• Journal of Welding and Joining
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• 제31권1호
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• pp.58-64
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• 2013

The following results were obtained, microstructures and tensile properties in arc brazed joints of DP(dual phase) steel using Cu-5.3wt%Sn insert metal was investigated as function of brazing current. 1) The Fusion Zone was composed of ${\alpha}Fe+{\gamma}Cu$ and Cu23Sn2. The reason for the formation of these solid solutions. Despite, Fe & Cu were impossible to solid solution at room temperature. It's melting & reaction to something of insert metal & Base Metal (DP Steel) by Arc. Brazing Process has faster cooling rate then Cast Process, Supersaturated solid solution at room temperature. 2) The increase Hardness of Fusion Zone was directly proportional to the rise of welding current. Because, ${\alpha}Fe+{\gamma}Cu$ phase (higher hardness than the Cu23Sn2.(104.1Hv < 271.9Hv)) Volume fraction was Growth, due to increasing the amount of base metal melting by High current. 3) The results of tensile shear test by Brazing, All specimens happen to fracture in Fusion Zone. On the other hand, when Brazing Current increasing tend to rise tensile load. but it was very small, about 26-30% of the base metal. 4) The result of fracture analysis, The crack initiate at Triple Point for meet to Upper B.M/Under B.M/Fusion Zone. This Crack propagated to Fusion zone. So ruptured by tensile strength. The Reason to in the fusion zone fracture, Fusion zone by Brazing of hardness (strength) was very lower then the base metal (DP steel). In addition the Fusion Zone's thickness in triple point was thin than the base metal's thickness in triple point.

• 열처리공학회지
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• 제6권1호
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• pp.1-8
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• 1993

In this paper, the surface roughness influenced by Sm45C hardness in high frequency induction hardening and mechanical characteristics for the changed Hv 598 part and the unchanged hardness Hv 223 part by use of cermet and ceramic cutting tools was experimentally examined. Finally, we could be had some important results by processing surface roughness on cutting conditions such as cutting speed, feed rate, depth of cut and changes of tool nose radius. The results are summarized as follows. 1. In case of the same cutting condition, the hardness of workpiece was high and acquired the best processing surface roughness when the radius of the tool nose had 0.8 mm and feed rate was 0.04 mm/rev. 2. In case of the hardness of workpiece, though the cutting speed didn't have an effect on processing surface roughness, the less feed rate and the more processing surface roughness improved. On the other hand, the low inside the hardness of workpiece, the more cutting speed and the more feed rate increase, the processing surface of roughness improved. 3. Regardless of the hardness of workpiece, the change of the cutting depth didn't have great effect on the surface roughness. 4. On cutting the high surface hardness part with cutting tools of cermet and ceramic, it can be acquired the higher processing surface roughness because it hadn't been taken effect on cutting speed, In case of the cutting process of the low inside hardness part the two cutting tools have acquired the similar processing surface roughness.

• 대한기계학회논문집A
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• 제35권12호
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• pp.1655-1662
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• 2011

본 연구는 레이저를 이용한 스테인리스강의 용접성 평가에 대한 연구이다. 사용된 금속인 스테인리스 스틸은 녹 및 열적변형이 우수하여 다양한 적용 분야를 가지고 있다. 본 연구는 50 W 레이저 열원에 자기장을 적용하여 스테인리스 스틸에 기계적 성질을 향상 시키는데 목적을 두고 있다. 이에 따른 기계적 성질을 분석하기 위하여 수치적 해석, 인장강도, 형상 및 미세조직, 경도 시험 등을 수행하였다. 결과적으로 수치적 해석을 통한 금속 용융점에서의 속도 증가, 인장강도 약 16 MPa 상승, 용융부에 섞임, 경도 약 7 Hv 상승으로 기계적 성질이 향상 되었다.

• 한국분말재료학회지
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• 제21권3호
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• pp.229-234
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• 2014

This study manufactured a CIG-based composite coating layer utilizing a new warm spray process, and a mixed powder of Cu-20at.%Ga and Cu-20at.%In. In order to obtain the mixed powder with desired composition, the Cu-20at.%Ga and Cu-20at.%In powders were mixed with a 7:1 ratio. The mixed powder had an average particle size of $35.4{\mu}m$. Through the utilization of a warm spray process, a CIG-based composite coating layer of $180{\mu}m$ thickness could be manufactured on a pure Al matrix. To analyze the microstructure and phase, the warm sprayed coating layer underwent XRD, SEM/EDS and EMPA analyses. In addition, to improve the physical properties of the coating layer, an annealing heat treatment was conducted at temperatures of $200^{\circ}C$, $400^{\circ}C$ and $600^{\circ}C$ for 1 hour each. The microstructure analysis identified ${\alpha}$-Cu, $Cu_4In$ and $Cu_3Ga$ phases in the early mixed powder, while $Cu_4In$ disappeared, and additional $Cu_9In_4$ and $Cu_9Ga_4$ phases were identified in the warm sprayed coating layer. Porosity after annealing heat treatment reduced from 0.75% (warm sprayed coating layer) to 0.6% (after $600^{\circ}C/1hr$. heat treatment), and hardness reduced from 288 Hv to 190 Hv. No significant phase changes were found after annealing heat treatment.

• 열처리공학회지
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• 제13권4호
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• pp.224-230
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• 2000

Garbon steel(SM35C) was gas nitrocarburized at $580^{\circ}C$ in $55%N_2-40%NH_3-5%CO_2$ mixed gas atmosphere, and then the steel was induction hardened at $850^{\circ}C$. The microstructure of gas nitrocarburized surface layer was observed by optical microscope and SEM. The phase analysis was carried out by X-ray diffraction method. The mechanical properties of gas nitrocarburized SM35C steel was evaluated by hardness, wear and fatigue test. The thickness of compound and diffusion layer were increased with increasing the gas nitrocarburizing time and the densest compound layer was obtained at 3 hours gas nitrocarburizing time. In case of 15sec induction hardening after gas nitrocarburizing, the surface hardness was decreased from 800Hv to 630Hv owing to the decomposition of compound layer, but wear resistance was increased because of increased hardness of diffusion layer. The fatigue strength of induction hardened steel after gas nitrocarburizing, $58kgf/mm^2$, was higher than $41.5kg/mm^2$ of gas nitrocarburized steel and $45kg/mm^2$ of induction hardened steel, respectively.

• 열처리공학회지
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• 제21권1호
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• pp.10-19
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• 2008

To investigate the effect of ultrasonic nano-crystalline surface modification (UNSM) treatment on rolling contact fatigue and residual stress properties of bearing steels, this paper carried out a rolling contact fatigue test, measured residual stress and retained austenite, performed a wear test, observed microstructure, measured micro hardness, and analyzed surface topology. After the UNSM treatment, it was found that the surface became minute by over $100{\mu}m$. The micro surface hardness was changed from Hv730~740 of base material to Hv850~880 with about 20% improvement, and hardening depth was about 1.3 mm. The compressive residual stress was measured as high as -700~-900 MPa, and the quantity of retained austenite was reduced to 27% from 34%. The polymet RCF-6 ball type rolling contact fatigue test showed over 4 times longer fatigue lifetime after the UNSM treatment under 551 kgf load and 8,000 rpm. In addition, this paper observed the samples, which went through the rolling contact fatigue test, with OM and SEM, and it was found that the samples had a spalling phenomenon (the race way is decentralized) after the UNSM treatment. However, before the treatment, the samples had excessive spalling and complete exploration. Comparison of the test samples before and after the UNSM treatment showed a big difference in the fatigue lifetime, which seems to result from the complicated effects of micro particles, compressive residual stress, retained austenite, and surface topology.

• 열처리공학회지
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• 제18권6호
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• pp.369-374
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• 2005

Nitrogen ion implantation in Nimonic 80A using plasma immersion ion implantation (PIII) was investigated at a pulse voltage of -60 kV and ion dose of $3{\times}10^{17}{\sharp}/cm^2$, $6{\times}10^{17}{\sharp}/cm^2$, $12{\times}10^{17}{\sharp}/cm^2$. PIII is an effective technology to improve the surface hardness and wear resistance of materials. And also this technology is not limited by the shape and size of materials. PIII would be a promising technique in the future. Surface hardness and wear resistance of the $N^+$ ion implanted Nimonic 80A were increased with the increase in the incident ion dose. The surface hardness of the untreated Nimonic 80A is 420 Hv, the hardness of implanted Nimonic 80A is 1050 Hv at $N^+$ ion dose of $12{\times}10^{17}{\sharp}/cm^2$. The wear loss of the untreated is 82.5 mg, the wear loss of the implanted is 0.004g at $N^+$ ion dose of $12{\times}10^{17}{\sharp}/cm^2$. The $Cr_2N$ is detected on the surface of the implanted Nimonic 80A by XRD analysis.

• 한국표면공학회지
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• 제42권3호
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• pp.116-121
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• 2009

The 2-step low temperature plasma processes (the combined carburizing and post-nitriding) offer the increase of both surface hardness and thickness of hardened layer and corrosion resistance than the individually processed low temperature nitriding and low temperature carburizing techniques. The 2-step low temperature plasma processes were carried out for improving both the surface hardness and corrosion resistance of AISI 316L stainless steel. The influence of gas compositions on the surface properties during nitriding step were investigated. The expanded austenite (${\gamma}_N$) was formed on all of the treated surface. The thickness of ${\gamma}_N$ and concentration of N on the surface increased with increasing both nitrogen gas and Ar gas levels in the atmosphere. The thickness of ${\gamma}_N$ increased up to about $20{\mu}m$ and the thickness of entire hardened layer was determined to be about $40{\mu}m$. The surface hardness was independent of nitrogen and Ar gas contents and reached up to about 1200 $HV_{0.1}$ which is about 5 times higher than that of untreated sample (250 $HV_{0.1}$). The corrosion resistance in 2-step low temperature plasma processed austenitic stainless steels was also much enhanced than that in the untreated austenitic stainless steels due to a high concentration of N on the surface.

• 마이크로전자및패키징학회지
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• 제13권4호
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• pp.37-43
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• 2006

플립칩 공정에 Sn 범프를 적용하기 위해 도금전류밀도와 전류모드에 따른 Sn 도금막의 표면 거칠기와 경도를 측정하였다. 전류밀도 $5{\sim}50\;ma/cm^{2}$에서 전기도금한 Sn 도금막은 $2.0{\sim}2.4{\mu}m$의 표면 거칠기를 나타내었으며, 직류모드보다 펄스모드로 형성한 Sn 도금막에서 표면 거칠기가 감소하였다 할로겐 램프를 사용하여 $300^{\circ}C$에서 3초간 유지하는 표면 열처리에 의해 Sn 도금의 표면 거칠기가 $1\;{\mu}m$ 정도로 현저히 저하되었다. 전류밀도 $5{\sim}50mA/cm^{2}$에서 전기도금한 Sn 도금막은 10 Hv의 경도를 나타내었다. Sn 범프들을 이용하여 플립칩 본딩한 시편들은 $33{\sim}17m{\Omega}$의 낮은 접속저항을 나타내었다.

• 한국재료학회지
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• 제30권9호
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• pp.465-473
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• 2020

For surface hardening of a continuous casting mold component, a fundamental metallurgical investigation on dissimilar laser clads (Cu-NiCrBSi) is performed. In particular, variation behavior of microstructures and mechanical properties (hardness and wear resistance) of dissimilar clads during long-term service is clarified by performing high-temperature post-clad heat treatment (temperature range: 500 ~ 1,000 ℃ and isothermal holding time: 20 ~ 500 min). The microstructures of clad metals (as-clads) consist of fine dendrite morphologies and severe microsegregations of the alloying elements (Cr and Si); substrate material (Cu) is clearly confirmed. During the post-clad heat treatment, the microsegregations are totally homogenized, and secondary phases (Cr-based borides and carbides) precipitated during the short-term heat treatment are also almost dissolved, especially at the heat treatment conditions of 950 ℃ for 500 min. Owing to these microstructural homogenization behaviors, an opposite tendency of the surface mechanical properties can be confirmed. In other words, the wear resistance (wear rate) improves from 4.1 × 10^-2 ㎣/Nm (as-clad condition) to 1.4 × 10^-2 ㎣/Nm (heat-treated at 950 ℃ for 500 min), whereas the hardness decreases from 453 HV (as-clad condition) to 142 HV (heat-treated at 950 ℃ for 500 min).