• Title/Summary/Keyword: Low temperature liquid

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Precise Temperature Control by Adjusting Flow of Liquid Nitrogen (액체 질소의 흐름 조절을 통한 저온 정밀 온도 제어)

  • Yang, Inseok;Lee, Jee-Ho
    • Journal of Sensor Science and Technology
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    • v.25 no.1
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    • pp.65-70
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    • 2016
  • We devised a method to control the temperature of a liquid bath as low as $-100^{\circ}C$ using the duty cycle control of a solenoid valve. The solenoid valve controls the flow of liquid nitrogen that we used as a cryogen in this system. By controlling the duty cycle of a solenoid valve using feedback from the measured temperature of the liquid bath, we were able to achieve temperature stability within ${\pm}19mK$ around $-100^{\circ}C$. We also demonstrated that by taking average values of the temperature readings for sequence of measurements from more than one thermometer, it is possible to use this system for the calibration of thermometers within 3 mK. This system and the control method can be used for the precise temperature control in the range between $0^{\circ}C$ and $-100^{\circ}C$, where commercially available precision baths are much expensive and hard to be built in customized configurations.

An Experimental study on the Freezing Phenomena of Saturated Porous Media in a Rectangular Cavity (장방형내 함수 다공성 물질의 동결거동에 관한 실험적 연구)

  • Kim, B.C.;Kim, J.I.;Kim, J.H.
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.3 no.5
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    • pp.386-394
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    • 1991
  • Freezing of saturated porous media contained in a rectangular cavity has been studied experimentally. Water and different diameter glass beads consitituted the liquid and porous media. Solidification front shape, the effects of bead diameter and initial liquid temperature was investigated. When the hot wall temperature was below $4^{\circ}C$, the freezing rate was higher at the top than at the bottom due to the density inversion, but with increasing the hot wall temperature the freezing rate at the top was effected by the liquid temperature and was lower than at the bottom. With increasing the bead diameter, the difference of freezing rate between top and bottom was increased and depends on thermal conductivity. When the liquid temperature was low in the beginning, the freezing rate was high, but with increasing the time almost the same with those of high temperature liquid.

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LIQUID PENETRANT TESTING AT LOW TEMPERATURE (저온에서 행하는 액체침투 탐상방법)

  • Barbier, R.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.3 no.1
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    • pp.26-30
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    • 1983
  • Tests on Liquid Penetrant products normally utilized in the temperature range $10^{\circ}C\;to\;40^{\circ}C$ have shown that the required sensibility can not be obtained at temperatures lower than $10^{\circ}C$ with the penetration and development time usually specified in the operating procedures. It is thus confirmed that $10^{\circ}C$ is the lowest allowable temperature for use of these products. The results obtained with a penetrant and develope. specially formulated for low temperatures (SHERWIN B 305+D100) are satisfactory between $0^{\circ}C\;and\;15^{\circ}C$.

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Effect of Heating Rate and $V_2O_5$ Addition on Densification and Electrical Properties of $Pb(Mn_{1/3}Sb_{2/3})O_3-PZT$ Ceramics for Piezoelectirc Transformer (압전변압기용 $Pb(Mn_{1/3}Sb_{2/3})O_3-PZT$ 세라믹스에서 승온속도 및 $V_2O_5$ 첨가가 치밀화 및 전기적 특성에 미치는 영향)

  • 허수정;손준호;손정호;이준형;김정주;정우환;박명식;조상희
    • Journal of the Korean Ceramic Society
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    • v.37 no.4
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    • pp.295-301
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    • 2000
  • The effect of V2O5 addition on the low temperature sintering of Pb(Mn1/3Sb2/3)O3-PZT ceramics, which is known as a prominent material for piezoelectric transformer application was studied, and the densification behavior and piezoelectric characteristics of the samples as a function of heating rate were also examined. V2O5 led the system to liquid phase sintering by forming liquid phase during sintering, which accelerated densification through the particle rearrangement in the early stage of sintering. The liquid phase mostly existed at grain boundaries retarded the evaporation of PbO, while the densification temperature and the weight loss of V2O5-free samples were higher than those of samples with V2O5. Faster heating improved the densification of the samples regardless of V2O5 addition. The low temperature sintering at 100$0^{\circ}C$ was achieved in PMS-PZT ceramics with high density and reasonable dielectric and piezoelectric characteristics. This result revealed optimistic way to the development of multi-layered piezoelectric transformers.

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A Preliminary Study of Low Temperature Condition by Heat Exchanger (열교환기를 이용한 저온 환경 구축에 대한 기초 연구)

  • Lee, Yang-Suk;Yang, Jae-Joon;Kim, Yoo;Ko, Young-Sung;Lim, Byeung-Jun
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2007.11a
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    • pp.23-26
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    • 2007
  • A preliminary, study of low temperature condition was performed to simulate high altitude condition. The mixed air temperature were investigated at various condition by experiments using cryogenic air by heat exchanger and normal temperature air. An experimental setup was constructed to simulate low temperature condition with liquid nitrogen. To control mass flow rate, orifice and pressure regulators were used. The experimental results show that the mixed air temperature increases linearly with mass flow rate of normal temperature air. Therefore it can be help to simulate a low temperature condition of high altitude.

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Influence of the Inclination Angle and Liquid Charge Ratio on the Condensation in Closed Two-Phase Thermosyphons with Axial Internal Low-Fins

  • Cho, Dong-Hyun;Han, Kyu-il
    • Journal of Mechanical Science and Technology
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    • v.17 no.3
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    • pp.422-428
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    • 2003
  • This study concerns the performance of the heat transfer of the thermosyphons having 60, 70, 80. 90 axial internal low-fins in which boiling and condensation occurr. Water, HCFC-141b and CFC-11 have been used as the working fluids. The operating temperature, the liquid charge ratio and the inclination angle of thermosyphons have been used as the experimental parameters. The heat flux and heat transfer coefficient at the condenser are estimated from experimental results. The experimental results have been assessed and compared with existing theories. As a result of the experimental investigation, it was found that the maximum heat flow rate in the thermosyphons is dependent upon the liquid charge ratio and inclination angle. A relatively high rate of heat transfer has been achieved by the thermosyphon with axial internal low-fins. The inclination of a thermosyphon has a notable influence on the condensation. In addition, the overall heat transfer coefficients and the characteristics at the operating temperature are obtained for the practical applications.

Analysis of cure behavior of low temperature curing liquid silicone rubber (LSR) for multi-material injection molding (이중사출 성형을 위한 저온 경화 액상실리콘고무 (LSR)의 경화 거동 분석)

  • Hyeong-min Yoo
    • Design & Manufacturing
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    • v.17 no.1
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    • pp.1-5
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    • 2023
  • In multi-material injection molding, since two or more materials with different process conditions are used, it is essential to maximize process efficiency by operating the cooling or heating system to a minimum. In this study, Liquid silicone rubber (LSR) that can be cured at a low temperature suitable for the multi-material injection molding was selected and the cure behavior according to the process conditions was analyzed through differential scanning calorimetry (DSC). Dynamic measurement results of DSC with different heating rate were obtained, and through this, the total heat of reaction when the LSR was completely cured was calculated. Isothermal measurement results of DSC were derived for 60 minutes at each temperature from 80 ℃ to 110 ℃ at 10 ℃ intervals, and the final degree of cure at each temperature was calculated based on the total heat of reaction identified from the Dynamic DSC measurement results. As the result, it was found that when the temperature is lowered, the curing start time and the time required for the curing reaction increase, but at a temperature of 90 ℃ or higher, LSR can secure a degree of cure of 80% or more. However, at 80 ℃., it was found that not only had a relatively low degree of curing of about 60%, but also significantly increased the curing start time. In addition, in the case of 110 ℃, the parameters were derived from experimental result using the Kamal kinetic model.

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The Characteristics of Insulation with Temperature Variations of $SF_{6}$ ($SF_{6}$ 가스의 온도변화에 따른 절연특성)

  • 이광식;박광서;박경태;김이국;박창기
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.52 no.8
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    • pp.354-358
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    • 2003
  • In this paper, insulations characteristics by temperature changes(+50~-50[$^{\circ}C$]) of $SF_{6}$ gas in the experimental chamber were studied. From this result, at the low temperature, the breakdown voltage was increased with a drop of temperature and an increase of inner pressure in GIS. In addition the ability of insulation of liquid $SF_{6}$ was higher than that of the highly pressurized $SF_{6}$ gas. That is, with progress of low temperature, the main reason of breakdown was not liquefaction of $SF_{6}$ but rapid decrease of inner pressure. This study will come in greatly handy for the insulation design of GIS in a hard cold region

Low-Temperature Chemical Sintered TiO2 Photoanodes Based on a Binary Liquid Mixture for Flexible Dye-Sensitized Solar Cells

  • Md. Mahbubur, Rahman;Hyeong Cheol, Kang;Kicheon, Yoo;Jae-Joon, Lee
    • Journal of Electrochemical Science and Technology
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    • v.13 no.4
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    • pp.453-461
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    • 2022
  • A chemically sintered and binder-free paste of TiO2 nanoparticles (NPs) was prepared using a binary-liquid mixture of 1-octanol and CCl4. The 1:1 (v/v) complex of CCl4 and 1-octanol easily interacted chemically with the TiO2 NPs and induced the formation of a highly viscous paste. The as-prepared binary-liquid paste (PBL)-based TiO2 film exhibited the complete removal of the binary-liquid and residuals with the subsequent low-temperature sintering (~150℃) and UV-O3 treatment. This facilitated the fabrication of TiO2 photoanodes for flexible dye-sensitized solar cells (f-DSSCs). For comparison purposes, pure 1-octanol-based TiO2 paste (PO) with moderate viscosity was prepared. The PBL-based TiO2 film exhibited strong adhesion and high mechanical stability with the conducting oxide coated glass and plastic substrates compared to the PO-based film. The corresponding low-temperature sintered PBL-based f-DSSC showed a power conversion efficiency (PCE) of 3.5%, while it was 2.0% for PO-based f-DSSC. The PBL-based low- and high-temperature (500℃) sintered glass-based rigid DSSCs exhibited the PCE of 6.0 and 6.3%, respectively, while this value was 7.1% for a 500℃ sintered rigid DSSC based on a commercial (or conventional) paste.

Design, Fabrication and Performance Testing of a High-impulse, Low-Power Microthruster using Liquid Propellant with High Viscous Fluid Plug (저전력소비, 고출력, 연발형 마이크로 분사기의 설계, 제작 및 성능 시험)

  • Kim, Sang-Wook;Kang, Tae-Goo;Cho, Young-Ho
    • Proceedings of the KSME Conference
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    • 2001.06c
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    • pp.59-63
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    • 2001
  • A high-impulse, low-power, continuous-shot microthruster has been developed using low boiling temperature liquid-propellant with high viscous fluid-plug. The viscous friction force of the fluid-plug increases the blast pressure and the low boiling temperature liquid-propellant is intended to reduce input power consumption. The three-layer microthruster has been fabricated by surface micromachining as well as bulk micromachining in the size of $7{\times}13{\times}1.5mm^{3}$. A continuous output impulse bit of $6.4{\times}10^{-8}N{\cdot}sec$ has been obtained from the fabricated microthruster using perfluoro normal hexane (FC72) propellant and oil plug, resulting in about ten times increase of the impulse bit using one hundredth electrical input energy compared to the conventional continuous microthruster.

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