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Development of a diagnostic coronagraph on the ISS: progress report

  • Kim, Yeon-Han;Choi, Seonghwan;Bong, Su-Chan;Cho, Kyungsuk;Park, Young-Deuk;Newmark, Jeffrey;Gopalswamy, Nat.;Yashiro, Seiji;Reginald, Nelson
    • The Bulletin of The Korean Astronomical Society
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    • v.44 no.1
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    • pp.51.1-51.1
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    • 2019
  • The Korea Astronomy and Space Science Institute (KASI) has been developing a coronagraph in collaboration with the National Aeronautics and Space Administration (NASA), to install it on the International Space Station (ISS). The coronagraph will utilize spectral information to simultaneously measure electron density, temperature, and velocity. For this, we develop the coronagraph as a two-step process. First, we will perform a stratospheric balloon-borne experiment, so called BITSE, in 2019 with a new type of coronagraph. Second, the coronagraph will be installed and operate on the ISS (CODEX) in 2021 to address a number of questions (e.g., source and acceleration of solar wind, and coronal heating) that are both fundamental and practically important in the physics of the solar corona and of the heliosphere. In this presentation, we will introduce recent progresses.

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Development of simultaneous analysis of Pheniramine Maleate and Naphazoline Hydrochloride Ophthalmic Solution

  • Shin, Myoung-Hee;Lee, Young-Ja;Lee, Chang-Hee;Jin, Jong-Sung;Kim, Mi-Kyeong;Jin, Sun-Kyung;Doh, Hea-Jeong;Jung, Jin-Su
    • Proceedings of the PSK Conference
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    • 2003.10b
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    • pp.219.2-219.2
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    • 2003
  • We want to actively cope with technological developments by improving our drug specification in Korean Pharmaceutical Codex. Pheniramine maleate and naphazoline HCl of Pheniramine Maleate and Naphazoline Hydrochloride Ophthalmic Solution were ordained as UV spectroscopy and HPLC, respectively. Simultaneous analysis of those using HPLC has been developed. The assays of two drug products were 97.2%, 102.2% (pheniramine maleate), 96.8%, 101.3% (naphazoline HC1) respectively ; the specification rage if 90.0∼110.0%. (omitted)

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A Simple Method for Determining Residual p-arsanilic Acid in Aquatic Products using EDTA-Assisted Solvent Extraction and LC-MRM

  • Min Kyeong Kwon;Ye Bin Shin;Young Min Kim;Jin Hwan Kim;Ji Seong Kim;Yong Seok Choi
    • Mass Spectrometry Letters
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    • v.14 no.2
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    • pp.36-41
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    • 2023
  • A simple method was developed to determine residual p-arsanilic acid (ASA), an organo-arsenic compound used as a feed additive, in aquatic products (eel, halibut, and shrimp) using EDTA-assisted solvent extraction and LC-MRM. The method was successfully validated in terms of specificity, linearity (coefficient of determination ≥ 0.995), accuracy (recovery or R, 72.72-78.73%), precision (the relative standard deviation of R, 2.08-6.98%), and sensitivity (the lower limit of quantitation, 5 ppb) according to CODEX guidelines (CAC-GL 71-2009). The use of EDTA in the extraction solvent and water with a suitable pH modifier as the reconstitution solvent may be the key factors for successful results. This is the first method that can be used for monitoring residual ASA in aquatic products using LC-MRM and could contribute to establishing a better aquatic product safety management system.

Development of a diagnostic coronagraph on the ISS: BITSE overview and progress report

  • Kim, Yeon-Han;Choi, Seonghwan;Bong, Su-Chan;Cho, Kyungsuk;Park, Young-Deuk;Newmark, Jeffrey;Gopalswamy, Nat.;Yashiro, Seiji;Reginald, Nelson
    • The Bulletin of The Korean Astronomical Society
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    • v.44 no.2
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    • pp.56.4-56.4
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    • 2019
  • The Korea Astronomy and Space Science Institute (KASI) has been collaborating with the NASA's Goddard Space Flight Center, to install a coronagraph on the International Space Station (ISS). The coronagraph will utilize spectral information to simultaneously measure electron density, temperature, and velocity. As a first step, we developed a new coronagraph and launched it on a stratospheric balloon in 2019 (BITSE) from Fort Sumner, New Mexico in USA. As the next step, the coronagraph will be be further developed, installed and operate on the ISS (CODEX) in 2022 to address a number of important questions (e.g., source and acceleration of solar wind, and coronal heating) in the physics of the solar corona and the heliosphere. Recently, BITSE has been launched at Fort Sumner, New Mexico. In this presentation, we will introduce the BITSE mission and discuss recent progress.

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Development of a diagnostic coronagraph on the ISS: progress report

  • Kim, Yeon-Han;Choi, Seonghwan;Bong, Su-Chan;Cho, Kyungsuk;Park, Young-Deuk;Newmark, Jeffrey;Gopalswamy, Nat.;Yashiro, Seiji;Reginald, Nelson
    • The Bulletin of The Korean Astronomical Society
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    • v.45 no.1
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    • pp.44.2-44.2
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    • 2020
  • The Korea Astronomy and Space Science Institute (KASI) has been collaborating with the NASA Goddard Space Flight Center (GSFC), to install a diagnostic coronagraph on the International Space Station (ISS). The coronagraph is designed to obtain simultaneous measurements of electron density, temperature, and velocity using multiple filters in the 3-10 Rs range. In 2019, we developed a new coronagraph and launched it on a stratospheric balloon (BITSE) from Fort Sumner, New Mexico in USA. As the next step, the coronagraph will be further developed, installed and operated on the ISS (CODEX) in 2023 to understand the physical conditions in the solar wind acceleration region, and enable and validate the next generation space weather models. In this presentation, we will report recent progress and introduce future plan.

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Monitoring of Lead and Cadmium Contents of Vegetables in Korea (국내 유통 중인 채소류의 납, 카드뮴 함량 모니터링)

  • Shim, Jee-Youn;Oh, Hyun-Suk;Jang, Mi-Ran;Lee, Yoon-Ae;Lee, Ryun-Kyung;Kim, Min-A;Lee, Hyo-Jung;Lee, Sang-Min;Cho, Tae-Youg
    • Journal of Food Hygiene and Safety
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    • v.25 no.4
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    • pp.395-401
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    • 2010
  • This research was carried out as a survey on the contents of Lead (Pb) and Cadmium (Cd) in 5 type agricultural products unestablished safety guideline in Korea. The average levels of Pb: onion 0.010 mg/kg, cucumber 0.018 mg/kg, garlic 0.012 mg/kg, green pepper 0.027 mg/kg, sesame 0.029 mg/kg. The average levels of Cd: onion 0.006 mg/kg, cucumber 0.002 mg/kg, garlic 0.008 mg/kg, green pepper 0.011 mg/kg, sesame 0.024 mg/kg. The present result of this study showed that Pb and Cd contents in the whole samples were less than the maximum residual levels of the codex standard. The levels of exposure assessment for Pb and Cd by intake from vegetables and sesame were merely at $1.3{\times}10^{-4}$(mean) ~ $5.1{\times}10^{-4}$($95^{th}$ percentiles) ${\mu}$g/kg bw/day for Pb, $7.5{\times}10^{-5}$(mean) ~ $3.6{\times}10^{-4}$($95^{th}$ percentiles) ${\mu$}g/kg bw/day for Cd. The data from this research will be valuable source for database construction for science-based safety control and management for the trace metal contamination in food including agricultural products.

Determination of Carazolol and Azaperone in Livestock and Fishery Products Using Liquid Chromatography-tandem Mass Spectrometry (축수산물에서 LC-MS/MS를 이용한 카라졸롤 및 아자페론 분석)

  • Choi, Soo Yeon;Kang, Hui-Seung;Kim, Joohye;Cheon, So-Young;Jeong, Jiyoon;Cho, Byung-Hoon;Lee, Kang-Bong
    • Journal of Food Hygiene and Safety
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    • v.33 no.3
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    • pp.176-184
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    • 2018
  • The aim of the present work was to develop simultaneous methods of quantification of carazolol, azaperone, and azaperol residues in livestock and fishery products using liquid chromatography-tandem mass spectrometry (LC-MS/MS). Samples were extracted from beef, pork, chicken, egg, milk and shrimp using acetonitrile (ACN); while flat fish and eel were extracted using 80% ACN. For purification, ACN saturated n-hexane was used to remove fat composition. The standard calibration curves showed good linearity as correlation coefficients; $r^2$ was > 0.99. Average recoveries expressed were within the range of 67.9-105% for samples fortified at three different levels ($0.5{\times}MRL$, $1{\times}MRL$ and $2{\times}MRL$). The correlation coefficient expressed as precision was within the range of 0.55-7.93%. The limit of quantification (LOQ) was 0.0002-0.002 mg/kg. The proposed analytical method showed high accuracy and acceptable sensitivity based on Codex guideline requirements (CAC/GL71-2009). This method can be used to analyze the residue of carazolol, azaperone, and azaperol in livestock and fishery products.

Monitoring and Risk Assessment of Cadmium and Lead in Agricultural Products (국내 농산물의 카드뮴 및 납 함량 조사 및 위해 평가)

  • Kim, Ji-Young;Choi, Nam-Geun;Yoo, Ji-Hyock;Lee, Ji-Ho;Lee, Young-Gu;Jo, Kyoung-Kyu;Lee, Cheol-Ho;Hong, Su-Myeong;Im, Geon-Jae;Hong, Moo-Ki;Kim, Won-Il
    • Korean Journal of Environmental Agriculture
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    • v.30 no.3
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    • pp.330-338
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    • 2011
  • BACKGROUND: This study was conducted to investigate the agricultural product (Pulses, Lettuces, Pumpkins, Apples, Pears and Tangerines) in Korea, monitoring of cadmium (Cd) and lead (Pb) contaminations of agricultural products in cultivated areas and abandoned mine areas were investigated, and risk assessment was performed through dietary intake of agricultural products. METHODS AND RESULTS: The average contents of Cd and Pb ranged from 0.001 to 0.018 mg/kg and from 0.007 to 0.032 mg/kg respectively. The result was showed that contents of Cd and Pb did not exceed maximum residual levels established by CODEX except pumpkins and apples. The average daily intake were in the range of $1.06{\times}10^{-3}$ to $4.76{\times}10^{-2}{\mu}g/kg$ b.w./day at the mean and 95th percentile for Cd, $4.53{\times}10^{-3}$ to $8.35{\times}10^{-2}{\mu}g/kg$ b.w./day at the mean and 95th percentile for Pb for general population, based on the Korean public nutrition report 2008. The Hazard Index (HI) from the ratio analysis between daily exposure and safety level values was smaller than 1.0. CONCLUSION(s): This results demonstrated that human exposure to Cd and Pb through dietary intake of agricultural produces from abandoned mine areas might not cause adverse effect exceeding to those from non-contaminated areas.

Development of an Official Analytical Method for Determination of Imazapyr in Agricultural Commodities using HPLC-UVD (HPLC-UVD를 이용한 농산물 중 Imazapyr의 공정분석법 확립)

  • Jang, Jin;Kim, Heejung;Ko, Ah-Young;Lee, Eun-Hyang;Joo, Yoon Ji;Kim, Jinhong;Chang, Moon-Ik;Rhee, Gyu-Seek
    • The Korean Journal of Pesticide Science
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    • v.19 no.1
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    • pp.5-13
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    • 2015
  • A chromatographic method for the determination of imazapyr, a non-selective herbicide, in agricultural commodities was developed to use safety control of pesticide residue on crops, and was fully validated as an official method for residue analysis. Agricultural commodities, mandarin (fruit), hulled rice (cereal grains), pepper (vegetables), potato (potatoes) and soybean (beans) were extracted with methanol and partitioned with dichloromethane to remove the interference obtained from sample extracts, adjusting pH to 2.5 by 4N hydrochloric acid. Finally, they were analyzed by high performance liquid chromatography coupled to UV detector (HPLC-UVD). The developed method had the linearity in the range of test concentrations with coefficients of determination ($r^2$) more than 0.99. Recovery studies were carried out at three concentration levels (LOQ, 10LOQ, and 50LOQ) performing five replicates at each level. Recoveries were ranged between 72.1 to 108.0%, with relative standard deviations less than 10%. A consistent recovery was determined according to the CODEX guidelines (CAC/GL40, 2003). Finally, LC/MS with selected ion monitoring was also applied to confirm the suspected residues of imazapyr in agricultural samples. This developed method for determination of imazapyr residues in agricultural commodities. can be used as an official method.

Study on the Vitamin Contents of Commercial Powdered Infant Formula (국내 시판 유아용 고형 조제분유의 비타민 함량에 관한 조사)

  • Bae, Hae-Jin;Jun, Mi-Ra;Kim, Young-Gil
    • Journal of Life Science
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    • v.17 no.12
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    • pp.1689-1694
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    • 2007
  • This study was conducted to investigate both fat-soluble and water-soluble vitamin contents of commercial powdered infant formula for obtaining basic data on infant nutrition. Ten commercial infant formula based on cow's milk were collected and the contents of fat-soluble vitamins (vitamin A, D, E, K) and water-soluble vitamins (vitamin C, thiamin, riboflavin, niacin, $B_6$, folate, $B_{12}$, pantothenic acid, biotin) were compared with Dietary Reference Intakes for Koreans (KDRIs). The overall vitamin contents in 100 g and in 100 kcal of infant formula satisfied the recommended formula regulation (KDRIs) and Codex. In infant formula during 0-5 monthly age, fat-soluble vitamin A, D, E, K could supply 178.6%, 205.3%, 208.4%, 976.3% of adequate daily vitamin intakes, respectively. Water soluble vitamins, vitamin C, thiamin, riboflavin, niacin, $B_6$, folate, $B_{12}$, pantothenic acid, biotin could supply 173.2%, 237.2%, 269.8%, 295.9%, 431.6%, 165.8%, 1186.3%, 203.8%, 408.3% of adequate daily vitamin intakes, respectively. In infant formula during 6-11 monthly age, all vitamins satisfied their adequate daily intakes as well. Vitamin A, D, E, K supplied 199.2%, 262.3%, 220.5%, 626.46% of adequate daily vitamin intakes. Vitamin C, thiamin, riboflavin, niacin, $B_6$, folate, $B_{12}$, pantothenic acid, biotin could supply 179.5%, 210.2%, 264.7%, 241.5%, 206.0%, 166.9%, 699.5%, 247.0%, 475.0% of adequate intake of KDRIs. From this study, evaluation of vitamin contents of commercial infant formula was established, which could strengthen the basic information on infant nutrition.