• 제목/요약/키워드: Improved synthesis

검색결과 808건 처리시간 0.035초

자기촉매 특성을 이용한 탄소나노튜브의 연소합성 연구 (Combustion synthesis of carbon nanotubes using their self-catalytic behavior)

  • 우상길;홍영택;권오채
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2008년도 추계학술대회A
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    • pp.1815-1820
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    • 2008
  • Self-catalytic behavior of combustion-synthesized carbon nanotubes (CNTs) is evaluated using a double-faced wall stagnation flow burner with a CNT-deposited stainless steel plate wall. CNT formation is observed using field-emission scanning and transmission electron microscopies and Raman spectroscopy. A self-catalytic behavior of multi-walled CNTs (MWCNTs) shows the enhanced ratio of channel diameter to tube wall thickness and the enhanced intensity ratio of G-band to D-band in Raman spectroscopy, implying that the quality of metal-catalytic, flame-synthesized MWCNTs can be much improved via a CNT self-catalytic flame-synthesis process. Thus, using a DWSF burner through the self-catalytic process has potential in mass production of CNTs having much improved quality.

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부구조물 합성법을 이용한 슬라이딩 모드 해석 (Sliding Mode Analysis Using Substructure Synthesis Method)

  • 김대관;이민수;한재흥;고태환
    • 한국소음진동공학회:학술대회논문집
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    • 한국소음진동공학회 2006년도 춘계학술대회논문집
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    • pp.1366-1371
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    • 2006
  • A structural coupling method is developed for the dynamic analysis of a nonlinear structure with concentrated nonlinear hinge joints or sliding lines. Component mode synthesis method is extended to couple substructures and the nonlinear models. In order to verify the improved coupling method, a numerical plate model consisting of two substructures and torsional springs, is synthesized by using the proposed method and its model parameters are compared with analysis data. Then the coupling method is applied to a three-substructure-model with the nonlinearity of sliding lines between the substructures. The coupled structural model is verified from its dynamic analysis. The analysis results show that the improved coupling method is adequate for the structural nonlinear analyses with the nonlinear hinge and sliding mode condition.

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Improved Manufacturing Process for Pyronaridine Tetraphosphate

  • Lee, Dong Won;Lee, Seung Kyu;Cho, Jun Ho;Yoon, Seung Soo
    • Bulletin of the Korean Chemical Society
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    • 제35권2호
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    • pp.521-524
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    • 2014
  • Pyronaridine tetraphosphate (1) is a well-known antimalarial drug. However, it required a carefully optimized production process for the manufacture of pyronaridine tetraphosphate. Each step of its manufacturing process was reinvestigated. For the cyclization of 4-chloro-2-(6-methoxy-pyridin-3-yl-amino)-benzoic acid 6 to 7,10-dichloro-2-methoxybenzo[b]-1,5-naphthyridine 5, an improved process was developed to eliminated critical process impurity (BIA). By the redesign of the formation of triphosphate salt, the purity as API grade was increased. Thus, a robust manufacturing process with an acceptable process performance has been developed to produce high quality pyronaridine tetraphosphate.

An improved synthesis of 2'-fluoro-2'-deoxyarabinofuranosyl pyrimidine nucleosides

  • Chun, Moon-Woo
    • Archives of Pharmacal Research
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    • 제6권1호
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    • pp.79-81
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    • 1983
  • Several potent anti-herpes virus nucleosides, 2'fluoro-2'-deoxyarabinofuranosyl pyrimidine nucleosides, were prepared in good yields by a new condensation method using sodium iodide and a new solvent system, and FMAU could be also prepared directly from thymine by this method.

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시뮬레이션 효율을 향상시킨 시뮬레이션 기반의 아날로그 셀 합성 (A Simulation-Based Analog Cell Synthesis with Improved Simulation Efficiency)

  • 송병근;곽규달
    • 전자공학회논문지C
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    • 제36C권10호
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    • pp.8-16
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    • 1999
  • 본 연구에서는 시뮬레이션 효율을 향상시킨 시뮬레이션 기반의 아날로그 셀 합성기법을 제안한다. 아날로그 셀을 계층적으로 합성하기 위하여 시뮬레이션 기반으로 전류미러, 차동입력단 등 각각의 부회로(sub circuit) 생성기들을 개발하였다. 이 부회로 생성기들을 모듈화 시키고 계층화시킴으로써 OTA(operational transconductance amplifier)나 2단(2-stage) OP-AMP, 비교기(comparator)등 일반적인 아날로그 셀들의 합성을 위하여 사용될 수 있게 하였다. 시뮬레이션 기반의 합성 시간을 줄이기 위하여 2단계 탐색 기법 (2-stage searching scheme)과 시뮬레이션 데이터 재사용기법(simulation data reusing scheme)을 제안하여 적용하였다 아날로그 셀(OTA) 합성 시 301.05sec에서 56.52sec로 최고 81.2%의 합성 시간을 줄이므로 시뮬레이션 기반의 회로 합성시 긴 합성시간의 문제를 해결하였다. 개발한 합성기는 SPICE의 모델 파라미터외에 추가적인 물리적 파라미터들을 필요로 하지 않으며 공정이나 SPICE 모델 레벨(level)에 독립적이기 때문에 새로운 공정에 적용할 때 필요한 준비 시간이 최소화되었다. 본 논문에서는 OTA와 2단 OP-AMP를 각각 합성하여 제안하는 합성기법의 유용성을 입증하였다.

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A Simple and Clean Synthesis of Polysubstituted 2,6-Dicyanoanilines Catalyzed by KF/alumina

  • Jain, Shubha;Keshwal, Balwant S.;Rajguru, Deepika;Bhagwat, Vasant W.
    • 대한화학회지
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    • 제56권6호
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    • pp.712-715
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    • 2012
  • A simple and clean synthesis of polysubstituted 2,6-dicyanoanilines has been developed via the reaction of arylidenemalonodinitriles with 1-arylethylidenemalonodinitriles in ethanol catalyzed by KF/alumina. Use of non-hazardous solid base as a catalyst, operational simplicity and improved product yields are the key advantages of the present protocol.

선형시스템을 위한 개선된수렴속도를 갖는 기준모델 적응제어기- SYNTHESIS METHOD (Model Reference Adaptive Control for Linear System with Improved Convergence Rate -SIGNAL SYNTHESIS METHOD-)

  • Lim, Kye-Young
    • 대한전기학회논문지
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    • 제37권10호
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    • pp.733-739
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    • 1988
  • Adaptive controllers for linear system whose nominal values of coefficients only are known, that is corrupted by disturbance, are designed by signal synthesis model reference adaptive control (MRAC). This design is stemmed from the Lyapunov direct method. To reduce the model following error and to improve the conrergence rate of the design, an indirect suboptimal control law is de rived using the Hamilton Jacobi Beellman equation. Proper compensaton for the effects of time varying coefficients and plant disturbance are suggested. In the design procedure no complete identification of unknown coefficients are required.

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Thangka Image Inpainting Algorithm Based on Wavelet Transform and Structural Constraints

  • Yao, Fan
    • Journal of Information Processing Systems
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    • 제16권5호
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    • pp.1129-1144
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    • 2020
  • The thangka image inpainting method based on wavelet transform is not ideal for contour curves when the high frequency information is repaired. In order to solve the problem, a new image inpainting algorithm is proposed based on edge structural constraints and wavelet transform coefficients. Firstly, a damaged thangka image is decomposed into low frequency subgraphs and high frequency subgraphs with different resolutions using wavelet transform. Then, the improved fast marching method is used to repair the low frequency subgraphs which represent structural information of the image. At the same time, for the high frequency subgraphs which represent textural information of the image, the extracted and repaired edge contour information is used to constrain structure inpainting in the proposed algorithm. Finally, the texture part is repaired using texture synthesis based on the wavelet coefficient characteristic of each subgraph. In this paper, the improved method is compared with the existing three methods. It is found that the improved method is superior to them in inpainting accuracy, especially in the case of contour curve. The experimental results show that the hierarchical method combined with structural constraints has a good effect on the edge damage of thangka images.

Model based optimal FIR synthesis filter for a nosy filter bank system

  • Lee, Hyun-Beom;Han, Soo-Hee;Kwon, Wook-Hyun
    • 제어로봇시스템학회:학술대회논문집
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    • 제어로봇시스템학회 2003년도 ICCAS
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    • pp.413-418
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    • 2003
  • In this paper, a new multirate optimal finite impulse response (FIR) filter is proposed for the signal reconstruction in the nosy filter bank systems. The multirate optimal FIR filter replaces the conventional synthesis filters and the Kalman synthesis filter. First, the generic linear model is derived from the multirate state space model for an autoregressive (AR)input signal. Second, the multirate optimal FIR filter is derived from the multirate generic linear model using the minimum variance criterion. This paper also provides numerical examples and results. The simulation results illustrate that the performance is improved compared with conventional synthesis filters and the proposed filter has advantages over the Kalman synthesis filter.

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부분구조합성법을 이용한 제직기 구조물의 진도특성에 관한 연구 (A Study on the Vibration Characteristics of Weaving Machine Structure using Component Mode Synthesis)

  • 권상석;김병옥;전두환
    • 한국소음진동공학회:학술대회논문집
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    • 한국소음진동공학회 2001년도 춘계학술대회논문집
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    • pp.535-539
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    • 2001
  • In these days. the finite element method(FEM) is a very common method for not only a simple vibration analysis but also the optimization of structures. Since the finite element model may contain thousands of degree of freedom, the eigensolutions require extreme computing power, which will result in a serious time-consuming problem. Thus, many researchers have challenged to find more improved modeling techniques and calculating methods to overcome such problems. The Guyan reduction method and the substructure synthesis method are typical examples of such methods. Of the substructure synthesis method, the component mode synthesis method (CMS) is widely used for dynamic analysis of structure. In this study. for the efficient analysis of jet loom structure. Component Mode Synthesis was carried out. The results of the finite element program developed are compared with those of the commercial package program ANSYS for the validation of the program. The results obtained by the program showed a good agreement with those of ANSYS. The program will be further refined and verified by test to yield more accurate results.

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