• Bulletin of the Korean Chemical Society
• /
• v.33 no.6
• /
• pp.1967-1971
• /
• 2012

A hexavalent chromium (Cr (VI)) is one of the hazardous substances regulated by the RoHS. The determination of Cr (VI) in various polymers and printed circuit board (PCB) has been very important. In this study, the three different analytical methods were investigated for the determination of a hexavalent chromium in Acrylonitrile Butadiene Styrene copolymer (ABS) and PCB. The results by three analytical methods were obtained and compared. An analytical method by UV-Visible spectrometer has been generally used for the determination of Cr (VI) in a sample, but a hexavalent chromium should complex with diphenylcarbazide for the detection in the method. The complexation did make an adverse effect on the quantitative analysis of Cr (VI) in ABS. The analytical method using diphenylcarbazide was also not applicable to printed circuit board (PCB) because PCB contained lots of irons. The irons interfered with the analysis of hexavalent chromium because those also could complex with diphenylcarbazide. In this study, hexavalent chromiums in PCB have been separated by ion chromatography (IC), then directly and selectively detected by inductively coupled plasma atomic emission spectrometry (ICP-AES). The quantity of Cr (VI) in PCB was 0.1 mg/kg.

• Natural Product Sciences
• /
• v.25 no.2
• /
• pp.122-129
• /
• 2019

The roots of Phlomis umbrosa (Turcz.) (Phlomidis Radix) have been traditionally used to treat cold, reduce swelling and staunch bleeding. Four iridoids (1 - 3 and 5) and six phenylethanoid derivatives (4, and 6 - 10) were isolated from the roots of P. umbrosa. A simple, sensitive, and reliable analytical HPLC/PDA method was developed, validated, and applied to determine 10 marker compounds in Phlomidis Radix. Furthermore, the isolates were evaluated for cytotoxic and anti-oxidant activities as well as DPPH-HPLC method. Among them, compounds 4 and 6 - 9 displayed potent anti-oxidant capacities using DPPH assay with $IC_{50}$ values of $27.7{\pm}2.4$, $10.2{\pm}1.1$, $18.0{\pm}0.8$, $19.1{\pm}0.3$, and $19.9{\pm}0.6{\mu}M$, and compounds 6, 8, and 9 displayed significant cytotoxic activity against HL-60 with $IC_{50}$ values of $35.4{\pm}3.1$, $18.6{\pm}2.0$, and $42.9{\pm}3.0{\mu}M$, respectively.

• Journal of the Institute of Electronics and Information Engineers
• /
• v.52 no.5
• /
• pp.74-82
• /
• 2015

As the complexity of an electronic device and the reduction of its operating voltage is progressing, susceptibility test of the chip and module for internal or external noises is essential. Although the immunity compliance of the chip was served with IEC 62132-4 Direct Power Injection method as an industry standard, in fact, EM immunity of the chip is influenced by their Power Domain Network (PDN). This paper evaluates the EM noise tolerance of a PLL and compares their noise transfer characteristics to the PLL on various PCB boards. To make differences of the PDNs of PCBs, various PCBs with or without LDO and with several types of capacitors are tested. For evaluation of discrepancies between EM characteristics of an IC only and the IC on real boards, the analysis of the noise transfer characteristics according to the PDNs shows that it gives important information for the design having robust EM characteristics. DPI measurement results show that greatly improved immunity of the PLL in the low-frequency region according to using the LDO and a frequency change of the PLL according to the DPI could also check with TEM cell measurement spectrum.

• Journal of the Korean Ceramic Society
• /
• v.42 no.6 s.277
• /
• pp.437-442
• /
• 2005

We fabricated BSCCO-2212 (2212) bulk superconductor by melt casting process, and evaluated the dependence of the critical properties on the temperature and cooling .ate of mold and the pouring methods of melt. It was observed that the critical current (Ic) of 2212 was significantly dependent on the pre-heating temperature of the mold. At the pre-heating temperature of $500^{\circ}C$ followed by air cooling condition, Ic of 48 A at 77 K was obtained which was higher than others processed at different temperatures. In addition, the Ic improved to 132 A when tilt casting method was applied. The improved Ic is probably due to the fact that the tilt casting reduced a turbulent flow of the melt during casting causing less porosity and more homogeneous microsructure. Critical temperature was measured to be 87-89 K after the first heat treatment and it improved to 90-91 K when subsequently heat treated at $650^{\circ}C$ in a nitrogen atmosphere. This improvement was considered to be due to an optimization of the oxygen content in the range of 8.16-8.2.

• Structural Engineering and Mechanics
• /
• v.43 no.6
• /
• pp.823-833
• /
• 2012

An experimental method was suggested for obtaining fracture toughness ($K_{Ic}$) and the tensile strength (${\sigma}_t$) of chopped strand glass fiber reinforced polymer concretes (PC). Semi-circular bend (SCB) specimens subjected to three-point bending were used for conducting the experiments on the PC material. While the edge cracked SCB specimen could be used to evaluate fracture toughness, the tensile strength was obtained from the un-cracked SCB specimen. The experiments showed the practical applicability of both cracked and un-cracked SCB specimens for using as suitable techniques for measuring $K_{Ic}$ and ${\sigma}_t$ in polymer concretes. In comparison with the conventional rectangular bend beam specimen, the suggested SCB samples need significantly less material due to its smaller size. Furthermore, the average values of ${\sigma}_t$ and $K_{Ic}$ of tested PC were approximately 3.5 to 4.5 times the corresponding values obtained for conventional concrete showing the improved strength properties of PC relative to the conventional concretes.

• The Journal of The Korea Institute of Intelligent Transport Systems
• /
• v.18 no.6
• /
• pp.262-274
• /
• 2019

The purpose of this study is to estimate the minimum proportion of probe vehicles for obtaining expressway traffic information using VISSIM, a micro traffic simulation model, between Yongin IC and Yangji IC on Yeongdong Expressway. 7,200 scenarios were created for the experiment, and 40 scenarios were adopted using the Latin hypercube sampling method because it was difficult to perform all the scenarios through experiments. The reliability of the experiment was improved by adding a situation when the general situation and the accident situation exist. In the experiments, the average travel time of probe vehicles at different market penetration rates were compared with the average travel time of the entire vehicles. As a result, the minimum market penetration rate of probe vehicles for obtaining expressway traffic information was found to be 45%. In addition, it is estimated that 25% market penetration rate of probe vehicle can meet 70% of traffic situations in accident scenario.

• Journal of Internet Computing and Services
• /
• v.21 no.2
• /
• pp.109-119
• /
• 2020

The FPGAs are semiconductors that can be redesigned after initial fabrication. It is used in various embedded systems such as signal processing, automotive industry, defense and military systems. However, as the complexity of hardware design increases and the design and manufacturing process globalizes, there is a growing concern about hardware trojan inserted into hardware. Many detection methods have been proposed to mitigate this threat. However, existing methods are mostly targeted at IC chips, therefore it is difficult to apply to FPGAs that have different components from IC chips, and there are few detection studies targeting FPGA chips. In this paper, we propose a method to detect hardware trojan by learning the static features of hardware trojan in LUT-level netlist of FPGA using machine learning.

• Journal of IKEEE
• /
• v.18 no.4
• /
• pp.586-592
• /
• 2014

In this paper, high efficiency power management IC(PMIC) with DT-CMOS(Dynamic threshold voltage Complementary MOSFET) switching device is presented. PMIC is controlled PWM control method in order to have high power efficiency at high current level. The DT-CMOS switch with low on-resistance is designed to decrease conduction loss. The control parts in Buck converter, that is, PWM control circuit consist of a saw-tooth generator, a band-gap reference(BGR) circuit, an error amplifier, comparator circuit, compensation circuit, and control block. The saw-tooth generator is made to have 1.2MHz oscillation frequency and full range of output swing from supply voltage(3.3V) to ground. The comparator is designed with two stage OP amplifier. And the error amplifier has 70dB DC gain and $64^{\circ}$ phase margin. DC-DC converter, based on current mode PWM control circuits and low on-resistance switching device, achieved the high efficiency nearly 96% at 100mA output current. And Buck converter is designed along LDO in standby mode which fewer than 1mA for high efficiency. Also, this paper proposes two protection circuit in order to ensure the reliability.

• The Journal of Korean Institute of Electromagnetic Engineering and Science
• /
• v.25 no.11
• /
• pp.1164-1171
• /
• 2014

Bulk Current Injection(BCI) test is a method of injecting current into Integrated Circuit(IC) using a current injection probe to qualify the standards of Electromagnetic Compatibility(EMC). This paper, we propose a microstrip coupler structure that can replace the BCI current injection probe that is used to inject a RF noise in standard IEC 62132-part 3 documented by International Electrotechnical Commission. Conventional high cost BCI probe has mostly been used in testing automotive ICs that use high supply voltage. We propose a compact microstrip coupler which is suitable for immunity testing of low power ICs. We tested its validity to replace the BCI injection probe from 100 MHz to 1,000 MHz. We compared the power[dBm] that is needed to generate the same level of noise between current injection probe and microstrip coupler by sweeping the frequency. Results show that microstrip coupler can inject the same level of noise into ICs for immunity test with less power.

• Applied Biological Chemistry
• /
• v.37 no.2
• /
• pp.105-109
• /
• 1994

Five cytotoxic and antioxidative flavonoids were isolated from the stem bark of Cudrania tricuspidata by consecutive purification using HP-20, silicagel and prep-HPLC. They were identified as taxifolin, orobol, eriodictyol, dihydrokaempferol and steppogenin by means of spectral studies. The antioxidative activities $(IC_{50})$ assayed by TBA method of these compound $1{\sim}5$ to were 6, 3, 3, >50, and $10\;{\mu}g/ml$, respectively. The effect on the growth inhibition $(IC_{50})$ of these compounds against P388 cell line were found to be 0.18, 3.3, 15 and $6.2\;{\mu}g/ml$, respectively in the order of compound 2 to 5.