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Analysis of the O-Ring Deformation Behavior by the Computed Tomography (전산화 단층촬영에 의한 오링 변형 거동 분석)

  • Kim, Dong-Ryun;Kim, Jae-Hoon;Park, Sung-Han;Lee, Hwan-Gyu
    • Journal of the Korean Society for Nondestructive Testing
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    • v.28 no.1
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    • pp.1-8
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    • 2008
  • The object of this study is to develop the examination technique for measuring the O-ring deformation behavior under the pressure and the squeezed condition simultaneously. The O-ring deformation measuring device in which two grooves were dug to insert the two O-rings was manufactured to be not deformed under the high pressure and the 1 mm and 0.1 mm gap were designed to measure the extrusion lengths under the internal pressure. The beam hardening correction, the histogram analysis and the dead zone correction were executed to exactly measure the shape of O-ring deformation and the lengths of the O-ring deformation were measured by the LSF and the ERF. The computed tomography applied the pressure of 0, 1.378, 4.902, 9.804, 15.692 MPa at 22.3% squeezed condition and the expanded diameter, contact length and extrusion depth were measured in each pressure. The shape of O-ring deformation was evaluated by the FEM to verify the results of measuring by the computed tomography and the area of O-ring was mutually compared to the area measured by the computed tomography.

Particle Attrition Characteristics in a Bubbling Fluidized Bed Under High Temperature and High Pressure Conditions (고온 고압 조건하의 기포유동층 반응기에서의 입자 마모특성)

  • Moon, Jong-Ho;Lee, Dong-Ho;Ryu, Ho-Jung;Park, Young Cheol;Lee, Jong-Seop;Min, Byoung-Moo;Jin, Gyoung Tae
    • Clean Technology
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    • v.20 no.4
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    • pp.359-366
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    • 2014
  • Attrition characteristics of PKM1-SU particles, $CO_2$ absorbents for pre-combustion $CO_2$ capture process, and FCC particles, catalytic particles for hydro cracking of crude oil, were investigated at high temperature and high pressure conditions. Particle attrition tests were executed at various kinds of temperature ($0-400^{\circ}C$) and pressure (0-20 bar) conditions in a cylinder type bubbling fluidized bed with 15.1 cm diameter, 120 cm height and 1 mm orifice-sparger tube. Attrited particles before and after tests were analyzed by BET, optical microscopy, and particle size analyzer. Effects of bed material height (solid inventory) and steam injection were also verified by using ASTM D5757-95, conventional attrition test method.

AFM을 이용한 나노급 $Ge_2Sb_2Te_5$의 전기적 특성

  • Bae, Byeong-Ju;Hong, Seong-Hun;Jo, Jung-Yeon;O, Sang-Cheol;Hwang, Jae-Yeon;Lee, Heon
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.05a
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    • pp.21.1-21.1
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    • 2009
  • 상변화 메모리는 비휘발성 메모리이면서 빠른 동작 속도, 낮은 동작 전압 등 다양한 장점을 지니고 있어 차세대 메모리로 주목 받고 있다. 최근 상변화 메모리의 동작 전류를 감소시키기 위해 상변화 물질 및 전극 물질에 대한 연구를 진행하고 있으며, 소자의 크기를 최소화 하기 위한 연구가 진행되고 있다. 본 연구에서는 나노 임프린트 리소그래피와 전도성 AFM을 이용하여 나노급 상변화 물질의 특성을 평가하였다. 나노급 상변화 물질을 형성하기 위해 열경화성 나노 임프린트 리소그래피를 이용하여 $Ge_2Sb_2Te_5$(GST)/Mo/SiO2 기판 위에 200nm급 홀 패턴을 형성하였다. 홀 패턴에 Cr을 증착하여 리프트 오프 한 뒤 Cr을 하드 마스크로 사용하여 GST를 식각하였다. 그 결과, Mo 하부 전극 위에200nm 지름과 100nm 높이를 가지는 GST 나노 기둥을 형성하였다. GST 나노 기둥의 전기적 특성 평가를 위해 저항 측정 장비 및 펄스 발생기와AFM을 사용하였다. AFM은 접촉 모드로 설정하였으며, Pt가 코팅된 AFM tip을 사용하여 Cr 하드 마스크와 함께 상부 전극으로 사용하였다. GST 나노 기둥을 초기화 시키기 위해 I-V sweep을 하였으며, 그 결과 $1M\Omega$에서 $10\;k\Omega$으로 저항이 변화함을 확인하였다. GST 나노 기둥은 2V, 5ns의 리셋 펄스에서 비정질로 변화하였으며, 1.3V, 150ns의 셋 펄스에서 결정질로 변화하였다. 이 동작 전압으로 5번의 스위칭 특성을 평가하였으며, 이 결과는 소자 형태의 200nm 급GST의 특성과 유사하여 나노급 상변화 물질을 테스트하는 새로운 방법으로 사용될 수 있을 것이다.

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Shearing Characteristics of Aluminium Rods Using Plane Strain - Shear Box Test and Close Range Photogrammetric Technique (평면변형률 전단시험과 근거리 사진계측기법을 통한 알루미늄 봉의 전단특성)

  • Lee, Yong-Joo;Song, Ki-Jung
    • Journal of the Korean Geotechnical Society
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    • v.26 no.8
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    • pp.5-14
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    • 2010
  • To simulate two-dimensional plane-strain conditions in the laboratory model test, the side frictional resistance between the soil and thick glass or plastic sheet of the soil container should be reduced as much as possible. However, in fact this side friction cannot be removed completely. In this paper, the ground model simulated as a multi-sized aluminium rod mixture was introduced to get rid of the side frictional resistance and applied to the laboratory shear box test. In addition, an application of the close range photogrammetric technique to the shear box test was validated. As a result, it was found that a mean value of dilation angle from the close range photogrammetry was close to the dilation angle defined by the curve of shear strain vs. volumetric strain.

Development of LSM-Coated Crofer Mesh for Current Collectors in Solid Oxide Fuel Cells (LSM이 코팅된 고체산화물 연료전지용 Crofer Mesh 집전체 개발)

  • Baek, Joo-Yul;Park, Seok-Joo;Lee, Seung-Bok;Lee, Jong-Won;Lim, Tak-Hyoung;Song, Rak-Hyun;Kim, Kwang-Bum;Shin, Dong-Ryul
    • Journal of the Korean Electrochemical Society
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    • v.13 no.4
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    • pp.256-263
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    • 2010
  • A Crofer 22 APU mesh coated with a conductive ceramic material was developed as an alternative cathode current collector to Ag-based materials for solid oxide fuel cells. $(La_{0.80}Sr_{0.20})_{0.98}MnO_3$ (LSM) layer was deposited onto the Crofer mesh using a spray-coating technique, in an attempt to mitigate the degradation of electrical properties due to surface oxidation at high temperatures. The oxidation experiments at $800^{\circ}C$ in air indicated that the areaspecific resistance (ASR) of the LSM-coated Crofer mesh was strongly dependent on the wire diameter and the contact morphology between mesh and cell. In addition, the post-heat-treatment in $H_2/N_2$ resulted in a reduced thickness of Cr-containing oxide scales at the interface between Crofer mesh and LSM layer, leading to a decreased ASR.

Thermal Conductivity Measurement of Rock Cores from Ulleung Island Using PEDB System at Room Temperature (상온 환경에서 PEDB를 이용한 울릉도 시추코어의 열전도도 예비 측정)

  • Lee, Sang Kyu;Lee, Tae Jong
    • Geophysics and Geophysical Exploration
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    • v.19 no.3
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    • pp.121-130
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    • 2016
  • Several factors are discussed that should be considered in measuring thermal conductivity of rock cores with a PEDB (potable electronic divided bar) system, which is relatively accurate and easy to operate, and can measure the thermal conductivity of rock cores for various diameters. Then the system is applied to measure thermal conductivity of 70 rock cores from Ulleung Island. Air temperature affects most on the thermal conductivity measurements, so that it is very important to minimize the temperature change during the measurement. Other factors such as the temperature of heat source, averaging time window on the thermal conductivity measurements do not affect much compared to air temperature. Slightly higher thermal conductivity is measured when using the thermal contact paste between the sample and heat source or heat sink. Especially, rock cores with irregular surface showed bigger difference. Repeatability showed less than ${\pm}0.3%$ for standard samples and less than ${\pm}4%$ for rock samples, respectively, when the room temperature changes within $1^{\circ}C$ during the measurements. Thermal conductivity of the rock cores from Ulleung Island roughly increases as depth increases but does not show any dependency on the rock types.

Effect of Total Resistance of Electrochemical Cell on Electrochemical Impedance of Reinforced Concrete Using a Three-Electrode System (3전극방식을 활용한 철근 콘크리트의 교류임피던스 측정 시 전기화학 셀저항의 영향)

  • Khan, Md. Al-Masrur;Kim, Je-Kyoung;Yee, Jurng-Jae;Kee, Seong-Hoon
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.26 no.6
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    • pp.82-92
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    • 2022
  • This study aims to investigate the effect of total electrochemical cell resistance (TECR) on electrochemical impedance (EI) measurements of reinforced concrete (RC) by electrochemical impedance spectroscopy (EIS) using a three-electrode system. A series of experimental study is performed to measure electrochemical behavior of a steel bar embedded in a concrete cube specimen, with a side length of 200 mm, in various experimental conditions. Main variables include concrete dry conditions, coupling resistance between sensing electrodes and concrete surface, and area of the counter electrode. It is demonstrated that EI values remains stable when the compliant voltage of a measuring device is sufficiently great compared to the potential drop caused by TECR of concrete specimens. It is confirmed that the effect of the coupling resistance of TECR is far more influential than other two factors (concrete dry conditions and area of the counter electrode). The results in this study can be used as a fundamental basis for development of a surface-mount sensor for corrosion monitoring of reinforced concrete structures exposed to wet-and-dry cycles under marine environment.

A Study on the adequate Aggregate Selection of the Exposed Aggregate PCC Pavements (골재노출 콘크리트포장의 적정 골재 선정에 대한 연구)

  • Kim, Young-Kyu;Chae, Sung-Wook;Lee, Seung-Woo;Yoo, Tae-Seok
    • International Journal of Highway Engineering
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    • v.9 no.4
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    • pp.117-127
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    • 2007
  • The exposed aggregate PCC(EAP) pavements have been successfully used in Europe and Japan as low-noise pavements. Coarse aggregate are exposed on the pavement surface texture of EAP by removing mortar of surface. The pavement surface texture should maintain not only low-noise characteristic but also adequate skid resistance level during the performance period. Skid resistance decreased with wearing and polishing of tire and pavement surface due to the repetition of tire-pavement contact. Since the tires mainly contact the exposed coarse aggregate, the shape and rock type of coarse aggregate significantly influence wearing and polishing of EAP pavements. The test for resistance to abrasion coarse aggregate by use of the Los Angeles machine(KS F 2508) and the method of test for resistance to abrasion coarse aggregate by use of the Accelerated Polishing Machine(ASTM D 3319-90) are generally used to evaluate polishing characteristics of aggregate. In this study, polishing of coarse aggregate of different five rock types were evaluated by KS F 2508(LA abrasion test) and ASTM D 3319-90(PSV method). The results of LA abrasion test and PSV method were contrary to each other. Since LA abrasion test is estimated the quantity of abrasion by the impact of aggregate, it may not be adequate to evaluate the polishing of aggregate by the repetition of tire. In the case of PSV method, the resistance of polishing is estimated the skid resistance variation of polished aggregate after repetition of tire. The PSV method is adequate for the evaluation on polishing of coarse aggregate. From the test results of PSV method, it was founded that rock type, specific gravity, coarse aggregate angularity, flat or elongated particles in coarse aggregate are significant to the resistance characteristic of coarse aggregate.

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Effect of Nd:YAG Laser Irradiation to Mental Region for Sensory Nerve Conduction Change (하악 이공부에 조사된 Nd:YAG 레이저가 감각신경전도변화에 미치는 영향)

  • Jeon, Jae-Woo;Kim, Kyoung-Hee;Ko, Myong-Yun;Ahn, Yong-Woo;Park, Jun-Sang
    • Journal of Oral Medicine and Pain
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    • v.30 no.4
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    • pp.447-455
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    • 2005
  • The purpose of this study was to examine the effect of Nd:YAG laser irradiation for sensory nerve conduction change. Nd:YAG laser was irradiated to mental region for 5 minutes with the parameters that 10 Hz and 20 Hz of 100 mJ/pulse. Target size of irradiation was 30 mm diameter of circle and target-tip distance was about 10 mm. Therefore, the power density were 212 $mW/cm^2$ and 424 $mW/cm^2$. Sensory nerve conduction was evaluated with $Neurometer^{\circled}$ CPT/C before and after Nd:YAG laser irradiation. As an outcomes, the current perception threshold(CPT) and pain tolerance threshold(PTT) were obtained. We made a comparison of these two values and the results were as follows. 1. There was no significant difference in CPT at 1W, 10 Hz and 2 W, 20 Hz Nd:YAG laser irradiation. 2. There was no significant difference in PTT at 10 Hz, 20 Hz of 100 mJ/pulse Nd:YAG laser. 3. There were no significant differences in CPT and PTT between 1 W, 10 Hz group and 2 W, 20 Hz group. Therefore, We can make a conclusion that Nd:YAG laser irradiation to mental region have no effect on mental nerve conduction in our study model.

The Production of Chitosanoligosaccharides Using Chitosan Bead (기질의 담체화를 이용한 키토산올리고당의 생산)

  • 김승모
    • KSBB Journal
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    • v.15 no.4
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    • pp.352-358
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    • 2000
  • Preparation for the simplified separation of chitosandoligosaccharides from enzymatic hydrolysate was investigated. Two different types of chitosan beads as substrate were prepared as organic-based bead by W/O emulsion method and water-based bead by alkaline treatement. The average size of organic-based bead was $200{\mu}m$, and that of water based beads were $4000{\mu}m$, $100{\mu}m$, $30{\mu}m$, in diameter respectively. Enzyme stability was maintained over 80% at PH 6 after 24 hours. The optimal condition for the production of chitosanoligosaccharides was at pH 6.0, $50^{\circ}C$ and 40U (200U/g-chitosan) According to final oligosaccharide concentration water-based bed showed the similar result with that of organic-based bead even through it had smaller surface area attacked by chitosanse than that of organic-based bead. It is probable that the structure of water-based chitosan bead was looser than that of organic-based bead so enzyme penetrated easily into the bead structure. For the oligosaccharide production versus surface area the different size of water-based beads was investigated, Maxiaml production yield was observed in the $30{\mu}m$ beads. Consequently the water-based chitosan bead was better than the organic-based bead in this reaction system.

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