• 한국철도학회논문집
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• 제13권2호
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• pp.131-138
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• 2010

최근에 철도의 고속화에 따라 차량의 경량화가 요구되기 때문에 알루미늄을 적용한 차량이 증가하고 있다. 알루미늄 차량의 차체는 대부분이 가스용접을 사용하였으나, 이 용접방법은 접합부의 기계적 성질이 모재에 비해 상당히 저하되는 경향이 있다. Hitachi, Bombardier 등의 철도 선진 제작사를 중심으로 가스용접에 비해 접합부의 기계적 성질이 우수한 마찰교반용접을 알루미늄 차체의 용접에 적용하고 있다. 본 논문에서는 철도차량에 사용되고 있는 A6005의 알루미늄 합금 압출재에 대하여 기존의 가스 용접방법인 GMAW와 새로운 용접방법인 마찰교반용접(FSW)을 적용한 경우에 접합부의 기계적 성질을 비교 분석하여 FSW가 GMAW에 비해 기계적 성질이 우수하다는 것을 확인하였다. 또한, FSW를 적용한 경우에 대해 용접 변수가 접합부의 기계적 성질에 미치는 영향을 민감도 분석을 통해 확인한 결과, 공구의 이송속도가 가장 큰 영향을 주는 용접 변수임을 알 수 있었다.

• 한국수산과학회지
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• 제11권3호
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• pp.139-146
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• 1978

The annual variations of some heavy metal concentrations, Al, Mn, Fe, Cu, Pb, Zn, Cd, Hg were determined on tile day of spring tides in every month from May 1977 to April 1978 at eight stations in the Nagdong River downstream. Samples were taken at intervals of one or two hours from 7 a.m. to 7 p.m. at each station. Annual ranges and means of concentrations of the heavy metals are as follows : aluminium 40.7-3700 ppb, 286 ppb; manganese 10.3-261.5 ppb, 80.8 ppb; iron ND-1237 ppb, 147.7 ppb; copper ND-30.9 ppb, 2.49 ppb; lead ND-29.9 ppb, 1.10 ppb; zinc ND-156.8 ppb, 5.61 ppb; cadmium ND-1.22 ppb, 0.09 ppb; mercury ND-0.37 ppb, 0.02 ppb respectively. In general, the contents of heavy metals except managanese and mercury were higher at the stations above station one, Kupo, though the ranges of the contents showed remarkable difference according to the sampling stations. Annual means of the concentrations of iron and manganese were exceeded already the desirable standards for industrial water and closed to the criteria of raw water for public supply. The values that over the criteria of raw water were sometimes found. Mercury concentration showed comparative high level such as ND-0.37 ppb in annual range but it was not over the environment criterion, 0.5 ppb. Aluminium, iron and mercury showed generally high values in summer period and other metals in winter period, through the patterns of seasonal variations were difference depending on the sampling stations and the kind of metals.

• 공업화학
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• 제9권2호
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• pp.177-184
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• 1998

분체 형태의 소수성 고분자 polymethylmethacrylate(PMMA), poly vinyl chloride(PVC)와 친수성 금속 aluminium에 대한 water, glycerol, formamide, diiodomethane, 1,1,2,2-tetrabromoethane, 1-bromonaphthalene, acetone, chloroform, benzene, ethanol과 methanol과의 접촉각을 Washburn식을 기본으로 한 wicking법으로 측정하였다. 또한, 농도에 따른 음이온 계면활성제 SDS(sodium dodecyl sulfate)와 양이온 계면활성제 CTAB(cetyl trimethylamonium bromide) 수용액과의 접촉각을 측정하였다. 유기액체들과의 측정된 접촉각으로부터 Zisman plot을 사용하여 임계표면장력, ${\gamma}_c$를 예측하였으며, 농도에 따른 계면활성제 SDS와 CTAB수용액과의 접촉각으로부터 adhesion tension plot을 사용하여 ${\gamma}_c$를 예측하였다. 유기액체, 계면활성제 SDS와 CTAB수용액에 대해서 분체 PMMA의 ${\gamma}_c$는 각각 43.5, 28.3과 $36.2mNm^{-1}$이며, 분체 PVC의 ${\gamma}_c$는 각각 44.2, 28.0과 $34.8mNm^{-1}$값을 얻었다. 이로부터, 고체 표면의 적심성과 성질이 계면활성제의 첨가에 의해 변화됨을 알 수 있었다. 또한, 측정된 접촉각으로부터 조화평균식을 사용하여 각 고체의 표면자유에너지. ${\gamma}_s$와 그 성분 값들을 결정하였다.

• Journal of Welding and Joining
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• 제13권3호
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• pp.134-146
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• 1995

Aluminium nitride(AlN) is currently under investigation as potential candidate for replacing alumium oxide(Al$_{2}$ $O_{3}$) as a substrate material for for electronic circuit packaging. Brazing of aluminium nitride(AlN) to Cu with Ag base active alloy containing Ti has been investigated in vacuum. Binary Ag$_{98}$ $Ti_{2}$(AT) and ternary At-1wt.%Al(ATA), AT-1wt.%Ni(ATN), AT-1wt.% Mn(ATM) alloys showed good wettability to AlN and led to the development of strong bond between brate alloy and AlN ceramic. The reaction between AlN and the melted brazing alloys resulted in the formation of continuous TiN layers at the AlN side iterface. This reaction layer was found to increase by increase by increasing brazing time and temperature for all filler metals. The bond strength, measured by 4-point bend test, was increased with bonding temperature and showed maximum value and then decreased with temperature. It might be concluded that optimum thickness of the reaction layer was existed for maximum bond strength. The joint brazed at 900.deg.C for 1800sec using binary AT alloy fractured at the maximum load of 35kgf which is the highest value measured in this work. The failure of this joint was initiated at the interface between AlN and TiN layer and then proceeded alternately through the interior of the reaction layer and AlN ceramic itself.

• Design & Manufacturing
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• 제11권3호
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• pp.19-24
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• 2017

In these days, increase requirement of TEM (Transmission Electro Microscope) in not only scientific field but also industrial field. Because TEM can measure inner-structure of specimen a variety of materials like metal, bio. etc. When use TEM, specimen should be thin about 50nm. So making for thin specimen, use Ion milling device that include specimen holder. The holder generally made of Aluminium Aluminium holder is worn away easily. For this reason, using time of ion milling with aluminum holder is too short. To solve the problem, we replace aluminium holer to molybdenum alloy holder. In this paper, we design molybdenum alloy holer for CAM and modify CAD modeling for effective machining process. So we array a specimen 3 by 4 and setup orientation for one-shot machining process. Next we make a CAM program for machining. we making a decision two machining strategy that chose condition of tool-path method, step-down, step-over. etc. And then conduct machining using CNC milling machining center. To make clear difference between case.1 and case.2, we fixed machining conditions like feed-rate, main spindle rpm, etc. After machining, we confirm the condition of workpiece and analysis the problems case by case. Finally, case.2 work piece that superior than case.1 cutting with WEDM because that method can not ant mechanical effect on workpiece.

• 한국세라믹학회지
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• 제35권9호
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• pp.923-932
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• 1998

Al2O3/Al composites were produced by displacement reaction method which was carried out by imm-ersing the sintered silica preform which was prepared form fused silica powder in molten aluminu. an ac-tivation energy of 94kJ/mole was calculated from Al-SiO2 reaction data in 1000-130$0^{\circ}C$ temperature range With increase of reaction temperature the alumina particle in the Al2O3/Al composites produced with pur metal Al showed grain growth and the growth of alumina particle in Al2O3/Al composite produced by using of Mg contained Al alloy was inhibited. The flexural strength of Al2O3/Al composites produced at 100$0^{\circ}C$ showed the highest value as 393 MPa. Flexural strength of the composite fabricated at 85$0^{\circ}C$ showed higher deviation than that of the composite produced at above 100$0^{\circ}C$ Low flexural strength of the composite fa-bricated at 120$0^{\circ}C$ due to the growth of pore and alumina particle size. The hardness of composites de-pended on alumina content in Al2O3/Al composite decreased with increasing of aluminium content in case the same alumina content and increased with increasing of silicon content in composite.

• 한국분말재료학회지
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• 제9권1호
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• pp.25-31
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• 2002

The efects of mechanical aloying conditions and the type of reducing agent on the solid state reductionof haematite $Fe_2O_3$ have been investigated at room temperature. Aluminium titanium zinc and copper were used as reducing agent. Nanocomposites of metal-oxide in which oxide particles with nano size were dispersed in Fe matrix were obtained by mechanical alloying of $Fe_2O_3$ with aluminium and titanium respectively However the reduction of $Fe_2O_3$ by coppe was not occurred Composite materials of iron with $Al_2O_3$ and $TiO_2$ were obtained from the system of $Fe_2O_3-Al$ and $Fe_2O_3-Ti$ after ball milling for 20 hrs and 30 hrs respectively. And the system of $Fe_2O_3-Zn$ resulted in the formationof FeO with ZnO after ball milling of 120 hrs. The final grain sizes of iron estimated by X-ray diffraction line-width measurement were in the ranges of 24~33 nm.

• International Journal of Advanced Culture Technology
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• 제3권1호
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• pp.138-144
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• 2015

This paper is aimed to study the influence of aluminium dross from Thai aluminum casting factory on polypropylene matrix-polymer composite material properties. The summarized experimental results are as follows. An increase in the amount of aluminum dross polymer composite material affected to increase hardness, modulus of elasticity and abrasion resistance. However, the increase of the aluminum dross had no effects to change the yield strength and the melting temperature of the polymer composite material. The aluminum dross also affected to form the crystallinity at $117-122^{\circ}C$ and directly increased the rigid property of the composite materials. The microstructure examination revealed that the aluminum dross was located in a polymer matrix and affected to increase the dark colour of the polymer composite material.

• 한국세라믹학회지
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• 제34권6호
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• pp.591-600
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• 1997

Al2O3/Al composites were produced by displacement reaction method, which was carried out by immersing the sintered silica preform, which was prepared from fused silica powder, in molten aluminum. Because the molten aluminum did not penetrate into the silica preform with higher than 20% of porosity when the displacement reaction was accomplished at 100$0^{\circ}C$ for 10 hours in air atmosphere, the optimum range of sintering temperature of silica preform was from 135$0^{\circ}C$ to 140$0^{\circ}C$. The microstructure of this Al2O3/Al composites showed three-dimentionally co-continuous alumina, which provides wear resistance and high stiffness, and aluminium which acts as a toughnening phase. The grain size of the alumina in composites did not change with the particle size of the silica preform. The exact shape of the preform was retained and a net-shaped composite was produced. The representative Al2O3/Al composite prepared in this study showed 3.30mg/㎤ of bulk density, 350-430 MPa of flexural strength, 7.0 MPa.m1/2 of fracture toughness, and good machinability.

• 한국철도학회:학술대회논문집
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• 한국철도학회 2008년도 춘계학술대회 논문집
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• pp.980-985
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• 2008

Since its invention at TWI in 1991, Friction Stir Welding (FSW) has become a major joining process in the aerospace, railway and ship building industries especially in the fabrication of aluminium alloys. In an attempt to optimize the friction stir welding process of Al alloys for extrusion Aluminium carbody of HEMU-400X (Extrusion Aluminum 6xxx series), effects of joining parameters such as tool rotating speed, plunging depth and dwelling time on the weld joints properties were evaluated. Experimental tests were carried out for butt joined Al plates. A wide range of joining conditions could be applied to join Al alloys for Extrusion Aluminum 6xxx series without defects in the weld zone except for certain welding conditions with an insufficient heat input. The microstructures of welds have dynamic-recrystallized grain similar to stir zone in FSW weld. For sound joints without defects, at the rotation speed of 700 rpm with different welding speeds, the tensile strengths of the Stir Zone(SZ) were almost the same, 80% of those of the base metal. (JIS Z 2201)