• Journal of the Korean Wood Science and Technology
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• 제23권2호
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• pp.26-31
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• 1995

Acetylcellulose(AC) was prepared with steam exploded wood(EXW) and EXW after delignification with sodium chlorite, pine (Pinus densiflora) and oak (Quercus mongolica) woods. The color of acetylated pine and oak exploded wood was brown, degree of substitution(D.S) of pine was 1.47~2.09, and this of oak was 1.49~2.29. The hemicellulose content of acetylated pine and oak exploded wood was 0~3.4% and 1.49~11.3%, individually. The degree of substitution of acetylated wood prepared from delignified EXW in the pine and oak wood was 0.50~0.71 and 0.70~0.88, individually. Hemicellulose content of acetylated EXW with sodium chlorite after delignification in the pine and oak wood was less than 1% and 0.6~2.5%. The color of acetylated wood after delignification was white. IR-spectra of acetylated pine and oak EXW after delignification were found that peaks at around 1740$cm^{-1}$ and 1200$cm^{-1}$ increase markedly, due to ester carbonyl group.

• Journal of the Korean Wood Science and Technology
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• 제22권2호
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• pp.30-36
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• 1994

Steam explosion process is one of the most efficient, pretreatment method for the utilization of lignocellulosic biomass. The carbxymethyl-cellulose(CMC) was prepared with steam exploded wood(EXW), pine(Pinus densiflora) and oak(Quercus mongolica), by standard method using isopropyl alcohol and monochloroacetic acid. The range of water solubility of carboxymethylated pine exploded wood was 45.2~66.8 % and those of oak was 60.7~84.7 %. The degree of substitution(D.S) of carboxymethylated pine exploded wood was 0.11~0.33 and oak exploded wood was 0.48~0.76. The color of carboxymethylated pine and oak exploded wood was brown-black. When carboxymethylated EXW was purified by sulfuric acid, the yield of carboxymethylated wood was lower than non-treated one. However, the color was still brown-black although after delignification. In carboxymethylated EXM prepared after delignification, the water solubility and degree of substitution(D.S) of pine were 81.4~95.9 % and 0.71~0.79, and those of oak were 76.2~89.5 % and 0.79~1.05. The values were higher than non-treated. The degree of substitution of purified carboxymethylated wood prepared with delignified EXM, pine and oak were 0.50~0.71 and 0.70~0.88. The color of carboxymethylated wood was white. In carboxymethylated wood preparde after delignification of EXM, swelling ratio and water retention value of pine were 95.9~96.5 and 580.0~751.2, those of oak were 76.2~89.5 and 124.3~307.6.

• 한국펄프종이공학회:학술대회논문집
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• 한국펄프종이공학회 2008년도 춘계학술대회
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• pp.222-228
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• 2008

The chemical composition and thermal, crystal characterization of oak mushroom waste were investigated in comparison with those normal oak wood for utilization of cellulose from oak mushroom waste. The oak mushroom waste contained a higher percentage of ash, and hot water extractives than oak wood. This results indicated that the materials inside the body are easily decomposed during the oak mushroom cultivation. The lower percentage of holocellulose and a-cellulose of oak mushroom waste caused by fungal decomposition too. Whereas, the thermal decomposition behavior and crystallinity of oak mushroom waste was similar to that of normal oak wood, which indicated that the cellulose characterization of oak mushroom waste is resistant to fungal decomposition. In additionally, a degree of polymerization of oak mushroom waste must be investigate for examination of cellulose crystalline characterization, especially.

• Journal of the Korean Wood Science and Technology
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• 제36권1호
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• pp.54-60
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• 2008

버섯종균에 의해 열화된 신갈나무 버섯폐골목의 흡음성능과 구조적 특징의 변화를 관찰하고자 버섯폐골목을 원반형으로 채취하여 무처리 목재와 구조적 특징의 변화를 비교하고, 전달함수법을 이용하여 흡음률을 측정 비교하였다. 측정주파수범위에서 버섯폐골목의 시험편이 보통의 시험편보다 높은 흡음률을 나타내었으며, 특히 2~6 KHz의 주파수영역에서는 보통 목재보다 2~3배 정도 높은 흡음률을 나타내었다. 버섯폐골목은 무 처리 목재보다 중량이 70% 정도 감소하였으며, 3단면에서 다수의 공극이 관찰되어 이들이 흡음공극으로 작용하여 측정주파수영역에서 흡음률이 증가된 것으로 사료된다.

• 한국축산식품학회지
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• 제18권1호
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• pp.42-49
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• 1998

The contents of holocellulose, one of the main components of the wood, were 83.9% in oak wood and 76.9% in apple wood, respectively. Those of hemicellulose were 16.41 and 20.33%, and in lignin 23.0 and 19.7%, respectively. Six species of domestic oak wood and apple wood were considered to be suitable for smoking materials due to the low content of lignin. Benzo(a)pyrene contents in smoke flavoring prepared with oak wood at 150, 400 and 500$^{\circ}C$ were 0. 4, 3. 7 and 5.6$\mu\textrm{g}$,/kg, respectively. The amounts of phenanthrene were 112.7, 131.4 and 255.9$\mu\textrm{g}$/kg, respectively, in each temperature. The amounts of polycyclic aromatic hydrocarbons(PAH) in smoke flavory were in the order of phenanthrene＞anthracene＞pyrene＞benzo(a)anthracene＞chrysene＞benzo(b)fluoranthens＞benzo(a)pyrene Benzo(a)pyrene contents in smoking extracts prepared with apple wood at 150, 400 and 500$^{\circ}C$ were 0.4, 3.3 and 5.5$\mu\textrm{g}$/kg, respectively. Phenanthrene contents in those samples were 72.7, 100.2 and 220.5$\mu\textrm{g}$/kg, respectively. Contents of each PAH showed the same order as in oak wood.

• Journal of the Korean Wood Science and Technology
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• 제45권6호
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• pp.809-827
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• 2017

Steam explosion was applied to extract phenolic compounds from oak wood (Quercus mongolica). The effects of three independent factors (ethanol concentration, extraction temperature and extraction time) on the total phenolic content, DPPH radical scavenging activity, and antimicrobial activity from the steam exploded oak wood were optimized using response surface methodology (RSM). The independent variables were coded at three levels and their actual values were selected on the basis of preliminary experimental results. The following optimal extraction conditions were selected: ethanol concentration 82.0%, extraction temperature $71.7^{\circ}C$, and extraction time 60.5 min for total phenolic content; ethanol concentration 78.3%, extraction temperature $70.3^{\circ}C$, and extraction time 57.6 min for DPPH radical scavenging activity; ethanol concentration 80.6%, extraction temperature $68.4^{\circ}C$, and extraction time 59.0 min for antimicrobial activity. The experimental values agreed with those were predicted within confidence intervals indicating the suitability of RSM in optimizing the ethanol extraction of phenolic compounds from the steam exploded oak wood. Under the optimized conditions, the experimental value of the total phenolic content was 111.8 mg GAE/g dry steam exploded oak wood, DPPH free radical scavenging activity was 65.7%, and antimicrobial activity was 17.0 mm, and those are reasonably close to the predicted values (109.2 mg GAE/g dry steam exploded oak wood, 62.3% and 15.9 mm, respectively).

• Journal of the Korean Wood Science and Technology
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• 제32권6호
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• pp.57-66
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• 2004

To study the efficient usage of small diameter logs and woods containing defects such as knots, slope of the grain and decay, six types of finger-jointed woods with various finger profiles were made of poplar, pine and oak with different density. We investigated the effect of finger profile on static bending strength performances of finger-jointed woods. The efficiency of bending MOE, MOR and deflection showed the highest value in poplar finger-jointed wood with the lowest density of three species, and the lowest value in oak finger-jointed wood with the highest density of three species. The values markedly decreased with increasing finger pitch for finger-jointed wood glued with polyvinyl acetate (PVAc) resin for all tested species, whereas for the finger-jointed wood glued with resorcinol-phenol formaldehyde (RPF) resin, the influence of finger pitch on the efficiency of MOE was not found in all tested species, and those on the efficiency of MOR and deflection indicated the same trend as finger-jointed wood glued with PVAc resin in the case of pine and oak finger-jointed wood with higher densities. It was found that the values tended to decrease with increasing density of species on the whole and the desirable finger pitches were L (6.8 mm) for poplar, M (4.4 mm) for pine and S (3.5 mm) for oak in a view of economy. For finger-jointed wood glued with PVAc resin, the fitness between a tip and a root width of a pair of fingers δ of 0.5 mm indicated the highest efficiency of MOE for all species. And, the influence of δ on MOR was only found in oak finger-jointed wood glued with RPF resin and the desirable δ value for oak was 0.1 mm. However, it was found that the influence of δ on the strength performance was very small.

• Journal of the Korean Wood Science and Technology
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• 제42권6호
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• pp.691-699
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• 2014

용융점이 $138^{\circ}C$인 Bi-Sn 혼합합금 주입방법을 이용한 용융합금주입목재복합체의 제조를 통해 목재의 단점인 치수 안정성과 내구성의 개선을 하고자 3가지 주요 침 활엽수 수종의 수종별 최적주입조건을 구명하고, 주입에 따른 금속주입목재복합체의 중량증가율, 열전도도, 전기저항 등의 물리적 성질과 기계적 성질을 실험하여 다음과 같은 결과를 얻었다. 1. 금속주입목재의 최적처리 조건은 $185^{\circ}C$, 진공시간 10분 조건하에서 radiata pine의 경우 $10kgf/cm^2$ 가압시간 2분 30초, red oak는 $30kgf/cm^2$, 가압시간 10분, white oak는 $50kgf/cm^2$, 가압시간 10분에서 최적의 주입조건을 나타냈다. 2. 금속주입목재복합체의 외관적 특징은 전체적으로 재색은 회백색을 나타냈으며, 목재의 무늬를 그대로 유지하고 있다. 3. 침엽수 수종인 radiata pine은 저온용융합금주입처리로 인해 중량증가율은 12배, 밀도는 $6.13g/cm^3$으로 15배나 증가하였으나, 인테리어용으로 주로 사용되는 red oak와 white oak 등의 활엽수의 경우 목재해부학적 특성으로 의해 radiata pine보다는 낮은 5~6배의 밀도증가율을 나타냈다. 4. 주입된 목재는 침 활엽수 모두 금속주입으로 인해 수분흡수율과 두께팽윤율이 현저히 감소하였고, 매우 높은 치수 안정성을 나타냈으며, 금속주입목재복합체의 휨강도, 휨영계수, 경도 및 전기전도도와 열전도도 등도 무처리목재보다 매우 크게 향상되었다.

• Journal of the Korean Wood Science and Technology
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• 제48권6호
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• pp.820-831
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• 2020

참나무시들음병 고사목으로부터 피해확산을 막기위해 주로 훈증처리 방법을 이용한다. 훈증처리에 따른 신갈나무 피해목의 강도적 활용 가능성을 검증하기 위해 훈증처리목재의 압축성능과 휨성능평가를 수행하였다. 훈증처리목재는 약 9개월 간 네마섹트(Metam-sodium)로 훈증처리하였다. 참나무시들음병 훈증처리목재의 기건 종압축강도는 58.87 MPa, 압축탄성계수는 5.66 GPa로 측정되었으며 건전목과 비슷한 경향을 보였다. 혼증목의 성숙재부 강도성능은 미성숙재부보다 16% 더 높은 강도값을 보였다. 참나무 건전목의 압축파괴형상은 다양한 형상으로 나타나지만 훈증처리목재의 경우 대부분 전단형 파괴형상을 보였다. 훈증처리목재의 휨강도는 157.43 MPa로 건전재보다 8% 높게 측정되었고 휨 탄성계수는 16.38 GPa로 건전재보다 16% 낮게 측정되었다. 그러나 훈증처리목재의 휨강도성능치에 대한 변동계수는 건전목보다 낮은 것을 확인하였다.

• Journal of the Korean Wood Science and Technology
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• 제46권2호
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• pp.178-188
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• 2018

The aim of this study was to assess the in vitro potential of water extract from torrefied oak wood as a natural antioxidant. The antioxidant potential of the extracts was assessed by employing different in vitro assays, including reducing power, DPPH (2,2-diphenyl-1-picrylhydrazyl), ABTS [2,2'-azino-bis(3-ethylbenzothiazoline-6-sulphonic acid)], and FRAP (ferric reducing antioxidant potential) assays. The DPPH activity of the extract was increased in a dose-dependent manner. Measurement of total flavonoid content of water extract from torrefied oak wood was achieved using an aluminum chloride colorimetric assay; the extract contained 192.12 mg/g flavonoid, which was significantly high when compared with standard quercetin. The results obtained in this study indicate that water extract from torrefied oak wood has significant potential for use as a natural antioxidant agent.