• Title/Summary/Keyword: Grain Structure

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Properties of the Green Gold Alloys with Indium Content

  • Song, Jeongho;Song, Ohsung
    • Korean Journal of Materials Research
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    • v.28 no.4
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    • pp.221-226
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    • 2018
  • The property changes of 18, 14, and 8K green gold alloys for jewelry are observed by adding 0.0, 3.0, and 5.0 wt% of indium (In), respectively. To check the composition of the alloys, an energy dispersive spectroscopy (EDS) analysis is conducted. Color and microstructure analysis is executed through bare-eye, macro camera, UV-VIS-NIR-colormeter, and optical microscope. The melting point, wetting angle, and hardness are measured using TGA-DTA, a wetting angle tester, and a Vickers hardness tester. The EDS analysis result demonstrates that each of the green gold alloys was manufactured with purposed contents. The color analysis result shows that the color of the alloys is similar to the color of the conventional 4 wt%-Cd 18K green gold, and the green color improves as the In content increases. The micro structure analysis result demonstrates that grain refinement improves as the amount of In increases. Enhancements in the melting point, wettability, and Vickers hardness changes appear as the In content increases and Au content decreases. The hardness is up to 260, which implies good durability. Therefore, the results suggest that the proposed 18, 14, and 8K In-added green gold alloys enhance the properties of jewelry products with regard to the green color, castability, and durability.

Effects of Electron Irradiation on the Properties of ZnO Thin Films

  • Kim, Seung-Hong;Kim, Sun-Kyung;Kim, So-Young;Kim, Daeil;Choi, Dae-Han;Lee, Byung-Hoon;Kim, Min-Gyu
    • Transactions on Electrical and Electronic Materials
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    • v.14 no.4
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    • pp.208-210
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    • 2013
  • ZnO films were deposited on glass substrates by radio frequency (RF) magnetron sputtering and exposed to intense electron beam irradiation to investigate the effects of electron irradiation on the properties of the films. Although all of the films had ZnO (002) textured structure regardless of electron irradiation, the grain sizes of the films decreased with electron irradiation. Surface roughness also depended on electron irradiation. The surface roughness varied between 2.3 and 1.6 nm, depending on the irradiation energy. Based on photoluminescence (PL) characterization, the most intense UV emission was observed from ZnO films irradiated at 900 eV. Since the intensity of UV emission is dependent upon the stoichiometric of ZnO films, we conclude that 900 eV was the optimum electron irradiation energy to achieve the best stoichiometric of ZnO films in this study.

Planting foundations and Turfgrass Species Adapted to Grounds (스포츠 그라운드에 적합한 식재지반과 잔디 초종에 관한 연구)

  • 심상렬;정대영;김경남
    • Journal of the Korean Institute of Landscape Architecture
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    • v.28 no.2
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    • pp.61-70
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    • 2000
  • The purpose of this study is to identify the proper species of turf and the ground structure for the turf sports grounds. Analysis items are particle distribution of sand and gravel, saturated hydraulic conductivity, soil hardness, and turf growth. Results of this study are as follows. 1)The particle distribution of sand used in the multi-layer rootzone is within the upper limit of the standard level. The diameter of mid-size grain({TEX}$D_{50}${/TEX})was 0.62mm and the value of uniformity ({TEX}$D_{90}${/TEX}/{TEX}$D_{10}${/TEX}) was 3.93. The particle size distribution of sand used in the single-layer rootzone was beyond the standard level as {TEX}$D_{50}${/TEX})=0.86 and {TEX}$D_{90}${/TEX}/{TEX}$D_{10}${/TEX}=8.86. 2) Saturated hydraulic conductivity of the sand was higher in the multi-layer rootzone than in the single-layer rootzone while bulk density was vice versa. 3) Surface hardness was high on Kentucky bluegrass+perennial ryegrass compared to zoysiagrass probably caused by root density. 4) Visual covering and visual rating were highly evaluated on zoysiagrass within summer while better evaluated on Kentucky bluegrass+perennial ryegrass throughout fall to spring. 5) Visual color was better evaluated on Kentucky bluegrass+perennial ryegrass than on zoysiagrass throughout the year. These studies are demanded urgently according to increase in interest in the ground and turf species of the turf sports ground because of World Cup 2002.

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Characteristics of AlN Dielectric Layer for Metal PCB as a Function of Nitrogen Partial Pressure Using RF-Magnetron Sputtering Method (RF-Magnetron Sputtering 방법을 이용해 질소분압비에 따른 금속 PCB용 AlN 절연막의 특성)

  • Kim, Hwa-Min;Park, Jeong-Sik;Kim, Dong-Young;Bae, Kang;Sohn, Sun-Young
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.23 no.10
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    • pp.759-762
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    • 2010
  • In this investigation, the effects of $N_2/(Ar+N_2)$ gas partial pressure on the structural, electrical, and thermal properties of AlN dielectric layers prepared on aluminum substrates using RF-magnetron sputtering method were analyzed. Among the films, the AlN dielectric film deposited under $N_2/(Ar+N_2)$ gas partial pressure of 75% exhibit the highest AlN (002) preferred orientation, which was grain size of about 15.32 nm and very dense structure. We suggest the possibilities of it's application as a dielectric layer for metal PCB because the AlN films prepared at optimized gas partial pressure can improving the insulating property, the thermal conductivity, and thermal diffusivity of the films.

(TlPbBi)-(SrBa)-Ca-Cu-O superconducting films obtained by electrodeposition process

  • 백상민;이준호;김봉준;박기곤;김영철;정대영;심윤보
    • Progress in Superconductivity
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    • v.4 no.2
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    • pp.157-161
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    • 2003
  • We have performed the electrochemical method to fabricate high temperature superconducting (TlPbBi) -(SrBa)-Ca-Cu-O films. The precursors of the superconducting sample were codeposited at a periodic pulsed-potential cycle (1 second at -4V and 1 second at -1V) on a silver substrate. The variation of structure, microstructure and element were analysed by ICP and SEM techniques. The specimens were consisted predominantly of the Tl-1212 phase and have a transition temperature of 80~87 K in low magnetic field. It was showed that each grain has the stoichiometric ratio of $T1_{0.7}$Pb_$Bi_{0.3}$ $_Sr{0.1}$ $Ba_{2.4}$ $Ca_{0.2}$ $Cu_{1.2}$ $2.5/O_{x}$ by EDX analysis.sis.

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Synthesis and Emission Properties of CaMoO4:Tb3+ Green Phosphor Powders and Thin Films (CaMoO4:Tb3+ 녹색 형광체 분말과 박막의 제조와 발광 특성)

  • Jeon, Yongil;Cho, Shinho
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.26 no.4
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    • pp.264-270
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    • 2013
  • $CaMoO_4:Tb^{3+}$ green phosphor powders and thin films were successfully prepared by using the solid-state reaction method and the radio-frequency magnetron sputtering technique, respectively. The crystalline structure of all phosphor powders with different $Tb^{3+}$ ion concentrations was found to be a tetragonal system with the maximum diffraction intensity at $28.58^{\circ}$, while that of the phosphor thin films, irrespective of the type of substrate, was amorphous. As for the phosphor powders, the grain particles showed the chain-like patterns with inhomogeneous size distribution, the excitation spectra were composed of a broad band peaked at 307 nm and two small narrow bands centered at 381 and 492 nm, and the highest green emission spectrum was observed at 0.01 mol of $Tb^{3+}$ ions. As for the phosphor thin films, the average transmittance exceeding 85% was measured in the 400~1,100 nm range and the optical band gap showed a significant dependence on the type of substrate.

Dielectric and Pyroelectric Properties of Dy-doped BSCT Thick Films by Screen-printing Method

  • Noh, Hyun-Ji;Lee, Sung-Gap;Nam, Sung-Pill
    • Journal of Electrical Engineering and Technology
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    • v.4 no.4
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    • pp.527-530
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    • 2009
  • $(Ba_{0.57}Sr_{0.33}Ca_{0.10})TiO_3$(=BSCT) powders, prepared by the sol-gel method, were doped using $MnCO_3$ as the acceptor and $Dy_2O_3$ as the donor. This powder was mixed with an organic vehicle. BSCT thick films were fabricated by the screen-printing techniques on the alumina substrate. The structural and dielectric properties of BSCT thick films were investigated with variation of the $Dy_2O_3$ amount. As a result of the differential thermal analysis (DTA), the exothermic peak was observed at around $670^{\circ}C$ due to the formation of the polycrystalline perovskite phase. All the BSCT thick films showed the XRD patterns of a typical polycrystalline perovskite structure. The average grain size of BSCT thick films decreased with an increasing amount of $Dy_2O_3$. The relative dielectric constant and dielectric loss of the BSCT thick film doped $Dy_2O_3$ 0.1mol% were 4637.4 and 1.6% at 1kHz, respectively.

Settlement Characteristics of Three Type of Artificial Reefs on Sandy Bottom in the Eastern Coast of Korea (동해안 사질지반에 시설된 인공어초 3종의 매몰 특성)

  • Kim, Dae-Kweon;Kim, Wan-Ki;Son, Yong-Soo;Yoon, Jang-Tack;Gong, Yong-Gun;Kim, Young-Dae;Lee, Ji-Hyun
    • Journal of Advanced Marine Engineering and Technology
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    • v.32 no.2
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    • pp.359-364
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    • 2008
  • Using multi beam echo sounder, side scan sonar and scuba diving equipment, ceramic type, uneven type and semicircle-ramus type reefs into sandy bottom were ascertained, the depth of submersion in 7.2-10.3m on the coast of Gangneung, East of Korea, forty uneven type artificial reefs(AR) were totally buried into the sandy bottom. Two of five semicircle-ramus type ARs had only of their top area exposed. For most of the 45 ceramic reefs, only the upper 25-150cm of ARs were visible. The burial pattern is different in west and east side of the reefs, where the east side is deeply buried compared to the west side. From these results. it is recommended that sufficient analysis of bottom structure and materials especially in the sandy sea area should be undertaken in order to determine the best type of artificial reefs to be deployed and the best location for depoloyment.

Densification of Copper Powders using High-pressure Torsion Process (고압비틀림 공정을 이용한 구리 분말의 치밀화)

  • Lee, Dong-Jun;Yoon, Eun-Yoo;Kang, Soo-Young;Lee, Jung-Hwan;Kim, Hyoung-Seop
    • Journal of Powder Materials
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    • v.19 no.5
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    • pp.333-337
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    • 2012
  • In this study, electrolytic copper powders were consolidated by high-pressure torsion process (HPT) which is the most effective process to produce bulk ultrafine grained and nanocrystalline metallic materials among various severe plastic deformation processes. The bulk samples were manufactured by the HPT process at 2.5 GPa and 1/2, 1 and 10 turns. After 10 turns, full densification was achieved by high pressure with shear deformation and ultrafine grained structure (average grain size of 677 nm) was observed by electron backscatter diffraction and a scanning transmission electron microscope.

A Study on the Moisture Adsorption and Permeability Characteristics of Weathered Granite Soils (화강토의 풍화도가 수분흡착 및 침투성에 미치는 영향)

  • 이대훈;도덕현
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.26 no.3
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    • pp.81-89
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    • 1984
  • To examine the moisture adsorption and permeability characteristics, weathered granite soils of different degrees of weathering, cultivated upland soils and sands of Han-river were sampled. The results are as follows: 1. In case that the mother rock was same, the pF values under same moisture content decreased according as the grain size of soil became finer by the weathering process. 2. In case that the mother rock was different, the pF value varied by the behavior of clay minerals, and the cultivated upland soils showed more sensitive reaction than sands and fresh granite soils. 3. The pF value changed by the difference of primary moisture content and also influenced by soil structure, testing method and etc. 4. The pF value and compaction curve had close relation, however under same moisture content, the pF value decreased by the increment of density. 5. The permeability depend on the available void ratio between the soil particles according to the degree of weathering, and the pF value of available void water between the soil particles which related directly to permeability was about 3.3 except the void water holded in the soil particles. 6. As the above, the pF value and permeability were differentiated by degree of weathering, primary moisture content, density and etc. Therefore it is considered unreasonable to define uniformly by soil texture.

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