• Title/Summary/Keyword: Analytical-synthetic

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Analysis of synthetic Antimicrobials in Livestock Products by MSPD Method (MSPD법에 의한 축산물 중 합성항균제 동시분석)

  • 김재관;도영숙;박준조;황혜정
    • Journal of Food Hygiene and Safety
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    • v.13 no.4
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    • pp.344-354
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    • 1998
  • This study was conducted to evaluate the MSPD and HPLC method about simultaneous determination for residual synthetic antimicrobials of sixteen species such as sulfonamide etc. in livestock products. Elution solvent used in HPLC was ethylacetate:acetonitrile (4:1), and mobile phases for solvent A and B were water:methanol:acetonit rile:phosphric acid (700:250:50:0.2) and 100% acetonitrile respectively. The detector and absorbency used in HPLC was UV 266 nm. This study showed the reduction effect of 99.1% for organic solvents, 94% for experimental steps, 95% for analytical time and manpower and 98.9% for costs compared with korea food standard method. The average recovery rates for chicken, bovine, pork and milk were 67.7% 96.2%, 67.7%~96.6%, 70.0%~96.2%, and 13.8%~97.8%.

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Prediction of concrete spall damage under blast: Neural approach with synthetic data

  • Dauji, Saha
    • Computers and Concrete
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    • v.26 no.6
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    • pp.533-546
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    • 2020
  • The prediction of spall response of reinforced concrete members like columns and slabs have been attempted by earlier researchers with analytical solutions, as well as with empirical models developed from data generated from physical or numerical experiments, with different degrees of success. In this article, compared to the empirical models, more versatile and accurate models are developed based on model-free approach of artificial neural network (ANN). Synthetic data extracted from the results of numerical experiments from literature have been utilized for the purpose of training and testing of the ANN models. For two concrete members, namely, slabs and columns, different sets of ANN models were developed, each of which proved to have definite advantages over the corresponding empirical model reported in literature. In case of slabs, for all three categories of spall, the ANN model results were superior to the empirical models as evaluated by the various performance metrics, such as correlation, root mean square error, mean absolute error, maximum overestimation and maximum underestimation. The ANN models for each category of column spall could handle three variables together: namely, depth, spacing of longitudinal and transverse reinforcement, as contrasted to the empirical models that handled one variable at a time, and at the same time yielded comparable performance. The application of the ANN models for spall prediction of concrete slabs and columns developed in this study has been discussed along with their limitations.

Seismic linear analytical research on the mechanical effects of RC frame structure under the different column orientations

  • Mo Shi;Min-woo Choi;Yeol Choi;Sanggoo Kang
    • Architectural research
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    • v.26 no.3
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    • pp.83-92
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    • 2024
  • The profound impact of earthquakes on human lives and the built environment emphasizes the substantial human and economic losses result-ing from structural collapses. Many researchers in this field highlight the longstanding societal challenge posed by earthquakes and under-score the imperative to minimize such losses. Over the decades, researchers have dedicated efforts to seismic design, focusing on improv-ing structural performance to mitigate earthquake-induced damages. This has led to the development of various structural analysis methods. In this research, a specific RC frame structure (401 Bldg.) at Kyungpook National University that is designed for educational purposes, serves as a representative case. This research employs SAP 2000 for simulation, aiming to assess the structural performance under seismic condi-tions, focusing on evaluating the structural behavior under different column orientations. This research utilizes RSA (Response Spectrum Analysis) to comprehensively examine parameters of displacement, base shear force, base moment, joint radians, and story drift. Referring to the results from RSA, this research also assesses the structural performance using LTHA (Linear Time History Analysis) by conducting synthetic frequency domain and synthetic time domain analyses based on the seismic wave from the Kobe 1995 earthquake (Abeno). Based on the findings from the discussions, this research is expected to be a valuable reference for structural design within seismic resistance and the seismic reinforcement of existing RC frame structures.

The National of Proof and the Improvement of Proof Education - In the Perspective on the Philosophy of Mathematics - (증명의 수리철학적 분석과 지도 방향 탐색)

  • 나귀수
    • Journal of Educational Research in Mathematics
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    • v.8 no.1
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    • pp.351-364
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    • 1998
  • This thesis analyzes the nature of proof in the perspective on the philosophy of mathematics. such as absolutism, quasi-empiricism and social constructivism. And this thesis searches for the improvement of teaching proof in the light of the result of those analyses of the nature of proof. Though the analyses of the nature of proof in the perspective on the philosophy of mathematics, it is revealed that proof is a dynamic reasoning process unifying the way of analytical thought and the way of synthetical thought, and plays remarkably important roles such as justification, discovery and conviction. Hence we should teach proof as a dynamic reasoning process unifying the way of analytic thought and the way of synthetic thought, avoiding the mistake of dealing with proof as a unilaterally synthetic method. At the same time, we should make students have the needs of proof in a natural way by providing them with the contexts of both justification and discovery simultaneously. Finally, we should introduce the aspect of proof that can be represented as conviction, understanding, explanation and communication to school mathematics.

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Comparison of CE and HPLC as analytical methods of (-)-yatein enantiomer from Cupressaceae plants

  • Lim, Hwan-Mee;Kim, Young-Ho;Ahn, Byung-Zun;Kim, Kyeong-Ho;Kang, Jong-Seong
    • Proceedings of the PSK Conference
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    • 2002.10a
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    • pp.404.3-405
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    • 2002
  • Cupressaceae plants are used in traditional folk medicine. whose extracts have been found to possess some bioactivities. (-)-Yatein is a lignan of the dibenzyl-butyrolactone type. that has been isolated from some Cupressaceae plants. It was reported that (-)-yatein. isolated from plants. showed different activities from the synthetic yatein [3]. Hence. the enantiosetective determination of yatein from synthetic materials and natural products would be necessary. (omitted)

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Effective Material Properties of Composite Materials by Using a Numerical Homogenization Approach (균질화 접근법을 통한 복합재의 유효물성치 계산)

  • Anto, Anik Das;Cho, Hee Keun
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.18 no.12
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    • pp.28-37
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    • 2019
  • Due to their flexible tailoring qualities, composites have become fascinating materials for structural engineers. While the research area of fiber-reinforced composite materials was previously limited to synthetic materials, natural fibers have recently become the primary research focus as the best alternative to artificial fibers. The natural fibers are eco-friendly and relatively cheaper than synthetic fibers. The main concern of current research into natural fiber-reinforced composites is the prediction and enhancement of the effective material properties. In the present work, finite element analysis is used with a numerical homogenization approach to determine the effective material properties of jute fiber-reinforced epoxy composites with various volume fractions of fiber. The finite element analysis results for the jute fiber-reinforced epoxy composite are then compared with several well-known analytical models.

Effects of Ca/Si Molar Ratio on the Interatomic Distance of Synthetic Calcium Silicate Hydrate (C-S-H) at Elevated Temperature (고온 가열시 Ca/Si 몰비율에 따른 합성 칼슘 실리케이트 수화물(C-S-H)의 구성 원자간 거리 변화)

  • Im, Su-Min;Bae, Sung Chul
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2021.05a
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    • pp.144-145
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    • 2021
  • Calcium silicate hydrate(C-S-H) is the principal binding phase that controls the strength and thermal stability of concrete. However, the effects of high temperature on the lattice structure and interatomic structure of C-S-H remains poorly understood due to its nanocrystallinity. This study aims to elucidate the change in interatomic distance of synthetic C-S-H with different Ca/Si molar ratios after exposure to high temperature via high energy X-ray scattering experiment which is a powerful analytical tool for amorphous materials.

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A Basic Study on the Development of Logical Tool for Analyzing Spatial Organization of Housing (주거공간 분석도구의 개발에 관한 기초적 연구 - 공간구문론을 중심으로 -)

  • 이현정;박선경;하재명
    • Proceeding of Spring/Autumn Annual Conference of KHA
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    • 2000.11b
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    • pp.97-102
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    • 2000
  • The final purpose of this study is to develop the synthetic and logical analytical tool for analyzing spatial organization of housing. For this purpose, this study made the starting-point by proposing some alternatives to improve one of the quantitative analytical tools of spatial organizations, Space Syntax. These propositions were intended to consider human behavior as well as physical structure in analyzing spatial organization. The propositions were as follow; 1) Classify the private outdoor space in detail, 2) Consider that the spatial organization which visitors cognize can differ from which residents do, and 3) Use distinctive spatial depth according to the states of connection.

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Determination of Stability Constants Using Electrochemical Methods for the Complex Formation of Platinum and Palladium with Polyelectrolytes

  • Park, Joon Seo;Chung, Koo Soon
    • Analytical Science and Technology
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    • v.8 no.4
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    • pp.691-698
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    • 1995
  • The complexation of platinum and palladium with synthetic polyelectrolytes was studied. The successive and overall stability constants of Pd(II) with PEI and 2PVP were obtained by potentiometric titration. Because of the slow equilibrium time, the potentiometric titrations were performed using the home-made automatic titrator in order to analyze the complexations according to the modified Bjerrum method. The complex formation constant of Pt(IV) with 2PVP, measured by differential pulse polarography, was calculated from the peak currents that were obtained in non-complexing media and in solution containing 2PVP.

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Synthesis and structural analysis of chromium(III) picolinate complexes (Cr(III)-picolinate 착물의 합성과 구조분석에 관한 연구)

  • Kim, Sung-Il;Kang, Dae-Kyung;Cha, Ki-Won
    • Analytical Science and Technology
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    • v.16 no.1
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    • pp.25-31
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    • 2003
  • Chromium(III) picolinate, a highly bioavailable compound, is known to be used for supplementing essential chromium(III) to human beings and animals. Two different methods were used to synthesize chromium(III) picolinate. The synthetic products were characterized by elemental analysis, FTI-IR, high performance liquid chromatography (HPLC) and MALDI-MS.