• The Journal of the Petrological Society of Korea
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• v.23 no.3
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• pp.187-195
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• 2014

In this paper, we report new OSL ages of the marine terrace sediments at Suryum fault site, using single grains of quartz, and briefly discuss their chronological implications on the timing of terrace formation along the southeastern coast of Korea. Of 1200 grains measured, 93 quartz grains were found to have OSL properties suitable for dating, the equivalent dose ($D_e$) values of which varied significantly, ranging from 50 Gy to 610 Gy with the overdispersion of $30{\pm}4%$. Applied to the Central Age Model (CAM) and Minimum Age Model (MAM), these quartz grains showed the OSL ages of $83{\pm}4ka$ and $60^{+3}{_{-7}}ka$, respectively, both of which are stratigraphically inconsistent with the previously reported OSL ages of lower $2^{nd}$ terrace (MIS 5a; ~80 ka). However, Finite Mixture Model (FMM) revealed that a small fraction of the measured quartz grains ($6{\pm}4%$) were of the ages ($194{\pm}24ka$) corresponding to MIS 7. Conclusively, based on single grain OSL ages, it would be prudent not to exclude the possibility that the marine terrace sediments at Suryum fault site have formed during MIS 7. Further, our single grain OSL ages imply that multiple grain(single aliquot) OSL dating methods are not applicable to the marine sediments at Suryum fault site.

• The Sea:JOURNAL OF THE KOREAN SOCIETY OF OCEANOGRAPHY
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• v.4 no.3
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• pp.180-187
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• 1999

Radiocarbon dating method using benzene liquid scintillation was performed on the oyster shell fragments which producted from the shell mounts at Hadong Mogdori in Kyeongsangnamdo. This paper described to the age dating method and compared to the result. The carbon in sample is synthesized to a benzene through the sample preparation, $SrCO_3$, $SrC_2$, $C_2H_2$ and $C_6H_6$ synthesizing process. Age dating is calculated by Wallac 1415 Liquid Scintillation Counter. The result of age dating is estimated to be $4905{\pm}112$ yr BP in Yosu Univ. which is a good agreement with the result in Shimane Univ. ($4912{\pm}123$ yr BP). Radiocarbon dating method using benzene liquid scintillation is a simple and economical in operation and establishment, it has a potential instrumentation in the university and research institute.

• Nuclear Engineering and Technology
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• v.15 no.1
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• pp.23-32
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• 1983

In the previous studies on Rb-Sr geochronology, Gyeonggi Massif was known as the oldest rock in Korea Peninsula but the detailed sequence of geochronology was not studied yet. In the present study, some of whole rock isochrons considered here can be geochronologically grouped as follows: The ages of leucocratic gneisses at Yangpyeong, and augen and banded gneisses at Anyang show 2200 to 2300 m.y. which may represent the time of the Massif formation or an igneous intrusion. The age of the granite gneiss distributed in Yangpyeong area shows about 1400 m.y., which apparently represents the intrusion time of the gneiss. The age of the extremely altered metamorphic rock shows about 500 m.y., which may represent the time of a Caledonian orogenic event probably with hydrothermal activities. The other episodic ages of 800 to 900 m.y. which was widely observed through the Massif, may represent the ages of Precambrian igneous activities or regional metamorphism in the Massif. It seems to be reasonable that the ages of 120 to 270 m.y. show the times of Mesozoic and Late Palaeozoic Plutonisms in the Massif.

• Journal of Radiation Protection and Research
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• v.36 no.2
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• pp.52-58
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• 2011

OSL dating for three hearths having the sequence of use and discard in No. 29 and 29-1 dwelling sites at Sogol cultural site was carried out. Resulting from the deconvolution of natural CW-OSL decay curve and thermal zeroing test, it was turned out that OSL signal was entirely composed of the heat- and light-sensitive fast component with high photoionization cross-section and all quartz OSL signals were thermally bleached under $300^{\circ}C$ which is the minimum temperature related to heating and cooking in Bronze age. After dose recovery test and plateau test, paleodose of each hearth sample was evaluated by using SAR method, and OSL age was determined from the ratio of paleodose to annual dose rate. For the purpose of the precision improvement of OSL age, Bayesian statistics was applied to each hearth's age and the archaeological sequence information. Finally, it could be concluded to the accurate use period of each hearth from the resultant OSL ages.

• The Journal of the Petrological Society of Korea
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• v.10 no.3
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• pp.179-189
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• 2001

The determination of trace concentration of U, Th and Pb was carried out for chemical dating of zircon and monazite by electron microprobe. Detection limit and error range should be considered to measure characteristic X-rays of M-line from those minerals, which are low in the ionization of atom and low peak intensity in the spectrum. The element of U, Th and Pb were simultaneously measured with 3 spectrometers equipped with PET crystal to reduce a total counting time and error due to drift of instrumental operating condition. Detection limit could be improved from increase of the peak/background ratio through adjusting pulse height analyzer about 1000 mv baseline. Under permissible maximum analytical conditions, theoretical detection limit of U, Th and Pb is down to 30 ppm (99% confidence level). The analytical result was maintained at a relative error $\pm$10% ($2{\sigma}$) in 800 ppm Pb, $\pm$5% ($2{\sigma}$) in 2330 ppm U and $\pm$10% ($2{\sigma}$) in dating from a single measurement of zircon at 15 keV and 100 nA. However, for the precise dating of zircon and monazite, if it is considered a 3 $\mu\textrm{m}$ spatial resolution, <100 ppm ($3{\sigma}$) detection limit and <$\pm$10% ($2{\sigma}$) relative error, optimum analytical conditions are given as 15~20 keV accelerating voltage, 100~200 nA beam current and 300~1200 sec total counting time. To reduce material damage by high current, there is need to be up to 3~5 $\mu\textrm{m}$ of electron beam diameter, or to use arithmetic average of multiple measuring at a shorter counting time. A younger or relatively low concentration rocks can be dated chemically by lower detection limit and improved precision resulted from increase of current and measuring time.

• The Journal of the Petrological Society of Korea
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• v.26 no.1
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• pp.1-11
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• 2017

We have dated the K-Ar, Ar-Ar and U-Pb ages of the Masan hornblende-biotite granite in the southern Cretaceous Gyeongsang basin to constrain its emplacement age. The ~108 Ma hornblende K-Ar age obtained in the study is similar to the previously reported Rb-Sr age. However, the single grain total fusion $^{40}Ar/^{39}Ar$ dating on hornblende failed to yield statistically meaningful ages because the isotopic system was open during its alteration. Thus the hornblende K-Ar age in the study is also unlikely to be reliable. The single grain total fusion $^{40}Ar/^{39}Ar$ dating on biotite yielded an average age of $75.8{\pm}3.0Ma$. Apart from scattered data in the range of ~45-75 Ma, the average age increased to ~80 Ma. The SHRIMP and LA-MC-ICPMS U-Pb isotopic compositions of zircon from the Masan hornblende-biotite granite yielded its emplacement age as $87.6{\pm}2.7Ma$ and $86.8{\pm}0.4Ma$, respectively. It is thus likely that the ~80 Ma $^{40}Ar/^{39}Ar$ age of biotite might reflect the cooling age of Masan hornblende-biotite granite or the thermal influences from later intense igneous activities in the Gyeongsang basin.

• Economic and Environmental Geology
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• v.56 no.2
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• pp.115-123
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• 2023

We introduce a new 'image-mapping' in-situ U-Pb dating method using LA-ICP-MS, proposed by Drost et al. (2018), and show the characteristics and usability of this method through several examples of absolute age results determined by first applying it to samples from the Joseon Supergroup of the Early Paleozoic Era in Korea. Unlike the previous in-situ spot analysis, this in-situ U-Pb dating method for carbonate minerals can determine the absolute age with high reliability by applying the 'image-mapping' method of micro-sized domains based on micro-textural observation, as well as determine the absolute age of multiple geological 'events' that occurred after deposition. This was confirmed in the case of determining the syn-depositional age and the multiple post-depositional ages from carbonate minerals of the Makgol and the Daegi Formations. Therefore, if the 'image-mapping' in-situ U-Pb dating method is applied to determine the absolute age of various types of carbonate minerals that exist in various geological environments throughout the geologic era, it will be possible to secure new geological age information.

• Journal of Conservation Science
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• v.28 no.3
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• pp.185-192
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• 2012

Issues of chronology on archaeological remains or relics have been a storm-center of controversy when various archaeological researches have been done. Sometimes there is a limit for figuring out issues of chronology by archaeological research. In that case, the field of natural science is often needed to work out issues of chronology. Among various subjects in natural science, archaeomagnetism plays an important role in dating archaeological remains for baked earth bearing relics. In particular, archaeomagnetism is of use for sites where directly excavated dating proxy is unavailable. Terrestrial magnetism changes along with the passage of time and leaves trace by many kinds of residual magnetization which could be called fossil of terrestrial magnetism. Archaeomagnetic dating method is used to assign a date to the archaeological remains in which baked earth is found by measuring the changes of terrestrial magnetism through the thermal remanent magnetization retained in baked earth. This study aims to constrain the age of fire at Buinsa, Daege, Korea using 27 samples that were collected from a layer of baked earth. Buinsa is famous for the place where kept the first edition of Tripitaka Koreana, which was lost in fire at the second invasion of mongolia. In addition, there is a record that there was revolt around this region in A.D.1203. According to archaeomagnetic dating, ages of A.D.1150~1200 and A.D.1130~1210 were assigned for the two building sites in Buinsa, respectively. To this end, it can be concluded that the layer of baked earth on the two building sites in Buinsa recorded the vestige of fire caused by revolt.

• Economic and Environmental Geology
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• v.53 no.6
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• pp.645-654
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• 2020

We present the K-Ar age dating results of <0.1㎛ fraction of the selected fault rocks from the Yangsan fault in the Yeonghae area. Based on the mineralogical characterization, the <0.1㎛ fractions were mostly composed of 1Md illite polytype, or I-S interstratified mineral, which should be formed by fault activation. Therefore, we determined the timings of fault activation events by analyzing K-Ar age-dating for the <0.1㎛ fractions. Accordingly, the activation timings of Yangsan Fault in the Yeonghae area were determined as 45.5±1.1 Ma, 50.9±1.2 Ma, 58.2±1.3 Ma, 60.8±1.4 Ma, 65.3±1.6 Ma, 66.8±1.5 Ma, 67.1±1.5 Ma, and 75.1±1.7 Ma. These results indicate that at least 5-times of major fault events occurred in the Yangsan fault from late Mesozoic to Cenozoic Era. In the outcrop, age dating results tend to be younger age from the location of the oldest sample(75.1±1.7 Ma) toward to the both sides. From the results, it suggests that the fault activation extends from the location of oldest age saple to both sides. This geochronological research of the multiple fault activation ages for the Yangsan Fault will provide crucial information for establishing the tectonic evolution model in the southeastern part of the Korean Peninsula.

• Journal of the Mineralogical Society of Korea
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• v.26 no.3
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• pp.161-174
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• 2013

The geology of the weondong deposit area consists mainly of Cambro-Ordovician and Carboniferous-Triassic formations, and intruded quartz porphyry and dyke. The skarn mineralized zone in the weondong deposit is the most prospective region for the useful W-mineral deposits. To determine the skarn-mineralization age, U-Pb SHRIMP and K-Ar age dating methods were employed. The U-Pb zircon ages of quartz porphyry intrusion (WD-A) and feldspar porphyry dyke (WD-B) are 79.37 Ma and 50.64 Ma. The K-Ar ages of coarse-grained crystalline phlogopite (WD-1), massive phlogopite (WDR-1), phlogopite coexisted with skarn minerals (WD-M), and vein type illite (WD-2) were determined as $49.1{\pm}1.1$ Ma, $49.2{\pm}1.2$ Ma, $49.9{\pm}3.6$ Ma, and $48.3{\pm}1.1$ Ma, respectively. And the ages of the high uranium zircon of hydrothermally altered quartz porphyry (WD-C) range from 59.7 to 38.7 Ma, which dependson zircon's textures affected by hydrothermal fluids. It is regarded as the effect of some hydrothermal events, which may precipitate and overgrow the high-U zircons, and happen the zircon's metamictization and dissolution-reprecipitation reactions. Based on the K-Ar age datings for the skarn minerals and field evidences, we suggest that the timing of W-skarn mineralization in weondong deposit may be about 50 Ma. However, for the accurate timing of skarn mineralization in this area, the additional researches about the sequence of superposition at the skarn minerals and geological relationship between skarn deposits and dyke should be needed in the future.