1 bar and 4 bars to find relationship between input pressure and droplet output rate. In addition, the size distribution of the droplets generated by the Liquid Particle Generator with different orifices was measured by the SMPS system and the optical particle counter. As a result, it was shown that the Liquid Particle Generator with 0.3 mm orifice generated droplets of around 0.3 ${\mu}m$ and atomized particles very stably. The Liquid Particle Generator having 0.5 mm orifice generated bigger droplets, compared with the Liquid Particle Generator with 0.3 mm orifice. Additionally, in these Liquid Particle Generators (0.3 mm and 0.5 mm orifice), little coagulation of particles did occur because of fine droplets atomized by the jet. Therefore, the Liquid Particle Generator could be used as an aerosol generator for atomizing fine particles.

• International Journal of Automotive Technology
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• v.4 no.4
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• pp.157-164
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• 2003

An experimental and numerical study was performed to investigate the macroscopic and microscopic atomization characteristics of high-speed diesel spray issued from the common-rail injection system. For the experiments, spray visualization system and a phase Doppler particle analyzer system were utilized to obtain the spray atomization characteristics such as the process of spray development, spray tip penetration, and SMD distribution. In order to analyze the process of spray atomization with KIVA-3 code, the TAB breakup model is changed to the KH-DDB competition model, which assumes the competition between the wave instability and droplet deformation causes the droplet breakup above the breakup length. The calculated results were also compared with the experiments in terms of spray tip penetration and SMD distribution. The results provide the process of spray development, axial and radial distribution of SMD, and calculated overall SMD as a function of time after start of injection.

• 한국연소학회:학술대회논문집
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• 2001.06a
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• pp.119-126
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• 2001

The effects of injection pressure and the distance between injectors on the droplet distribution characteristics of liquid spray for dual orifice type swirl injectors were experimentally investigated. The SMD distributions, volume concentration and Rosin- Rammler variation N of liquid spray droplets for water and a fuel were measured by using the laser diffraction particle sizer. The results of present study show that SMD decreases and spray angle increases as the injection pressure increases. The interaction of sprays from two injectors gives more uniform SMD distribution in the radial direction. As the distance between two injectors increases, SMD that is measured in the interacting region increases. The effect of viscosity on the droplet distribution in the interacting region is greater than the that of surface tension of liquid.

• Journal of the Korean Applied Science and Technology
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• v.23 no.1
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• pp.1-11
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• 2006

The W/O emulsion was formed by mixing hydrophobic nonion surfactants of span 80 and tween 60 with kerosine, and by adding sodium silicate aqueous solution. Precipitating the W/O emulsion by sodium bicarbonate resulted in spherical silica particles. Shape and size distribution of silica particles were observed. The particles were spherical and they have narrow size distribution. Particle sizes were 9.29, 7.39 and $5.73\;{\mu}m$ at homogenizer speed of 2500, 3000, and 3500 rpm, respectively. The particle size was decreased by increasing agitation speed due to the formation of emulsion droplet. At fixed agitation speed, absorbed paraffin oil weight were measured and the $SiO_2/Na_2O$ mole ratio effects on particle size were investigated. Particle size was decreased by increasing the mole ratio of $SiO_2/Na_2O$.