• 마이크로전자및패키징학회지
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• 제26권2호
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• pp.23-29
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• 2019

Thermally expandable microsphere and aerogel composite was prepared by chemical compositization. Microsphere can produce synergies with aerogel, especially an enhancement of mechanical property. Through condensation between sulfonated microsphere and hydrolyzed silica sol, chemically-connected composite aerogel could be prepared. The presence of hydroxyl group on the sulfonated microsphere was observed, which was the prime functional group of reaction with hydrolyzed silica sol. Silica aerogel-coated microsphere was confirmed through microstructure analysis. The presence of silicon-carbon absorption band and peaks from composite aerogel was observed, which proved the chemical bonding between them. A relatively low thermal conductivity value of $0.063W/m{\cdot}K$ was obtained.

• 한국염색가공학회지
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• 제27권1호
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• pp.11-17
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• 2015

Recently, super fiber reinforced composite materials are widely used in many industries due to high mechanical properties. In this study, 2 different types of composite materials were manufactured in order to compare their mechanical properties. Carbon and Aramid fibers were used for reinforcement materials and Bisphenol-A type epoxy resin was for matrix. Two kinds of fiber-reinforced materials were manufactured by RIM(Resin Injection Molding) method. Before manufacturing composite materials, the optimal manufacturing and curing process condition were established and the ratio of reinforcement to epoxy resin was discussed. FT-IR analysis was conducted to clarify the structure of epoxy resin. Thermal and mechanical property test were also carried out. The cross-section of composite materials was observed using a scanning electron microscope(SEM).

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2002년도 춘계학술대회 논문집 초전도 자성체
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• pp.17-20
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• 2002

The effects of relatively low lead content (0.2~0.3) on the 2223 phase formation and transport property of Bi-2223/Ag tapes have been investigated. The results show that lead contents have great impact on the phase assemblage of precursors, subsequently, on the phase formation and transport property of silver sheathed BSCCO-2223 tapes. Powders containing Pb=0.25 and Pb=0.3 resulted in the nearly identical $J_c$ values in fully processed tapes, but leaded to significant difference on the phase formation process. For the case of Pb=0.2, both low conversion fraction of 2212 to 2223 and low $J_c$ value were obtained in final reacted tape, which was probably due to lack of enough liquid phase to facilitate the phase transformation.

• 한국분말재료학회지
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• 제21권1호
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• pp.16-20
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• 2014

In order to fabricate the porous $Al_2O_3$ with dispersion of nano-sized Cu particles, freeze-drying of camphene/$Al_2O_3$ slurry and solution chemistry process using Cu-nitrate are introduced. Camphene slurries with 10 vol% $Al_2O_3$ was frozen at $-25^{\circ}C$. Pores were generated by sublimation of the camphene during drying in air. The sintered samples at 1400 and $1500^{\circ}C$ showed the same size of large pores which were aligned parallel to the sublimable vehicles growth direction. However, the size of fine pores in the internal walls of large pores decreased with increase in sintering temperature. It was shown that Cu particles with the size of 100 nm were homogeneously dispersed on the surfaces of the large pores. Antibacterial test using fungus revealed that the porous $Al_2O_3$/1 vol% Cu composite showed antifungal property due to the dispersion of Cu particles. The results are suggested that the porous composites with required pore characteristics and functional property can be fabricated by freeze-drying process and addition of functional nano particles by chemical method.

• 한국재료학회지
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• 제14권9호
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• pp.659-663
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• 2004

Magnetite was prepared by wet method and oil-based magnetic fluid also was prepared by its magnetite. Ahead of making magnetite, we investigated the variation of physical properties for changing $Fe^{3+}/Fe^{2+}$. Through the variation of the process mixing time, pH, magnetite content, we made magnetic fluid of magnetite. We examined the magnetic and frequency property by a toroidal mold. In result $Fe^{3+}/Fe^{2+}=1.2$, over the minute mixing time property of magnetite, Ms was 61.98 emu/g. Moreover, the B-H loop result indicated that the magnetic fluid followed paramagnetic behavior.

• Applied Microscopy
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• 제45권2호
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• pp.63-73
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• 2015

Shear banding is an evidence of plastic instability that localizes large shear strains in a relatively thin band when a material is plastically deformed. Shear bands have attracted much attention in amorphous metals, because shear bands are the key feature that controls the plastic deformation process. In this article, we review recent advances in understanding of the shear bands in amorphous metals regarding: dislocations versus shear bands, the formation of shear bands, hot versus cold shear bands, and property manipulation by shear band engineering. Although there are many key issues that remain puzzling, the understanding built-up from these approaches will provide a new insight for tailoring shear bands in amorphous metals, which potentially leads to unique property changes as well as improved mechanical properties. Indeed, this effort might open a new era to the future use of amorphous metals as a new menu of engineering materials.

• 한국윤활학회:학술대회논문집
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• 한국윤활학회 2001년도 제34회 추계학술대회 개최
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• pp.59-62
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• 2001

Flow induced vibration in steam generators has caused dynamic interactions between tubes and contacting materials resulting in fretting wear . Series of experiments have been performed to examine the wear properties of Inconel 690 steam generator tubes in various environmental conditions. For the present study, the test rig was designed to examine the fretting wear and rolling wear properties in high temperature(room temperature - 290。C) water. The test was performed at constant applied load and sliding distance to investigate the effect of test temperature on wear properties of the steam generator tube materials. To investigate the wear mechanism of material, the worn was observed using scanning electron microscopy. The weight loss increase at higher test temperature was caused by the decrease of water viscosity and the mechanical property change of tube material. The mechanical property changes of steam generator tube material, such as decrease of hardness or yield stress in the high temperature tests. From the SEM observation of worn surfaces, the severe wear scars were observed in specimens tested at the higher temperature.

• 한국분말재료학회지
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• 제1권2호
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• pp.174-180
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• 1994

Electrical contact property of the W-20wt%Cu contact materials manufactured by liquid phase sintering of nanocomposite W-Cu powders was investigated and discussed in terms of microstructural development during performance test. Nanocomposite powders were prepared by hydrogen reduction of ball milled W-Cu oxide mixture. They underwent complete densification and microstructural homogenization during liquid phase sintering. As a consequence, the W-Cu contacts produced from nanocomposite powders showed superior contact property of lower arc erosion and stable contact resistance. This might be mostly due to the fact that the arc erosion by evaporation of Cu liquid droplets and surface cracking remarkably became weakened. It is concluded that the improvement of anti-arc erosion of the composite specimen is basically attributed to microstructural homogeneity.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 1999년도 춘계학술대회 논문집
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• pp.126-129
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• 1999

Dielectric and piezoelectric properties of perovskite materials such as La modified $Pb(Zr,Ti)O_3$ ceramics and $Pb(Zn_{1/3}Nb_{2/3})O_3-PbTiO_3$ single crystals were investigated for cryogenic capacitor and actuator applications. Enhanced extrinsic contributions resulted in piezoelectric coefficient (d33) as high as 250 pC/N at 30 K, superior to that of PZT ($d_{33}$ ~ 100 pC/N). This cryogenic property enhancement was associated with retuning the MPB (or cryogenic temperatures. PZN-PT single crystals exhibited dramatic property improvements such as $d_{33}$ > 500 pC/N at 30 K as a result of an engineered domain state.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2004년도 춘계학술발표대회 논문집
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• pp.147-150
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• 2004

Graphite reinforced conductive polymer composites were fabricated by the compression molding technique. Graphite powder (conductive filler) was mixed with an epoxy resin to impart electrical property in composites. The ratio of graphite powder was varied to investigate electrical property of cured conductive composites. In this study, graphite filled conductive polymer composites with high filler loadings$(>60wt.\%)$ were manufactured to accomplish high electrical conductivity(> 100S/cm). Graphite powder increase electrical conductivity of composites by direct physical contact between particles. While high filler loadings are needed to attain good electrical property, the composites becomes brittle. So the ratio of filler to epoxy was varied to optimize of cured composites. The optimum molding pressure according to filler was proposed experimentally.