• 한국세라믹학회지
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• 제42권9호
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• pp.607-612
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• 2005

The effect of MgO diluents in combustion synthesis of $TiB_2$ nano particles was investigated. The reaction $TiO_2\;+\;B_2O_3\;+\;xMg\;{\rightarrow}\;TiB_2\;+\;5MgO$ was used to synthesize $TiB_2$ nano particles. The combustion velocity was measured to examine the relation between the reaction temperature and the morphologies of particles. The diluent MgO did not react with the reactants and played a role to decrease combustion temperature. As the MgO diluents contents increased, the particles with the smaller size and the narrower size distribution were synthesized. At the condition of 6 mole of MgO, the combustion wave velocity was about 5 cm/see and the synthesized particles showed the size of 60 nm with narrow size distribution.

• 산업기술연구
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• 제3권
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• pp.47-51
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• 1983

The fragmentation of Mg and Mg-25(w/o) Al alloy particles in hydriding-dehydriding was studied. The formation of hydride was made in autoclave, and formed hydrides were $MgH_2$ in both pure Mg and Mg-25(w/o) Al alloy particles. Pure Mg was more fractured than Mg-25(w/o) Al alloy in hydriding. The addition of Al exhibited fragmentation in hydriding, but displayed the same fragmentation as Mg in dehydriding.

• Progress in Superconductivity
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• 제3권2호
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• pp.188-192
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• 2002

To introduce flux pinning center in HTS-BSCCO system, nano-size MgO particles were uniformly distributed within the Bi-2223 grain by partial hydration of MgO. The existing method MgO doped Bi-2223 used nato-size MgO powders, which resulted in agglomeration during mixing or grain growth during heat-treatment due to the high surface energy of the fine particles. By hydration of the MgO surface, the agglomeration of the MgO powders was avoided and the size of remaining MgO core was controlled by changing hydration medium and time. The thin film obtained by spin coating of (Bi_$1.8/Pb_{0.4}$)$Sr_2$$_{Ca}$$2.2/Cu_3$ $O_{y}$ nitrate solution mixed with hydrated MgO showed the even distribution of nano-size MgO particles in the Bi-2212 grains.s.s.

• 한국주조공학회지
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• 제15권6호
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• pp.588-595
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• 1995

SiC particles reinforced Mg-Zr, Mg-Zn and Mg-Zn-Zr composites were manufactured by Rheocompocasting method. Effects of Zn, Zr addition on microstructures and hardness were investigated by using the micro Vickers hardness tester, the optical and scanning electron microscopy. By the Zr addition to the pureMg/SiCp composites, SiC particles become more homogeneously dispersed and grain refined so that the micro hardness of the composite increased. In case of Zn addition, although grain refinement and homogeneous dispersion effects of SiC particles were not obtained, hardness was more increased than the only Zr added composite by the formation of many Mg-Zn intermetallic compounds at grain boundary. In the Mg-Zn-Zr/SiCp composite, the highest value of hardness was obtained by triple effects such as grain refining, dispersion hardening of SiC particles and Mg-Zn compounds.

• 공업화학
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• 제25권4호
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• pp.374-379
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• 2014

기록물 보존을 위한 탈산처리 완료 후 탈산제 성분인 MgO 입자가 기록물 표면에 미세 입자 형태로 남아있는 일명 백화현상이 나타나고 있다. 이 MgO 미세입자에 의한 백화현상은 MgO 입자가 분산되어 종이의 섬유질에 흡착함으로써 탈산효과를 나타내야 하나, MgO 입자의 농도와 입자크기가 적합하지 않을 경우 분산이 잘 이루어지지 않아 종이표면에 과량 흡착됨으로써 흰색인 MgO 미세입자로 입혀지는 현상이다. 이는 작업환경의 저해를 가져오고 또한 탈산처리 시 작업자 건강에 대한 우려가 증대되고 있으나, 이에 대한 원인 규명 및 대책은 없는 상황이다. 따라서 백화현상의 원인 규명 및 향후 대책을 수립하기 위하여 국내외에서 널리 사용되는 탈산제의 물성분석과 탈산제의 주요성분인 MgO 입자 크기 및 함량 변화에 따른 탈산 실험을 수행하였다. 탈산 실험은 산성지와 백상지를 사용하였으며, 탈산처리 후 SEM 기기분석으로 MgO 입자의 산성지 및 백상지의 지류 표면 흡착정도를 비교하였다. 실험결과 MgO 입자크기가 847 nm 크기로 유지되는 경우 실험한 두 종류의 지류 모두에서 백화현상이 현저하게 감소되는 것을 확인하였으며, MgO 입자크기가 백화현상의 주요 원인이다.

• 한국가금학회지
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• 제20권1호
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• pp.11-15
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• 1993

Environmental measurements were made in 10 broiler confinement houses in order to characterize dust contaminants. Particles were collected by filters on nine stages Anderson Air Sampler, The obtained results were summarized as follows ; 1. The concentrations of the total suspended particles(TSP) were 7.584 mg/$m_3$~11.589mg/$m_3$ in 10 day old broiler houses and 15.836 mg/$m_3$~22.471 mg/$m_3$ in 30 day old broiler houses. 2. The concentrations of the coarse particles were 4.974 mg/$m_3$~18.981 mg/$m_3$ in 10 broiler confinement houses. Therefore, it was found that the coarse particles contributed to TSP between 65.6% and 85.0%. 3. The dust levels were higher in 30 day old broiler houses with TSP averaging about 19.341 mg/$m_3$ than 9.491 mg/$m_3$ in 10 day old broiler houses. In view of the above results , It was concluded that domestic broiler houses need artificial ventilation system.

• Progress in Superconductivity
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• 제5권2호
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• pp.109-113
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• 2004

MgB$_2$ and FeTi composites was prepared to study the effect of FeTi particles on superconductivity of MgB$_2$. The sample, which had contained magnesium, boron and FeTi particles, was synthesized by the Commercial Stainless Steel Tube Enveloping Technique(COSSET) at 92$0^{\circ}C$ for 2 hours. The structure and properties of the sample was investigated by XRD, SEM, and SQUID magnetometer. It was found that there was a little change of T$_{c}$ compared with pure MgB$_2$ superconductor in spite of high percentage of FeTi particles, and there was no proof of structure change of MgB$_2$ superconductor due to FeTi particles. But the high porosity which was appeared in the pure MgB$_2$ was disappeared in the composites. We conclude that FeTi particles do not influence the superconductivity of MgB$_2$ and it is expected that fe-Ti material system will be a good material for a tube of the PIT process and for a substrate of the film.m.

• 한국주조공학회지
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• 제16권6호
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• pp.556-564
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• 1996

Variation of shape and size of solid particles and solute redistribution in Mg-9wt.%Al, AI-4.5wt.% Cu, and AI-7wt.%Si alloys were investigated when they were heated to semi-solid temperatures and held without stirring. In the case of Mg-9wt.% Al and Al-4.5wt.%Cu alloys, the polygonal shaped solid particles were agglomerated with non-uniform distribution, and there were no disappearance of the solid/solid boundary until the end of melting. But in the case of an Al-7wt.%Si alloys, two or three spherical shaped particles were coalesced or separated individually, and the coalesced particles had no solid/solid interface on the contrary to the prevous case. The maximum size of solid particles during isothermal heating at high temperature was smaller than that at lower temperature, but the time required to reach the maximum size at high temperature was shorter than that at lower temperature. The concentrations of main solute atom whose distribution coefficient is lower than 1, decreased in the primary solid particles as the liquid fraction increased, and the gradient of solute concentration was steeper in Mg-9wt.%Al alloy and Al-4.5wt.%Cu alloy than that of Al-7wt.%Si alloy.

• 청정기술
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• 제27권1호
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• pp.39-46
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• 2021

4 HP, 80 LPM 급 초미세기포수 발생장치를 탑재한 도로 구조물 세척차량을 이용하여 도시 내 아파트 단지 주변 차량 통행이 많은 터널 내 콘크리트 표면과 타일 벽면을 세척하였다. 초미세기포 생성은 대기 중 공기를 2 ~ 3 LPM 으로 기액혼합 자흡펌프로 가압된 공기를 임펠러 회전력을 이용하여 마이크로 크기의 미세기포(fine-bubble)를 생성한다. 생성된 기포를 다단충돌판과 회전 노즐을 통과하면서 평균 직경 크기는 164.5 nm, 6.81 × 107 particles mL-1의 초미세기포(ultrafine bubble)를 생산하였다. 생산된 초미세기포를 함유한 세척수는 압력 150 bar, 토출량 30 LPM 으로 도로 구조물 표면에 흡착된 분진을 고압세척 분사하여 제거하였다. 분석실험은 세척 전과 후로 구분하여 표면에 흡착한 분진을 ISO 8502-3의 표면 오염 측정방법을 적용하였으며, 테이프 흡착으로 분진 입자를 채취하였다. 수집된 테이프는 중량법과 소프트웨어 ImageJ를 적용하여 분진의 무게와 입자 개수에 대한 제거율을 산정하였다. 실험 결과, 타일 벽면 표면에 흡착된 분진 입자 개수는 세척 전과 후로 각각 3,063 ± 218 particles mL-1, 20 ± 5 particles mL-1, 중량은 580 ± 82 mg, 13 ± 4 mg 으로 나타났다. 콘크리트 구조물 표면에서의 입자개수는 세척 전과 후로 각각 8,105 ± 1,738 particles mL-1, 39 ± 6 particles mL-1이었으며, 중량은 1,448 ± 190 mg, 118 ± 32 mg으로 나타났다.

• 열처리공학회지
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• 제26권4호
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• pp.185-190
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• 2013

Influence of solution treatment (T4) and peak-aging (T6) on damping capacity was investigated in permanent-mold cast Mg-3%Nd alloy. In as-cast state, the microstructure was characterized by eutectic $Mg_{12}Nd$ intermetallic phase network in the intergranular region. T4 treatment resulted in a dissolution of the eutectic particles, but small amount of the particles still remained in the microstructure. After T6 treatment, nano-sized ${\beta}^{\prime}(Mg_{12}Nd)$ particles were precipitated within the matrix. T4 microstructure showed higher damping capacity than as-cast and T6 ones. In view of the microstructural features, this may well be associated with the dissolution of second-phase particles which play a role in pinning the dislocations acting as a damping source.