• Nuclear Engineering and Technology
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• v.27 no.2
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• pp.234-247
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• 1995

Trace elements in airborne particulates were analyzed by instrumental neutron activation analysis (INAA) under the optimum analytical condition. Neutron irradiation for sample was done at the irradiation hole(neutron flux 1$\times$10$^{13}$ n/$\textrm{cm}^2$.s) of TRIGA MARK-III research reactor in the Korea Atomic Energy Research Institute. For the verification of the analytical method, NIST SRM-1648 and NIES CRM No.8 ore chosen and analyzed. The accuracy and precision of the analysis of 40 and 24 trace elements in the samples were compared with the certified and reported values, respectively. The analytical method was found to be reliable enough when the analytical data of NIES sample were compared with those of different counties. In the analytical result of two or both of standard reference materials, relative standard deviation wes within the 15％ except a few elements and the relative error was within the 10％. We used this method to analyze 30 trace elements in airborne particulates collected with the high volume air sampler(PM-10) at too different locations and also confirmed the possibility to use this method as a routine monitoring tool to find out environmental pollution sources.

• Bulletin of the Korean Chemical Society
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• v.7 no.5
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• pp.347-353
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• 1986

Fisher's discriminant method has been applied to the problem of the classification of Korean potsherds, using their elemental composition as analyzed by neutron activation analysis. A combination of analytical data by means of statistical linear discriminant analysis has resulted in removal of redundant variables, optimal linear combination of meaningful variables and formulation of classification rules.

• Journal of Nutrition and Health
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• v.31 no.2
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• pp.213-219
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• 1998

This study was conducted to compare and evaluate the iodide specific ion electrode method (ISE) and neutron activation analysis method (NAA) for determining iodine in human milk and cow milk. The neutron irradiation and counting operations were carried out at the TRIGA Mark-III reactor facility of the Korea Atomic Energy Research Institute. The mean concentrations of iodine in human milk samples by the ISE and the NAA were 1450$\mu\textrm{g}$/L and 1350$\mu\textrm{g}$/L, respectively. The levels were not significantly different. In cow milk samples , the mean concentrations of iodine by the ISE and the NAA were 250$\mu\textrm{g}$.L and 200$\mu\textrm{g}$/L, respectively. here, the ISE reading was significantly higher than the NAA. reading. The correlations of the two methods were 0.92(p<0.001) for human milk samples and 0.65 for cow milk samples . The coefficient of variation was 8.3% in the ISE and 4.9% in the NAA. Therefore, the iodide specific ion electrode method is sample and fast method, but probably not in processed milk since free sulfhydryl groups in milk are also detected by the iodide electrode. However, these also indicate that the ISE method may be applicable to human milk and pasteurized milk if the conventional pasteurization time-temperature relationship of standards is not exceeded. On the other hand, the NAA method , which is independent of chemical forms and matrix, can be used for determining iodine in all kinds of milk and foods.

• Journal of the Korean Society of Radiology
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• v.13 no.1
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• pp.45-53
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• 2019

This study is a neutron activation for concrete that shields medical linear accelerator facilities. Comparison of general concrete and low activation concrete. The simulation method was simulated using MCNPX (Ver. 2.5.0) and FISPACT-2010, and the shielding ability for photon and neutron beams was calculated and neutron activation evaluation was carried out. As a result, the shielding capacity was 20 ~ 50 cm efficient in general concrete, and activate evaluation in low activation concrete was calculated to be low in radioactivity concrete, but all were estimated to not exceed their own allowable concentration in self - disposal. As a result of the comprehensive analysis, it is considered effective to use ordinary concrete.

• Advances in Energy Research
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• v.3 no.2
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• pp.125-131
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• 2015

Prompt neutron lifetime calculations have been performed for the NIRR-1 reactor HEU and LEU cores using the 1/v insertion and the Adjoint flux weighing methods. Results of calculations obtained for the HEU and LEU cores are respectively $57.3{\pm}0.8$ and $47.5{\pm}0.7$ for the 1/v insertion and $56.9{\pm}0.3$ and $46.3{\pm}0.5$ for the Adjoint flux. There is a good agreement seen between the two methods for both cores. The prompt neutron lifetime was observed to be shorter in the LEU than for the HEU as expected. However, the Adjoint flux weighing method seemed to be the easiest method in calculating the prompt neutron lifetime for NIRR-1.

• Bulletin of the Korean Chemical Society
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• v.10 no.1
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• pp.30-32
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• 1989

Traces of nine elements, gold, arsenic, cobalt, chromium, copper, europium, hafnium, sodium and antimony in commercially available silicon crystals were determined by the instrumental neutron activation analysis using the single comparator method. The values of the concentrations of these elements in both single and polycrystals were found to decrease significantly to a low limiting level by simply washing and etching surface contaminants having been introduced during various steps of sample preparation and irradiation. However, the chromium levels in polycrystals were not easily decreased, these depending upon the cutting tools employed. The Sb-doped content in each semiconductor has been compared with the associated quantities such as the concentration and the conductivity range given by the sample donor. Uncertainty in the sodium analysis due to the fission neutron reaction by silicon itself was discussed.

• Analytical Science and Technology
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• v.14 no.4
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• pp.1075-1081
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• 2001

Instrumental Neutron Activation Analysis as a representative method of nuclear analytical technique, has advantages of non-destructive, simultaneous multi-element analysis with the characteristics of absolute measurement method. Up to date, $k_0$-quantitative method which is accurate, convenient and user-friendly, has been generalized world-widely. In this study, it is intented to introduce the general concept of $k_0$-method and to measure $k_0$-parameters for the future implementation to our NAA system. For this objectives, the definition of relevant factors for the quantitative analysis and the equation for the experimental determination of parameters such as $Q_0$(${\alpha}$) and f were summarized. Furthermore, a foundation for the $k_0$-standardization method was prepared through the measurement of ${\alpha}$ and f-value which depend on the specific character of irradiation hole at NAA#1-hole of HANARO research reactor.

• Analytical Science and Technology
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• v.7 no.3
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• pp.293-299
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• 1994

Fifty ancient Korean coins originated in Choson period have been determined for 11 elements such as Sn, Fe, As, Au, Co, Sb, Ir, Os, Ru and Ni by destructive and non-destructive neutron activation analysis as well as for 3 elements such as Cu, Pb and Zn by atomic absorption spectroscopy. The multivariate data have been analyzed by principal component mapping method. The spread of sample points in the eigenvector polt has been attributed to common origins of some elements.

• The Korean Journal of Nuclear Medicine
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• v.27 no.1
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• pp.104-111
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• 1993

Trace elements are important components in the biological system, as a structural material and metabolic controller. Neutron activation analysis (NAA) with high neutron flux and high energy resolution Ge (Li) detector coupled to multichannel analyzer (MCA) has been one of the most accurate method for the determination of ultra-trace level components, and is applicable to biological material. In human body, the NAA can be used for quantitation of trace elements in various organs and tissue with endocrinological and metabolic disease and industrial metal poisoning. In this study, Triga Mark III nuclear reactor in Korea Atomic Research Institute was used for quantitation of trace eleement in human lung cancer tissues by neutron activation analysis. In the squamous cell carcinoma tissues, Br, Hg, La, Sb, Sc, Cl, Fe and I content were lower than normal lung tissues, and K, Rb and Se content were higher. In the adenocarcinoma tissues, Fe, Au, La, Sc and Zn content were lower than normal lung tissues, and Rb, Co and Se content were higher. Rb content was higher in the adenocarcinoma tissues than in the squamous cell carcinoma tissues. Fe and Na content were higher in the squamous cell carcinoma tissues than in the adenocarcinoma tissues.

• Nuclear Engineering and Technology
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• v.56 no.4
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• pp.1330-1338
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• 2024

Information on isotopic composition and geometric structure is necessary for identifying a true warhead. Nevertheless, such classified information should be protected physically or electronically. With a novel Hash encryption algorithm, this paper presents a Monte Carlo-based design of a neutron activation analysis verification module. The verification module employs a thermal neutron source, a non-uniform mask (physically encrypting information about isotopic composition and geometric structure), a gamma detector array, and a Hash encryption algorithm (for electronic encryption). In the physical field, a non-uniform mask is designed to distort the characteristic gamma rays emitted by the inspected item. Furthermore, as part of the Hash algorithm, a key is introduced to encrypt the data and improve the system resolution through electronic design. In order to quantify the difference between items, Hamming distance is used, which allows data encryption and analysis simultaneously. Simulated inspections of simple objects are used to quantify system performance. It is demonstrated that the method retains superior resolution even with 1% noise level. And the performances of anti-statistical attack and anti-brute force cracking are evaluated and found to be very excellent. The verification method lays a solid foundation for nuclear disarmament verification in the upcoming era.