• Title/Summary/Keyword: 함침공정

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Comparison of Resin Impregnation and Mechanical Properties of Composites Based on Fiber Plasma Treatment (섬유 플라즈마 처리에 따른 복합재료의 수지 함침성 및 기계적 특성 비교)

  • Seong Baek Yang;Donghyeon Lee;Yongseok Lee;Dong-Jun Kwon
    • Composites Research
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    • v.36 no.6
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    • pp.388-394
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    • 2023
  • In composites manufacturing, increasing resin impregnation is a key way to speed up the manufacturing process and improve product quality. While resin improvement is important, simple fiber surface treatments can also improve resin flowability. In this study, different plasma treatment times were applied to carbon fiber fabrics to improve the impregnation between resin and fiber. Electrical resistivity measurements were used to evaluate the dispersion of resin in the fibers, which changed with plasma treatment. The effect of fiber surface treatment on resin spreadability could be observed in real time. When inserting a carbon fiber tow into the resin, the amount of resin that soaked into the tow was measured to objectively compare resin impregnation. Five minutes of plasma treatment improved the tensile and compressive strength of the composite by more than 50%, while reducing the void content and increasing the fire point impregnation flow rate. Finally, a dynamic flexural fatigue test was conducted using a portion of the composite used as an architectural composite part, and the composite part did not fail after one million cycles of a 3 kN load.

The Influence of Fabrication Parameters on the Porosity Formation during Squeeze Infiltration Process (가압함침공정 중 기공 형성에 대한 제조 변수의 영향)

  • 서영호;이형국
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2001.05a
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    • pp.184-188
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    • 2001
  • The squeeze infiltration process is potentially of considerable industrial importance. The performance enhancements resulting from incorporation of short alumina fiber into aluminum are well documented. These are particularly significant for certain automobile components. But the solidification process gets complicated with manufacturing parameters and factors for porosity formation do not fully understand yet. In this study porosity defects were observed under several infiltrating conditions ; a kind of matrix, an initial temperature of melt, and a volume fraction of reinforcement. The desimetry and the microscopic image analysis were done to measure the amount of porosity. A correlation between manufacturing parameters and defects was investigated through these.

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Enhancement of Penetration by Using Mechenical Micro Needle in Textile Strain Sensor (텍스타일 스트레인 센서에 마이크로 니들을 이용한 전도성입자 침투력 향상)

  • Hayeong Yun;Wonjin Kim;Jooyong Kim
    • Science of Emotion and Sensibility
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    • v.25 no.4
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    • pp.45-52
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    • 2022
  • Recently, interest in and demand for sensors that recognize physical activity and their products are increasing. In particular, the development of wearable materials that are flexible, stretchable, and able to detect the user's biological signals is drawing attention. In this study, an experiment was conducted to improve the dip-coating efficiency of a single-walled carbon nanotube dispersion solution after fine holes were made in a hydrophobic material with a micro needle. In this study, dip-coating was performed with a material that was not penetrated, and comparative analysis was performed. The electrical conductivity of the sensor was measured when the sensor was stretched using a strain universal testing machine (Dacell Co. Ltd., Seoul, Korea) and a multimeter (Keysight Technologies, Santa Rosa, CA, USA) was used to measure resistance. It was found that the electrical conductivity of a sensor that was subjected to needling was at least 16 times better than that of a sensor that was not. In addition, the gauge factor was excellent, relative to the initial resistance of the sensor, so good performance as a sensor could be confirmed. Here, the dip-coating efficiency of hydrophobic materials, which have superior physical properties to hydrophilic materials but are not suitable due to their high surface tension, can be adopted to more effectively detect body movements and manufacture sensors with excellent durability and usability.

A Study on the Resin Flow through Fibrous Preform in Resin Transfer Molding Process (수지이동 성형공정에서 섬유직조내의 수지유동에 관한 연구)

  • 김성우
    • The Korean Journal of Rheology
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    • v.5 no.1
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    • pp.85-92
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    • 1993
  • 수지이동 성형공정에서 수지가 섬유직조망에 함침될 때의 투과계수와 수지의 표면 장력으로 인하여 유동진전면에서 발생하는 모세관압을 실험적으로 측정하였다. 두 종류의 섬유조직망에 대해서 가공율이 증가함에 따라투과계수는 증가한다. 수지, 섬유 그리고 공기 가 서로 다른 세 개의 상을 구성함으로써 수지의 표면장력의 영향을 받는 비정상상태의 투 과계수가 수지의 섬유직조망에 포화된 정상상태에서 측정된 투과계수보다 본 실험에서 수행 된 모든 기공을 범위에서 크다는 것을 보여주었다. 수지 유동진전면에서 발생되는 모세관압 은 기공율이 감소함에 따라 증가하였고 섬유직 조망의 기공율이 0.469인 경우에는 금형입구 에서의 수지주입압력의 25%에 해당되는 모세관압이 발생되는 것으로 나타났다. 따라서 모 세관압을 가공조건으로 고려해다 한다는 것을 제시할수 있었다. 또한 본연구에서 사용된 임 의 배향 섬유직조망에 대해 실리콘 오일과 유리섬유 계면의 동적접촉각 측정을 통하여 섬유 배향 및 기공의 분포를 나타내는 형상인자의 값을 구함으로써 실제 RTM 공정에서 발생되 는 모세관압을 예측할 수 dLT는 기초자료를 제시하였다.

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A Study On the Separation of Carbon Dioxide Using IS Membranes (용융염 무기막을 이용한 이산화탄소의 분리에 관한 연구)

  • 한건우;김태정;이건홍
    • Proceedings of the Membrane Society of Korea Conference
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    • 1994.10a
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    • pp.26-27
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    • 1994
  • 이산화탄소는 지구 온난화를 일으키는 대표적인 온실 기체로 알려져 왔으며 이에 따라 고온의 배가스에서 이산화탄소를 효율적으로 분리해 낼수 있는 기술이 국가 산업적 필요성을 갖게 되었다. 막을 이용한 기체 분리 기술은 낮은 가격, 비교적 간단한 공정상의 잇점 등 때문에 많은 관심을 끌고 있는 분리 기술이며, 특히 무기막은 열적, 화학적 안정성 등의 장점으로 인해 혹독한 조건에의 응용이 가능하다. 본 연구에서는 다공성 지지체에 염을 함침시킨 무기막(Immmobilized Salt Membrane)을 제조하여 기체 분리 특성을 조사하였다.

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Manufacture of Continuous Glass Fiber Reinforced Polylactic Acid (PLA) Composite and Its Properties (연속 유리섬유 강화 폴리유산 복합재료의 제조 및 물성)

  • Roh, Jeong U;Lee, Woo Il
    • Composites Research
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    • v.26 no.4
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    • pp.230-234
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    • 2013
  • The continuous glass fiber reinforced poly-lactic acid (PLA) composite was manufactured by direct melt impregnation. The mechanical and thermal properties of continuous glass fiber reinforced PLA composite were observed. Measured properties were compared with the reference values of neat PLA and the injection molded glass fiber/ PLA composite. The continuous glass fiber reinforced PLA composite having a fiber volume fraction of 27.7% shows enhanced tensile strength of 331.1 MPa, flexural strength of 528.6 MPa, and flexural modulus of 24.0 GPa. The enhanced heat deflection temperature (HDT) and the increased cystallinity were also observed. The degree of impregnation as a function of pulling speed was also assessed. The degree of impregnation at the pulling speed of 5 m/min was over 90% in this research.

Preparation of Polypropylene Grafted Polystyrene Sulfonic Acid Membranes for DMFCs in Supercritical CO2 (초임계 이산화탄소 함침을 이용한 연료전지용 폴리스타이렌/폴리프로필렌 복합막의 제조)

  • Byun, Jungyeon;Sauk, Junho;Synn, Wookyun;Kim, Hwayong
    • Clean Technology
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    • v.11 no.3
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    • pp.141-146
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    • 2005
  • The composite membranes were made by grafting using supercritical carbon dioxide (scCO2) impregnation and polymerization procedures. The membranes were synthesized by changing amount of monomer. The polypropylene grafted polystyrene sulfonic acid (PP-g-pssa) membranes were characterized with various methods. The morphology and structure of PP-g-pssa membranes were analyzed with scanning electron microscopy (SEM) and energy dispersive spectrometer (EDS). As amount of monomer was increased, ion conductivity, cell performance was increased and methanol permeability was decreased. However PP-g-pssa membranes with 1.5g monomer and over had similar values of methanol permeability, ion conductivity and cell performance.

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CO2 Absorption by Alkali-modified Amino Acid Salts (알칼리금속을 함침시킨 아미노산 염 수용액의 이산화탄소 흡수특성 연구)

  • Lim, Yun-Hui;Jo, Young-Min;Park, Joon-Seok
    • Applied Chemistry for Engineering
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    • v.22 no.5
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    • pp.526-531
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    • 2011
  • The present study attempted to impregnate alkali metals to amino acid in order to improve $CO_2$ absorption capacity. A used amino acid was glycine, of which pH increased up to about 11 with the addition of alkalies. $CO_2$ absorption capacity of amino acid salts was evaluated in a batch and a continuous process. The absorption capacity appeared in turns as; Sodium Glycinate ${\geq}$ Lithium Glycinate > Potassium Glycinate. Amino acid salts showed lower absolute capacity of $CO_2$ absorption than primary amine (Monoethanolamine) at $20^{\circ}C$. In a continuous absorption with 10% $CO_2$ flow, the increasing the reaction temperature, the increasing rate of absorption for amino and was higher that of than amino absorbent.

Kinetic Study of Copper Hydrotalcite Catalyst in Methanol Steam Reforming (메탄올 수증기 개질반응에서 구리가 함침된 하이드로탈사이트 촉매를 이용한 키네틱 연구)

  • Lee, Jae-hyeok;Jang, Seung Soo;Ahn, Ho-Geun
    • Journal of the Korean Institute of Gas
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    • v.26 no.5
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    • pp.16-21
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    • 2022
  • The reaction rate of a catalyst for producing hydrogen using the methanol steam reforming reaction was studied. It was prepared by impregnating copper, which is often used in methanol synthesis, as the main active metal, using hydrotalcite, which has excellent porosity and thermal stability, high specific surface area, weak Lewis acid point, and basicity, as a support. Activation energy and Pre-exponential factors were identified. In this study, the activation energy of the hydrotalcite catalyst impregnated with 20 wt% copper was calculated to be 97.4 kJ/mol and the Pre-exponential was 5.904 × 1010. Process simulation was performed using the calculated values and showed a similar tendency to the experimental results.