• 제목/요약/키워드: Capillary method

검색결과 503건 처리시간 0.025초

Pressure Bomb법을 이용한 섬유방향 액체투과성 측정 (Measurement of Longitudinal Liquid Permeability Using Pressure Bomb Method)

  • 허종윤;강호양
    • Journal of the Korean Wood Science and Technology
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    • 제25권3호
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    • pp.66-74
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    • 1997
  • Liquid permeabilities of red oak and several softwoods were measured by the pressure bomb method and a modified liquid permeability method in order to investigate their efficacy. The effect of preboiling and prefreezing on wood permeability were also examined for both green and resaturated specimens. Regardless of some disadvantages these two methods were revealed as a handy tool for quick evaluation of the permeability of an unknown species. The permeabilities of the resaturated specimens increased when preboiled. but decreased when prefrozen. For green specimens, however, pre freezing increased permeability. The discrepancy of the pre freezing effect on two specimens partially attributes to their difference of initial permeabilities. For all species except radiata pine heartwood, the radii of the effective capillary pores, derived from the water potential equation, distribute from $0.42{\mu}m$ to $7.2{\mu}m$. Those of radiata pine heartwood are below $0.46{\mu}m$.

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Biological Monitoring of Human Exposure to Volatile Halogenated Hydrocarbons Using Urinalysis with Capillary GC-ECD

  • Jung, Won-Tae;Sohn, Dong-Hun
    • Archives of Pharmacal Research
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    • 제15권2호
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    • pp.109-114
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    • 1992
  • For the risk assessment of human exposure to volatile halogenated hydrocarbons, a dynamic purge trap/on-column cryofocusing method using capillary gas chromatograph-$^{63}Ni$ electron capture detector and thermal desorption unit was applied to analyze the free forms, metabolites of 1, 1, 2-trichloroethylene and 1, 1, 2, 2-tetrachloroethylene. The urine sample was diluted with distilled water, hydrolyzed and sealed. Then the inert gas was infused to purge out free 1, 1, 2-trichloroethylene, free 1, 1, 2, 2-tetrachloroethylene and urichloroethanol. These compounds were trapped to $Tenax^R$ / GC-gas trap device throughout clean up tube. Being undertectable to gas chromatograph directly, trichloroacetic acid was methyl esterificated and trapped in the manner above mentioned. The optimal incubation time to get best recovery of methyl ester was 4 hours at $60^circ$C. The concentrations of free volatile halogenated hydrocarbons and their metabolites in urine were obtained of free volatile halogenated hydrocarbons and their metabolites in urine were obtained from 5 healthy volunteers. This analytical method is expected to make the biological monitoring more precise and convenient.

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충전컬럼 및 모세관컬럼 가스크로마토그라프에 의한 마요네즈 중의 스테롤 분석연구 (Studies on Analysis of Sterols in Mayonnaise by GLC with Packed and Capillary Column)

  • 김현위;정소영;정창기;윤형식;박기문;안평욱;최춘언
    • 한국식품과학회지
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    • 제24권1호
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    • pp.82-85
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    • 1992
  • 가스크로마토그라프법으로 마요네즈 중의 스테롤을 정량하는데 있어서 충전컬럼과 모세관 컬럼을 사용하여 비교 연구하였다. 두 컬럼의 경우 4종의 스테롤(cholesterol, campesterol, stigmasterol, ${\beta}-sitosterol$)이 모두 뚜렷히 분리되었으나 모세관 컬럼이 신속성, 재현성, 분리능 면에서 우수하였다. 한편, 제품에 적용하여 분석한 결과, 측정된 cholesterol 함량으로부터 추정한 시판 마요네즈 난황사용량은 충전컬럼의 경우 $2.69{\sim}7.11%$, 모세관 컬럼의 경우 $2.42{\sim}6.08%$ 범위이었으며, 스테롤 조성으로부터 마요네즈 제조에 사용된 식용유는 대두유 및 면실유임을 알 수 있었다.

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양액공급방법이 수경재배 멜론의 생육에 미치는 영향 (Effect of Nutrient Supply Methods on the Growth of Hydroponically Grown Melon)

  • 김성배;장전익
    • 생물환경조절학회지
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    • 제13권3호
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    • pp.125-129
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    • 2004
  • 모관 양액 공급시스템을 이용한 수경 재배 시 공급시스템의 효율성을 검증하고 제주 송이와 펄라이트 혼합배지에서의 멜론 및 엽채류의 생육특성을 구명코자하였다. 모관 양액 공급 시스템에서의 네트 멜론의 품종별 생육 및 과실 특성은 양호하였으며, 과중은 일반재배에서의 국ㆍ내 상품기준인 1과당 1.8~2.0kg과 비슷한 경향을 보였다. 무네트형 멜론인 아리스 품종은 급액 방법에 따라 과실 특성의 차이는 없었으나 당도에 있어서는 점적 및 모관 시스템에서 15.6과 $15.5^{\circ}$Brix로 분무 시스템의 $14.4^{\circ}$Brix보다 높았다. 네트형 멜론인 얼스엘리트 품종에서는 분무시스템보다 점적 및 모관시스템에서 과실 특성이 양호하였으며 당도도 높은 경향이었다. 멜론 재배 전ㆍ후 배지내 pH의 변화는 시스템별로 차이가 없었으나 하층부보다는 상층부에서 pH가 높게 나타났다. 배지내 무기성분 함량은 점적시스템에서 상층부보다 하층부에서 높았고, 모관시스템에서는 상층부에서 높은 경향이었다.

경사관법(傾斜管法)에 의한 우혈액(牛血液)의 적혈구침강율(赤血球沈降率) 측정(測定) (Angled Tube Method for Determining Erythrocyte Sedimentation Rate of Cattle)

  • 이방환;신종욱
    • 대한수의학회지
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    • 제26권1호
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    • pp.175-185
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    • 1986
  • The measurement of angled erythrocyte sedimentation rate (ESR), as a replacement for perpendicular ESR, for cattle blood was scrutinized since it has been well known that perpendicular ESR in cattle is too slow to be adopted as an effective clinical test. Samples of blood were taken from 186 Korean native cattle over 2 years old. The results obtained in the experiment were summarized as follows. 1. Average values of perpendicular ESR/24hrs in 15 apparently healthy cattle, as measured by Wintrobe, Westergren and capillary tubes, were $5.8{\pm}2.2$, $11.1{\pm}3.7$ and $10.4{\pm}4.5%$ respectively, which were found to be similar to the values of perpendicular ESR/hr of normal blood of human. 2. The ESR was determined in the tubes held at 90, 75, 60, 45, 30 and 15-degree angles, using 3 types of tubes. For the diagnostic purposes, the best results were obtained from the tubes held at 45-degree angle. 3. The angled ESR values increased as the diameters of the tube-bores decreased. 4. The tube length did not affect the angled ESR(%). 5. The angled ESR values increased with the increased environmental temperature during the ESR measurement. 6. The storage temperature at $5^{\circ}C$, $20^{\circ}C$ and $35^{\circ}C$, of the blood for 24 hours did not affect the angled ESR. 7. Samples of blood were treated with 4 kinds of anticoagulants (heparin, $K_2$-EDTA, double oxalate and sodium citrate) and the ESR was determined at 45-degree angle, using capillary hematocrit tubes. The ESR values were higher in the blood samples treated with sodium citrate than in those treated with other anticoagulants. 8. By using the autologous plasma, the PCV was adjusted to be 5, 10, 20, 30, 40 and 50ml/100ml and the ESR was determined in the capillary hematocrit and Wintrobe tubes held at 45 degrees. In both of the methods the ESRs increased as the values of PCV decreased. The regressions of ESR to PCV in both 45-degree-angled capillary and Wintrobe tubes were curvilinear. For the capillary hematocrit tubes the second degree polynomial $Y=61.9779-2.3533x+0.0228x^2$ (r=0.9999) fits the data. And in the case of Wintrobe tubes the second degree polynomial $Y=27.9767-1.1314x-0.0117x^2$ (r=0.9998) fits the data. 9. The 45-degree angled ESR was determined in the blood of 71 healthy Korean native cows using capillary hematocrit tubes. The average PCV was $35.4{\pm}3.6ml/100ml$. The observed ESR/hr averaged $7.2{\pm}2.7%$, while the corrected ESR/hr to a PCV of 36ml/100ml averaged $6.6{\pm}1.3%$. From these results it was concluded that to obtain the best results the ESR/hr of Korean native cattle should be determined at 45-degree angle at room temperature($20^{\circ}C$) using capillary hematocrit tubes.

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마이크로/나노 계층구조 형성법 및 응용 (Fabrication of micro/nanoscale hierarchical structures and its application)

  • 정훈의;곽노균;이승석;서갑양
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2007년도 춘계학술대회A
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    • pp.426-428
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    • 2007
  • A simple method is presented for fabricating micro/nanoscale combined hierarchical structures using a two-step UV-assisted capillary molding technique. This lithographic method consists of two steps: (i) fabrication of partially cured polymer microstructures using a PDMS mold and (ii) subsequent nanofabrication using a high-resolution polyurethane acrylate (PUA) mold on top of the pre-formed microstructures. Using this technique, various micro/nano hierarchical structures were fabricated with minimum resolution down to 70 nm over a large area with very good reproducibility.

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액체 필름 끝단에서의 유동특성에 관한 수치연구 (Blob and Wave Formation at the Free Edge of an Initially Stationary fluid Sheet)

  • 송무석;안자일
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2002년도 학술대회지
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    • pp.307-310
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    • 2002
  • A two-dimensional numerical method for inviscid two-fluid flows with evolution of density interface is developed, and an initially stationary two-dimensional fluid sheet surrounded by another fluid is studied. The Interface between two fluids is modeled as a vertex sheet, and the flow field u÷th the evolution of interface is solved by using vortex-in-cell/front-tracking method. The edge of the sheet Is pulled back into the sheet due to surface tension and a blob is formed at the edge. This blob and fluid sheet are connected by a thin neck. In the inviscid limit, such process of the blob and neck formation is examined in detail and their kinematic characteristics are summarized with dimensionless parameters. The edge recedes at $V=1.06({\sigma}/{\rho}h)^{0.5}$ and the capillary wave Propagating into the fluid sheet must be considered for bettor understanding of the edge receding.

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Flow Behavior at the Embossing Stage of Nanoimprint Lithography

  • Jeong, Jun-Ho;Park, Youn-Suk;Shin, Young-Jae;Lee, Jae-Jong;Park, Kyoung-Taik
    • Fibers and Polymers
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    • 제3권3호
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    • pp.113-119
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    • 2002
  • Nanoimprint lithography (NIL) is a nanofabrication method known to be a low cost method of fabricating nanoscale patterns as small as 6 m. This study is focused on understanding physical phenomena in the embossing of nano/micro scale structures with 100 nm minimum feature size. We present the effects of capillary force and width of stamp groove on flow behavior at the embossing stage through numerical experimentation. We also compare our numerical results with previous experimental results and discuss our results.

$LaCl_3-NaCl$ 2성분계 용융염의 점도 (Viscosities of $LaCl_3-NaCl$ Binary Melts)

  • 김기호
    • 한국표면공학회지
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    • 제39권6호
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    • pp.282-287
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    • 2006
  • Viscosities of $LaCl_3-NaCl$ binary melts were measured by the capillary method over the range of their liquidus temperatures to about 1200K. The cell constant were determined by using pure water. The results obtained are summerized as follows: Viscosities were decreased with the content of NaCl for all over the composition range of binary melts. Composition - viscosity relation for the binary melts show a non-linear from the additivity line and the deviations shows a maximum at about 60 mol% NaCl. This suggests the existence of the complex ion of $LaCl_4^-$ in the melt. Activation energy for viscous flow of the binary melts decrease monotonously with the increasing content of NaCl.

Optimization of Composite MIM Feedstock Rheological Behaviour by Experimental Analysis

  • Chen, Chih-Cherng;Wu, Chi-Wen;Yen, Chih-Ming
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.495-496
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    • 2006
  • The kneading process and formulations of feedstock obviously affect the quality of MIM products. In the present work, the rheological behaviour of the composite MIM feedstock, metal matrix (Cu) with few additions of ceramic powders $(Al_2O_3)$, was measured by a self-designed/manufactured simple capillary rheometer. Experimental results show that the distribution between powders and binder is more uniformly when blending time increased. Though high powder loading will increase the feedstock viscosity, the fluidity reveals relatively stable through the load curves of extrusion. Besides, the temperature-dependence of viscosity of the feedstock approximately follows an Arrehnius equation. Basing on Taguchi's method, the kneading optimization conditions and the rheological model of the feedstock were established, respectively.

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