• Title/Summary/Keyword: Distillation Method

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Basic Study for Distillation of Rocket Grade Hydrogen Peroxide (추진제 급 과산화수소 증류를 위한 기초 연구)

  • Chung, Seung-Mi;An, Sung-Yong;Kwon, Se-Jin
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2009.05a
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    • pp.67-70
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    • 2009
  • Because many research using rocket grade peroxide is studied, distillation method for domestic production of rocket grade hydrogen peroxide is required. Distillation methods are very various and divided by feeding method, distillation time, distillation pressure, and so on. Among these, vacuum distillation is a suitable method for hydrogen peroxide. This method can reduce thermal decomposition and reaction with impurities. Distillation condition is determined by Raoult's law. Low vacuum level and vacuum level control are appeared as important problems of the experiment equipment, which are solved by using less leakage vacuum chamber and metering valve.

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The Validation Study of Auto Anlysis Method Combined with Aqua Regia Digestion for Fluorine of Soil (왕수분해와 결합한 자동분석법의 토양 중 불소시험 유효성 연구)

  • Na, Kyung-Ho;Yun, In-Chul;Lee, Jung-Bok
    • Journal of Soil and Groundwater Environment
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    • v.15 no.5
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    • pp.8-15
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    • 2010
  • The purpose of this research is to check the validation of an auto-analysis method combined with aqua regia digestion apparatus for improvement of water distillation method used as a fluorine test of soil. Fluorine contents of CaO used in the pretreatment course of water distillation method were 120 mg/kg ~ 5,064 mg/kg at the blank test, which was exceeded up to maximum 12.5 times of the soil standard, so it was estimated due to a effect of fluorine existing as impurities of CaO. The recovery test of the same samples indicated that water distillation method and auto-analysis method were 134.5mg/kg and 161.7mg/kg respectively, the recovery ratio of the latter was 16.8% higher than the formal. The validation test of two methods satisfied the standard, but auto analysis method was excellent more than distillation method. Also, auto analysis method could save a analysis time up to maximum 4.7 times by comparison with water distillation method.

Extraction Method of Antioxidants in Soybean Oil (Sweep Co-Distillation 법에 의한 산화방지제의 추출법)

  • 황혜정
    • The Korean Journal of Food And Nutrition
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    • v.12 no.4
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    • pp.358-363
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    • 1999
  • This study was conducted to evaluate the extraction methods for the determination of antioxidants in soybean oil. Recovery rates of various antioxidants in soybean oil showed similar rates as 80.4~102.1% by solvent/solvent extraction method and 89.9~106.4% by sweep co-distillation method except 46.6~61.2% of PG at corresponding spiked concentractions. The maximun recovery rates of antioxidnts were obtained when extraction time and extraction temperature used in UNITREX were 20min and 21$0^{\circ}C$ respectively. In the recovery rates with the activation of florisil when 2% ofwater was added to florisil the highest recovery rates for TBHQ, BHA, BHT were obtained by sweep co-distillation met-hod. Therefore sweep co-distillation method showed less solvent simple operation and high recovery rate compared with solvent/solvent extraction method.

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Performance analysis of Object detection using Self-Knowledge distillation method (자가 지식 증류 기법을 적용한 객체 검출 기법의 성능 분석)

  • Dong-Jun Kim;Seunghyun Lee;Byung-Cheol Song
    • Proceedings of the Korean Society of Broadcast Engineers Conference
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    • 2022.11a
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    • pp.126-128
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    • 2022
  • 경량화 기법 중 하나인 Knowledge distillation 은 최근 object detection task 에 적용되고 있다. Knowledge distillation 은 3 가지 범주로 나뉘는데 그들 중에서 Self-Knowledge distillation 은 기존의 Knowledge distillation 에서의 pre-trained teacher 에 대한 의존성 문제를 완화시켜준다. Self-Knowledge distillation 또한 object detection task 에 적용되어 training cost 를 줄이고 고전적인 teacher-based methods 보다 좋은 성능을 성취했다.

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Experimental Distillation Using a Fully Thermally Coupled Distillation Column with Separated Main Columns (분리주탑형 열복합 증류탑에서의 증류실험)

  • Park, Young-Min;Kang, Hyun-Woog;Kim, Young-Han
    • Journal of Institute of Control, Robotics and Systems
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    • v.12 no.12
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    • pp.1197-1201
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    • 2006
  • In order to improve the operability in a fully thermally coupled distillation column the main column is separated into an upper and a lower column, and its design method is explained. With a distillation experiment using a two-inch column the operability of the proposed column is examined. Readily available methanol, ethanol and propanol are used as the feed, and the experimental result is compared with that of the HYSYS simulation. It is found from the experiment that the recovery ranges between 58.8% and 68% and the distillation efficiency is lower than that of the simulation. consumes less energy than an original column, it is not widely implemented in practice due to its operational difficulty. However, it is proved that the proposed distillation column can be operated without compressors and it can be practically utilized.

A Study on Optimal Reflux Ratio for Batch Distillation (회분식 증류공정의 환류비 최적에 관한 연구)

  • 이영상;이의수
    • Journal of Institute of Control, Robotics and Systems
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    • v.8 no.10
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    • pp.833-841
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    • 2002
  • We develope a model that can manipulate the reflux ratio of a batch distillation process in real time for optimal operations. Firstly, reflux ratio decision model for batch distillation unit was developed using the simple short-cut method. Secondly, more detailed rigorous method was applied to improve the accuracy of the model. Based on these models, operational strategies for the optimal reflux ratio was proposed. The results are illustrated with suitable examples and compared with the results using commercial simulator.

Vacuum Distillation of Rocket Grade Hydrogen Peroxide with Temperature (온도 조건에 따른 추진제급 과산화수소의 진공 증류)

  • Chung, Seung-Mi;An, Sung-Yong;Kwon, Se-Jin
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2009.11a
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    • pp.89-92
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    • 2009
  • Because many research using concentrated hydrogen peroxide as propellant is studied, research for distillation method for domestic production of rocket grade hydrogen peroxide is needed. To distill hydrogen peroxide, vacuum distillation will be used because of heat decomposition of hydrogen peroxide. Distillation pressure is 30 torr which is determined by Raoult's law to distill under $40^{\circ}C$. Variable of distillation experiment is distillation temperature. And the comparison of distillation results was done by yield and operation time. In the result, generally, yield was lower and the water in receiver had higher concentration with shorter distillation time. And with similar time, when distillation temperature was higher, yield was lower and hydrogen peroxide became higher concentration.

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Performance Improvement of SRGAN's Discriminator via Mutual Distillation (상호증류를 통한 SRGAN 판별자의 성능 개선)

  • Yeojin Lee;Hanhoon Park
    • Journal of the Institute of Convergence Signal Processing
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    • v.23 no.3
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    • pp.160-165
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    • 2022
  • Mutual distillation is a knowledge distillation method that guides a cohort of neural networks to learn cooperatively by transferring knowledge between them, without the help of a teacher network. This paper aims to confirm whether mutual distillation is also applicable to super-resolution networks. To this regard, we conduct experiments to apply mutual distillation to the discriminators of SRGANs and analyze the effect of mutual distillation on improving SRGAN's performance. As a result of the experiment, it was confirmed that SRGANs whose discriminators shared their knowledge through mutual distillation can produce super-resolution images enhanced in both quantitative and qualitative qualities.

An Rapid Extraction of Ginseng Saponin Compounds (인삼사포닌 화합물의 신속한 추출)

  • Kwak, Yi-Seong;Kim, Mi-Ju;Kim, Eun-Hee;Kim, Yeoung-Ae
    • Korean Journal of Food Science and Technology
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    • v.29 no.6
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    • pp.1327-1329
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    • 1997
  • A new rapid saponin extraction method was developed with using of organic solvent and waring blonder. There was a good correlation between previous distillation method and this method in f major ginsenosides ($Rb_1$, $Rb_2$, Rc, Rd, Re, Rg1) contents. When the ratio of methanol and chloroform was 7:3, this method showed similar saponin contents (total major. ginsenosides contents) comparing with distillation method. Contents of total major ginsenosides were 2.41% in this method and 2.54% in distillation method. However, crude saponin content of this method was higher than that of distillation method.

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A Study on the Water-Ethanol Separation by Membrane-Aided Distillation in Bio-Ethanol Process (바이오 에탄올 생산을 위한 Membrane-Aided Distillation에 의한 물-에탄올 분리공정에 관한 연구)

  • Jung, Heon;Choi, Young-Seok;Yang, Dae-Rook;Joo, Oh-Shim;Jung, Kwang-Deog
    • Clean Technology
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    • v.14 no.2
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    • pp.129-135
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    • 2008
  • Nylon membrane was used to separate ethanol-water by a pervaporation method. Experimental equations were derived to use the simulation of membrane-aided distillation using nylon. The increases in permeation pressure resulted in the decrease in selectivity and energy consumption. The energy cost to enrich ethanol from 94 wt% to 99.5 wt% was calculated to be 53.3 won/kg of ethanol with extractive distillation and 18.9 won/kg of ethanol with a pervaporation method. The saving energy by the pervaporation method is consumed by recycling the permeate residue into the distillation column in the membrane-aided distillation column. Therefore, membrane with the high selectivity to minimize the permeate residue recycle is required to effectively enrich ethanol in the membrane-aided distillation method.

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