Hobun(Oyster shell W.) is a traditional material used as extender and white pigment from ancient times. The production method of it, however, has been discontinued. We have studied the traditional production method of Hobun through calcination of oyster shell, which is one of the traditional ways for preparing Hobun. Our work has the important meaning in that we can reproduce the manufacturing method of the discontinued traditional material and also it provides a solid background knowledge to stabilize the production and supply of Hobun for the cultural asset repairing materials. The result can be summarized as followings: The production processes of Hobun by calcination method are divided into 4 steps - calcination ${\rightarrow}$ slaking(pulverization) ${\rightarrow}$ separating fine powder by submergence in water ${\rightarrow}$ drying. In calcination step, the temperature is required to exceed $700^{\circ}$ to get pure white color of Hobun, since organic materials in the shell cause the final powder to be less white below $600^{\circ}$. And the calcination methods produce significant amount of calcium hydroxide, which is incongruent for pigment materials without additional treatments. The experimental study also demonstrated that the additional treatment process introduced in traditional paintings can be a probable process since the calcium of potassium hydroxide is observed to be promoted by this treatment. It is also concluded that, the calcination method of Hobun is appropriate for a small amount and high quality production.
Kim, Seong Eun;Lee, Jin Kyung;Lee, Chae Hoon;Chung, Yong Jae
Journal of Conservation Science
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v.35
no.6
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pp.681-688
/
2019
In this study, the characteristics of natural and synthetic adhesives used in woodcraft were evaluated. The pattern of deterioration of wood and adhesives according to changes in temperature and humidity were compared. For materials, one type of anlmal glue, three kinds of polyvinyl acetate adhesives, one type of epoxy adhesive and one type of zelkova wood were selected. Characteristics of physical and chemical characteristics, weather resistance and drying speed assessment were carried out. The adhesion characteristic evaluation showed that the adhesion strength of anlmal glue and one type of polyvinyl acetate adhesive were 6.54 N/㎟ and 7.01 N/㎟, pH meter of anlmal glue and polyvinyl acetate adhesives was pH 7.03 and pH 3.32-3.59 which were range of available as an adhesive. According to the test results of weather resistance, epoxy adhesives had the highest decreasing value in adhesion strength after deterioration. In the reversible test of the adhesive, it was found to be highly reversible in NaOH, a soluble solvent excluding epoxy, but attention is required when using the wood since it may show discoloration during processing.
Journal of the Korea Academia-Industrial cooperation Society
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v.19
no.2
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pp.683-688
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2018
In this study, we analyzed the heat generation state of a flat heating element by using image processing technology in conjunction with carbon fiber. The flat heating element is manufactured by chopping the carbon fiber to a small size and bonding it again using a dispersing agent. The solution of carbon fiber, bound together using the dispersant, is then filtered onto the nonwoven fabric. The last step is to obtain flat carbon fibers in the form of nonwoven fabrics for the purpose of drying the filtered carbon fibers. In the flat heating element, electricity may be applied to the carbon fiber on the surface produced in this manner. In this study, the flat heating element was analyzed by four methods. The analysis of the heat generation characteristics and heating rate of the flat heating element confirmed that the fabricated sheet heating element corresponds to a normal army. The analysis of the insulation coating and flat heating element module, which can be used for actual product manufacturing, involves two dimensional image analysis using image processing technology. The thermal image analysis of the flat heating element is a programming technique that not only analyzes the heat generation state in both two and three dimensions, but also displays the upper and lower 15 to 20% ranges of temperature corresponding to the heat generation in the image. In the final analysis, it is possible to easily find the erroneous part in the manufacturing process by directly showing the state of the fabricated flat heating element on the screen. By combining this image analysis method of the flat heating element with the existing method, we were able to more accurately analyze the heat generation state.
For the effective utilization of the coastal fish resources in Korea, an investigation on the optimum processing conditions and the quality of a textured fish protein concentrate similar to the texture of animal meat has been carried out with the fish meat of Alaska pollack and mackerel. A noodle shaped product was prepared with the fish meat paste after the adjustment of pH and salt content. The product was soaked in $96\%$ ethyl alcohol to produce textured fish protein concentrate and then dried. The processing conditions were estimated with the rehydration capacity of the textured fish protein concentrate(FFC). The quality of the final product was evaluated with chemical composition, sensory test and texture measurement. The optimum pH and salt content of the fish meat for the processing of meaty textured FPC were 7.5 and $1.0\%$ respectively. The most effective soaking conditions were as follows:soaking time, 40 min. ; temperature of alcohol, 5 to $20^{\circ}C$;amount of alcohol, 4 times the weight of tile fish meat paste, number of soaking in alcohol, 4 times. The alcohol remaining in meaty textured FPC could be removed effectively by forced air drying. The yield and the contents of protein and lipid in the meaty textured FPC from Alaska pollack were $19.9\%\;84.3\%\;and\;0.5\%$ and those from mackerel were $29.8\%,\;78.1\%\;and\;3.6\%$ respectively. The content of essential amino acid in the meaty textured FPC from Alaska pollack and mackerel was not inferior to that of beef, textured soybean protein and FAO pattern. Beef meat can be substituted with the meaty textured FPC up to $50\%$ in processing meat balls withoutanysignificantlossinthetaste, ordor and texture.
This study was carried out to confirm the effects of the knife-incising and kerfing pretreatment on the moisture content and surface check occurrence of Douglas-fir heavy timber. In the case of moisture content, the moisture gradient that formed in the inner part of the specimen was observed in all specimens. In addition, the moisture gradient was formed differently from the surface layer to 72 mm depending on the pretreatment conditions, and it was formed gradually in the kerfing than the knife-incising. In addition, it was found that the solid volume should be considered when measuring the average moisture content. In the case of surface check, the surface check occurrence was reduced in the knife-incising, kerfing, and the combination of knife-incising and kerfing than the control. In particular, the kerfing treatment was shown that the expansion of surface check width was effectively suppressed. In the case of knife-incising treatment, although the surface check was less than the control, the preventive effect on the surface check occurrence did not reach the level of the kerfing treatment.
Kim, Chong-Gun;Park, Cheul-Woo;Yoon, Tae-Ho;Lim, Nam-Gi
Journal of the Korean Wood Science and Technology
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v.41
no.3
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pp.234-246
/
2013
It was found that test piece heated rapidly by 3 kW microwave for 5 minutes satisfies the targeted temperature and the percentage of moisture content, and the highest rate of weight increase is obtained in case of 120 minute immersion in the mixture of phosphates and heterocyclic compounds, from the result of such analysis as: kiln drying schedule, flame retardent by flammability test, insect resistance by termites, and permeability of combined penetrant for the wood after assigning multifunctional finish by immersing conifer structural frame, which is used for the frame work of wooden house and indoor/outdoor finishing in flame retardant and insect repellent materials mixture with the remaining heat of microwave. In addition, after a test of flame retardent treated item, it was identified that every mixture of phosphates corresponds with the standards of flame retardent, and upon investigation of moritality of 7 days after putting termites, it was showed that test piece immersed in the mixture of phosphates and heterocyclic compounds has the best characteristics, showing over 96% of high moritality. From the analysis of inward permeability of combined penetrant for the wood, it was decided that excellent performance in the flame retardent and insect resistance of the wood revealed due to full penetration of combined penetrant as it was found that combined penetrant penetrated through the whole inner cells of the wood.
Filtered containment venting system (FCVS) is one of the severe accident mitigation systems designed to release containment pressurization to maintain its integrity. The thermal-hydraulic behaviors in FCVSs are important since they affect the operation characteristics of the FCVS. In this study, a representative FCVS was modeled by RELAP5/Mod3.3 code, and the Station BlackOut (SBO) was chosen as an accident scenario. The thermal-hydraulic behaviors of an FCVS during long-term operation with two venting strategies (open-and-close strategy, open-and-non-close strategy) and the sensitivity analysis of important parameters were investigated. The results show that the FCVS can operate up to 250 h with a periodic open-and-close strategy during an SBO. Under the combined effects of steam condensation and water evaporation, the solution inventory in the FCVS increases during the venting phase and decreases during the intermission phase, showing a periodic pattern. Under this condition, the appropriate initial water level is 3-4 m; however, it should be adjusted according to the environment temperature. The FCVS can accommodate a decay heat power of 150-260 kW and may need to feed water for a higher decay heat power or drain water for a lower decay heat power during the late phase. The FCVS can function within an opening pressure range from 450 kPa to 500 kPa and a closing pressure range between 250 kPa and 350 kPa. When the open-and-non-close strategy is adopted, the solution inventory increases quickly in the early venting phase due to steam condensation and then decreases gradually due to the evaporation of water; drying-up may occur in the late venting phase. Decreasing the venting pipe diameter and increasing the initial water level can mitigate the evaporation of the scrubbing solution. These results are expected to provide useful references for the design and engineering application of FCVSs.
Journal of the Korean Society of Food Science and Nutrition
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v.43
no.9
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pp.1400-1406
/
2014
This study investigated the quality characteristics of sea salt coated with coffee oil (SCO). Three-year-old salt was used after drying in an oven at $105^{\circ}C$ for 2 hours. Product A was composed of 100 g of sea salt and 8 g of coffee oil, product B was 100 g of sea salt and 16 g of coffee oil, and product C was 100 g of sea salt, 8 g of coffee oil, and 0.3 g of shell powder. The moisture content, ash content, color, peroxide value, acid value, and sensory evaluation of sea salt coated with coffee oil were determined monthly during 5 months of storage at room temperature. The contents of moisture and ash of SCO were 2~3% and 81~83%, respectively, but not significantly different during the storage period. Calcium content of product C was higher than that of product A or B. Coffee flavor in all SCO products was retained for 3 months. Hunter L, a, and b color values in SCO decreased with increasing storage period. However, redness and yellowness of product B were higher than those of other products. The peroxide and acid values of products A and C were lower than those of product B during storage period. Sensory evaluation during the storage period showed that quality of product A and C was maintained for 4 months, whereas product B was preserved for 3 months.
A preparation process's conditions of aqueous sol which contains anatase-type nano titania particles with photocatalyic properties was established by using Yoldas process, so called, DCS(Destabilization of Colloidal Solution) process in this study. And crystal size change and phase transformation of titania particles in aqueous titania sol depending on reaction conditions was investigated by a light scattering method and XRD analysis of frozen dried powders, respectively. This sol with photo catalytic nano titania particles was used to the following hydrophilic hybrid coating film's fabrication and its properties was evaluated. Subsequently, for coating film using the above mentioned aqueous titania sol, non-aqueous titania sol was prepared without any chemical additives and its time stability according to aging time was investigate. By using the above mentioned aqueous titania sol and non-aqueous sol, a complex oxide coating sol for metal and ceramic substrate and a organic-inorganic hybrid coating sol for polymer substrate was prepared and it's hydrophilicity depending on UV irradiation conditions was evaluated. As a conclusions, the following results were obtained. (1)Aqueous titania sol The average particle size of titania in formed aqueous titania sol was distributed between 20$\sim$90nm range depending on reaction conditions. And the crystal phase of titania powders obtained by frozen drying method was changed from amorphous state to anatase and subsequently transformed to rutile crystal phase and it is attributed to concentration gradient in aqueous sol. (2)Non-aqueous titania sol Non-aqueous titania sol was prepared using methanol as a solvent and a little distilled water for hydrolysis and nitric acid as a catalyst were used. The obtained non-aqueous titania sol was stable at room temperature for 20 days. Additionally, non-aqueous titania sol with addition of chealating reagent such as acethylaceton and ethylene glycol prolonged the stability of sol by six months. (3)Complex sol and hybrid sol with super hydrophilicity The above mentioned aqueous titania sol as a main photocataylic component and non-aqueous titania sol as a binder for coating process was used to prepare a complex sol used for metal, ceramic and wood material substrate and also to prepare the organic-inorganic hybrid sol for polymer substrate such as polycarbonate and polyethylene, in which process APMS(3-Aminopropyltrimethoxysilane), GPTS(3-Glycidoxypropyl-trimethoxysilane) as a hydrophilic silane compound and HEMA(2-Hydroxyethyl methacrylate) as a forming network in hybrid coating film were used. The hybrid coating film such as prepared through this process showed a superhydrophilicity below 1$10^{\circ}$ depending on processing conditions and a pencil's hardness over 6 H.
Journal of the Korean Crystal Growth and Crystal Technology
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v.27
no.1
/
pp.18-21
/
2017
In this study, spherical monodispersed cerium-doped yttrium aluminum garnet (YAG : $Ce^{3+}$) phosphor particles were synthesized via homogeneous precipitation method using the mixed solution of yttrium nitrate, cerium nitrate, aluminum nitrate, ammonium aluminum sulfate, and urea as a precipitant. During the process of precursors of monodispersed YAG : $Ce^{3+}$, aluminum ions which form spherical aluminum compounds precipitated first and yttrium compounds precipitated onto the surface of the existing spherical aluminum compounds. Drying process using lyophilization could obtain monodispered spherical YAG : $Ce^{3+}$ particles compare to using oven. The thermal calcination process of YAG : $Ce^{3+}$ precursors under the temperature of $1200^{\circ}C$ for 6 h was enough to obtain 400~500 nm sized YAG particles with pure YAG phase.
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