• 제목/요약/키워드: Electron Beam Melting

검색결과 56건 처리시간 0.031초

전자빔용해법(溶解法)에 의한 탄탈럼 스크랩의 재활용(再活用) 및 정련(精鍊) (Recycling and refining of tantalum scraps by electron beam melting)

  • 이백규;오정민;최국선;김형석;임재원
    • 자원리싸이클링
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    • 제21권2호
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    • pp.59-65
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    • 2012
  • 본 연구는 전자산업용 탄탈럼 스크랩의 재활용을 위하여 전자빔 용해에 의한 정련 효과를 조사 하였고 정련된 탄탈럼의 극미량 불순물은 글로방전 질량분석기를 이용하여 분석하였다. 탄탈럼 내 대부분의 불순물은 전자빔 용해에 의하여 수 ppm 수준으로 제거되어 초기 탄탈럼 스크랩의 순도인 4 N(99.996%)급에서 5 N(99.9991%)급으로 향상되었다. 탄탈럼 내 금속 불순물의 경우 초기 30 ppm에서 전자빔 반복 용해에 의해 8 ppm으로 감소된 것을 확인하였다. 또한 탄탈럼 내 가스 불순물의 경우 초기 470 ppm에서 전자빔 반복 용해에 의해 50 ppm으로 크게 감소하였다. 본 연구 결과를 통하여 탄탈럼 스크랩에 있어서 전자빔 용해에 의한 재활용 가능성 및 반복 용해에 의한 정련 효과를 확인하였다.

전자선 조사가 저밀도 폴리에틸렌 필름의 전기 전도도특성에 미치는 영향 (The Effect of Electron Beam Irradiation on the Electrical Conductivity Characteristics in Low Density Polyethylene Film)

  • 이종필;이수원;홍진웅
    • 한국안전학회지
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    • 제14권2호
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    • pp.77-82
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    • 1999
  • In this paper, physical properties and electrical conductivity of electron beam irradiated low density polyethylene are studied. The specimens of thickness 100 $\mu\textrm{m}$ irradiated as each 1 Mrad, 2 Mrad, 4 Mrad, 8 Mrad, 16 Mrad and virgin are used in this experiment. FTIR analysis shows strong absorptions by methyl groups in wavenumbers 720 $cm^{-1}$ and 1463 $cm^{-1}$, and did not show any evidences of the presence of residual carbonyl groups. From the DSC analysis, the crystalline melting point of electron beam irradiated specimen is lower than that of virgin specimen. 1 Mrad irradiated sample shows the stable electrical conductivity characteristics with both temperature and electric field.

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저밀도 폴리에틸렌의 도전율에 미치는 전자선 조사의 영향 (The Influence of Electron Beam Irradiation due to Conductivity in the Low Density Polyethylene)

  • 조경순;김이두;신현택;이수원;이종필;홍진웅
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1998년도 추계학술대회 논문집
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    • pp.191-194
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    • 1998
  • In this paper, the physical and conductivity properties due to the electron beam irradiation for low density polyethylene using insulating materials of the distribution cable and ultra-high voltage cable are studied. The specimens of the low density polyethylene of thickness 100[$\mu\textrm{m}$] irradiated as each 1 [Mrad], 2[Mrad], 4[Mrad], 8[Mrad], 16[Mrad] and virgin are used in this experiment. In order to measure the conductivity properties, the micro electrometer is used, the range of temperature and app1ying voltage are 20 to 120[$^{\circ}C$], from 100 to 1000[V] respectively So. as a result of the conductivity properties, it is confirmed that the conductivity is increased nearly to 50[$^{\circ}C$], and is not changed until the crystalline melting point from the temperature over 60[$^{\circ}C$] because of the defects of morphology and the formation of many trap centers by means of electron beam irradiation

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Tiled Ribbon-shaped Thin Silicon Grains Produced with Comb-shaped Beam in ZMR-ELA

  • Nakata, Mitsuru;Okumura, Hiroshi;Kanoh, Hiroshi;Hayama, Hiroshi
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2004년도 Asia Display / IMID 04
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    • pp.412-414
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    • 2004
  • We have developed nucleation control methods applicable to a zone-melting recrystallization excimer laser annealing process for poly-Si films. Ribbon-shaped Si grains of 2 ${\mu}m$-width were successfully aligned side by side by means of a comb-shaped beam, and we have successfully fabricated TFTs with channels formed in those grains. Electron mobility in the TFTs is as high as 677-$cm^2$/Vs.

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Microstructure and Hardness of Surface Melting Hardened Zone of Mold Steel, SM45C using Yb:YAG Disk Laser

  • Lee, Kwang-Hyeon;Choi, Seong-Won;Yoon, Tae-Jin;Kang, Chung-Yun
    • Journal of Welding and Joining
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    • 제34권1호
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    • pp.75-81
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    • 2016
  • This study applied laser surface melting process using CW(Continuous wave) Yb:YAG laser and cold-work die steel SM45C and investigated microstructure and hardness. Laser beam speed, power and beam interval are fixed at 70 mm/sec, 2.8 kW and $800{\mu}m$ respectively. Depth of Hardening layer(Melting zone) was a minimum of 0.8 mm and a maximum of 1.0 mm that exceeds the limit of minimum depth 0.5 mm applying trimming die. In all weld zone, macrostructure was dendrite structure. At the dendrite boundary, Mn, Al, S and O was segregated and MnS and Al oxide existed. However, this inclusion didn't observe in the heat-affected zone (HAZ). As a result of interpreting phase transformation of binary diagram, MnS crystallizes from liquid. Also, it estimated that Al oxide forms by reacting with oxygen in the atmosphere. The hardness of the melting zone was from 650 Hv to 660 Hv regardless of the location that higher 60 Hv than the hardness of the HAZ that had maximum 600 Hv. In comparison with the size of microstructure using electron backscatter diffraction(EBSD), the size of microstructure in the melting zone was smaller than HAZ. Because it estimated that cooling rate of laser surface melting process is faster than water quenching.

전자선 조사에 따른 절연재료(LDPE)의 전기전도특성 (Electrical Conduction Properties due to Electron Beam Irradiation of Low Density Polyethylene)

  • 이종필;김이두;오세영;김석환;김왕곤;이충호;홍진웅
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1998년도 하계학술대회 논문집 D
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    • pp.1416-1418
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    • 1998
  • In this paper, the physical and electrical conduction properties due to the electron beam irradiation for low density polyethylene using insulating materials of the distribution cable and ultra-high voltage cable are studied. In FTIR spectrum for physical properties, the strong absorptions by methyl groups in wavenumbers 720[$cm^{-l}$] and 1463[$cm^{-l}$] are observed, and the effect by residual carbonyl groups (C = 0) is hardly appeared. So, as a result of the electrical conduction properties, it is confirmed that the conduction current is increased nearly to 50[$^{\circ}C$], and is not changed until the crystalline melting point from the temperature over 60[$^{\circ}C$] because of the defects of morphology and the formation of many trap centers by means of electron beam irradiation.

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Structure and Property Modification of Bimodal Molecular Weight Distribution Polyethylene by Electron Beam Irradiation

  • Lee, Sang-Man;Jeon, Hye-Jin;Choi, Sun-Woong;Song, Hyun-Hoon;Nho, Young-Chang;Cho, Kyu-Cheol
    • Macromolecular Research
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    • 제14권6호
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    • pp.640-645
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    • 2006
  • Polyethylene of bimodal molecular weight distribution was irradiated with an electron beam. The thermal and mechanical properties were examined by DSC, small and wide angle X-ray scattering and static tensile test according to the crystal morphology of the irradiated samples. The crystal morphology change upon irradiation, as revealed by wide angle X-ray scattering, correlated well with the changes in melting enthalpy, whereas the lamellar thickness and the amorphous gap thickness remained virtually unchanged at irradiation doses up to 500 kGy. Crosslinks in the crystal domains became evident at an energy level of 250 kGy, resulting in reduced crystallinity and crystal size of the (110) and (200) planes. The samples became stiff and brittle with increased irradiation dose, which seem to be more relevant to the amount of cross links than the crystal morphology changes.

후판 Al 6061합금의 전자빔용접 특성 평가 (The Characteristic Evaluation of Electron Beam Welding for Al 6061 alloy with thick-thickness plate)

  • 정인철;심덕남;김용재
    • 대한용접접합학회:학술대회논문집
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    • 대한용접접합학회 2006년도 춘계 학술대회 개요집
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    • pp.68-70
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    • 2006
  • For the aluminum material of the thick-thickness more than 100mm Penetration depth Electron beam welding is effectively applicable with a characteristic of high energy intensity. But Al 6061 alloy has high crack sensitivity due to minor alloys, which are silicon, magnesium, copper etc. With a sample block of 135mm thickness EBW test was performed in vertical position. As tensile strength has $210{\sim}220N/mm^2$ with weld area broken. Bend test shows low ductility with fracture of partly specimens. Chemical contents of alloys show no difference between weld and base metal. Defect in middle weld area figures out typical hot crack due to low melting materials. Micro structure of weld area has some difference compare to HAZ and base metal. As a result of EBW test for Al 6061 alloy, it shows that weld defect could be occurred even though establishing of optimum weld parameter condition.

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마이크로컬럼 어레이에 적용 가능한 웨이퍼단위의 수직 배선 방법 (Wafer level vertical interconnection method for microcolumn array)

  • 한창호;김현철;강문구;전국진
    • 대한전자공학회:학술대회논문집
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    • 대한전자공학회 2005년도 추계종합학술대회
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    • pp.793-796
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    • 2005
  • In this paper, we propose a method which can improve uniformity of a miniaturized electron beam array for inspection of very small pattern with high speed using vertical interconnection. This method enables the individual control of columns so that it can reduce the deviation of beam current, beam size, scan range and so on. The test device that used vertical interconnection method was fabricated by multiple wafer bonding and metal reflow. Two silicon and one glass wafers were bonded and metal interconnection by melting of electroplated AuSn was performed. The contact resistance was under $10{\Omega}$.

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전자선 가교된 유리섬유 강화 나일론 12의 열적 거동 및 내마모 특성 (Thermal Behavior and Abrasion Properties of Glass Fiber Reinforced Nylon 12 Crosslinked by Electron Beam Irradiation)

  • 신범식;전준표;김현빈;강필현
    • 폴리머
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    • 제35권1호
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    • pp.30-34
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    • 2011
  • 나일론 12의 열적 거동 및 내마모 특성을 확인하기 위해서 100~600 kGy로 조사선량을 달리 하여 전자선가교 반응을 진행하였다. 가교효과를 증대시키기 위해서 TAC, TAIC, TMPTMA의 가교제를 추가로 사용하였다. 나일론 12는 200 kGy 이상 전자선 가교가 진행되어야 높은 젤화율을 보이며, 조사선량이 증가할수록 결정성이 낮아져 $T_m$과 DSC 피크 면적이 서서히 감소되는 것을 확인하였고, 또한 열분해 온도가 상승하여 열적 안정성이 우수해짐을 확인하였다. 그리고 나일론 12의 내마모 특성도 향상되어 가교 전과 비교하였을 때 마모량, 마모계수가 감소하는 경향을 나타내었고, 마모 표변을 SEM 분석을 통해서 확인하였다. 나일론 12에 첨가된 가교제는 전자선 가교시 우수한 가교 효과를 나타내며, 열적, 내마모 특성을 향상시키는 것으로 확인되었다.