• The korean journal of orthodontics
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• v.40 no.3
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• pp.184-194
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• 2010

Objective: The purpose of this study was to investigate the effect of tribochemical silica coating on the shear bond strength (SBS) of rebonded ceramic brackets using nano-filled flowable composite resin. Methods: A total of 60 premolars were prepared and divided into 4 equal groups as follows: Tribochemical silica coating (TC) + Transbond XT (XT), TC + Transbond supreme LV (LV), Sandblast treatment (SA) + XT, SA + LV. Treated ceramic brackets were rebonded on the premolars using each adhesive. All samples were tested in shear mode on a universal testing machine. Results: SBS of silica coated groups were high enough for clinical usage (TCLV: 10.82 $\pm$ 1.82 MPa, TCXT: 11.50 $\pm$ 1.72 MPa). But, SBS of the sandblast treated groups had significantly lower values than the tribochemical silica coated groups (SALV, 1.23 $\pm$ 1.16 MPa; SAXT, 1.76 $\pm$ 1.39 MPa; p < 0.05). There was no difference between the shear bond strength by type of adhesive. In the silica coated groups, 77% of the samples showed bonding failure in the adhesive. In the sandblast treated group, all bonding failures occurred at the bracket-adhesive interface. Conclusions: The result of this study suggest that newly introduced nano-filled flowable composite resin and tribochemical silica coating application on debonded ceramic bracket bases can produce appropriate bond strengths for orthodontic bonding.

• The korean journal of orthodontics
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• v.28 no.4 s.69
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• pp.641-657
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• 1998

This study was undertaken to compare the bond strength and the fracture site of new and recycled brackets according to the base design. 252 sound premolars extracted for orthodontic treatment were collected and Type I, Type II, Type III brackets were divided into four groups by recycling method Each bracket was then bonded to an extracted premolar. Instron Universal Testing Machine(model W) was used to measure the shear bond strength, and the surface of the recycled brackets were viewed in SEM For the analysis of the results, one way ANOVA and Scheffe's multiple range test was executed using the SPSSWIN program. 1. The shear bond strength showed statistically significant difference according to the bracket base design(p<0.001). Type III bracket(round indentation base, micro-etched) showed the highest bond strength, Type I bracket(foil-mesh base) was second, and Type II bracket(grooved integral base, micro-etched) was last. 2. The effect of recycling on the bond strength was different according to bracket type. The shear bond strength of Type I, Type II brackets showed the smallist reduction when treated for 1 minute in Big Jane(p<0.05), but the shear bond strength of Type III brackets showed no statistically significant difference according to recycling method(p>0.05). 3. In Type I, Type II brackets, frequent fracture site was bracket-resin interface, but in Type III brackets, about half of the resin was retained on the tooth surface frequently. 4. The shear bond strength was highest when about half of the resin was retained on the tooth surface(p<0.05). 5. The resin remnant on the bracket base after recycling had no effect on the shear bond strength.

• Restorative Dentistry and Endodontics
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• v.32 no.5
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• pp.426-436
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• 2007

The objective of this study is to evaluate the effect of an additional application of bonding resin on the bond strength of resin luting cements in both the light-cure (LC) and self-cure (SC) modes by means of the ${\mu}TBS$ tests. Three combinations of One-Step Plus with Choice, Single Bond with Rely X ARC, and One-Up Bond F with Bistite II were used. D/E resin and Pre-Bond resin were used for the additional application. Twelve experimental groups were made. Three mandibular $3^{rd}$ molars were used in each group. Indirect composite blocks were cemented on the tooth surface. $1\;{\times}\;1\;mm^2$ dentin-composite beam for ${\mu}TBS$ testing were made and tested. When total-etching dentin adhesives were used, an additional application of the bonding resin increased the bond strength (P < 0.05). However, this additional application didn't influence the bond strength of self-etching dentin adhesives (P > 0.05). In conclusion, the results suggest that an additional application of the bonding resin increases bond strength and enhances quality of bonding when using total-etching dentin adhesives.

• Proceedings of the Korean Society of Dyers and Finishers Conference
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• 2011.03a
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• pp.60-60
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• 2011

막구조는 근래에 와서 대공간 구조 및 지붕구조에 가장 보편적으로 사용되는 경량 인장 구조물로 각광받고 있다. 구조용 막재는 풍하중 및 설하중에 충분히 감당할 수 있도록 강도와 내구성을 가지고 있어야 한다. 일반적으로 막구조 재는 PVC코팅 폴리에스터막, 실리콘코팅 유리섬유막, PTFE코팅 유리섬유막이 있다. 제직되는 원단의 크기가 한정되어 있기 때문에 재단 후 접착하여 제작한다. 이 때문에 이음부분이 나 재단부분에 코팅으로 인한 접착이 어려워 고온고압으로 접착을 한다. 이 연구에서는 실리콘코팅 유리섬유막의 접착시 어려움을 보완하기 위해 저온 Plasma를 이용한 처리법으로 방전에 의해 Plasma를 발생시켜 50w, 100w 출력으로 10분, 20분간 처리하여 그 결과를 접촉각과 SEM 관찰을 통해 표면처리를 관찰하였다. Plasma 처리로 인해 실리콘 표면층에 균열이 발생하고 표면이 갈라짐을 확인할 수 있었다. 접촉각측정 결과 Plasma 출력과 시간의 증가함에 따라 접촉각은 감소하였다. 실리콘코팅 원단에 저온 Plasma 처리한 후 표면 특성을 분석하고 원단을 접착을 시켜 박리 강도를 측정함으로써 막구조 원단의 접착력 향상에 대한 연구를 진행하였다. KS K 0533 접착포의 박리 강도 시험방법으로 실리콘코팅 원단의 박리 강도를 측정한 결과 플라즈마 처리 원단이 플라즈마 미처리 원단보다 박리 강도가 향상된 것을 확인할 수 있었다. 저온 Plasma 처리 시간이 증가할수록 표면의 젖음성을 향상시켜 접촉각을 낮추었다. 이는 곧 표면에너지의 증가를 뜻하는 것으로 접착력을 증가시켜 실리콘코팅 원단의 접착성을 시킴으로써 강한 강도와 내구성을 갖춘 막구조물의 개발에 기대되고 있다.

• Proceedings of the Korea Concrete Institute Conference
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• 2008.04a
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• pp.609-612
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• 2008

Ultra Super Early Strength Cement is a material that satisfies these requirements. early hydration heat however, is significant over regular concrete, thus discretion is advised for thermal cracks in accordance with heat generation when constructing a large-scale structures. In addition, the negative point that it is difficult to achieve required strength in a short period of time following rubbing process while retaining workability, the cement is being used conditionally for engineering material and Ultra Super Early Strength Cement for maintenance material for construction doesn't exist. Magnesia Phosphate Cement, which is currently under studies in overseas uses no extra admixture and has strong points of Ultra Super Early Strength as well as favorable construction-ability and adhesive stability to the prototype concrete. These factors stem recognition that it could be used as maintenance material for construction of diverse applicability. In order to provide necessary data to increase practicality of the magnesia phosphate cement for Ultra Super Early Strength Mortar, the study carried out simulate experiment on member of framework to review field applicability.

• Journal of the Korea Institute of Building Construction
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• v.18 no.4
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• pp.329-335
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• 2018

The objective of this study is to develop a mortar mixture with high workability and adhesive strength for section jacketing in seismic strengthening technology of existing concrete structures. To achieve targeted requirements of the mortars (initial flow exceeding 200 mm, compressive strength of 30MPa, and adhesive strength exceeding 1MPa), step-by-step tests were conducted under the variation of the following mixture parameters: water-to-binder ratio, sand-to-binder ratio, polymer-to-binder ratio, dosage of viscosity agent, and content of ultra-rapid-hardening cement. The adhesive strength of the mortars was also estimated with respect to the various surface treatment states of existing concrete. Based on the test results, the mortar mixture with the polymer-to-binder ratio of 10% and the content of ultra-rapid-hardening cement of 5% can be recommended for the section jacketing materials. The recommended mortar mixture satisfied the targeted requirements as follows: initial flow of 220 mm, high-early strength gain, 28-day compressive strength of 35MPa, and adhesive strength exceeding 1.2MPa.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.37 no.8
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• pp.751-758
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• 2009

Failure strengths of composite single-lap adhesive joints were investigated with various parameters such as manufacturing method, overlap length and adherend thickness. A total of 335 single-lap joint specimens were tested under tension. Specimens were fabricated with 4 different manufacturing processes; cocuring without and with adhesive, secondary bonding and co-bonding. Each manufacturing process has 5 different overlap lengths and 4 different thicknesses, respectively. As expected, failure strength is higher in thicker adherend joints and lower in larger overlap length specimens. Interesting result is that the secondary bonded joints show the higher strength than the cobonded and cocured joints with adhesive, and give close or even higher strength compared with non-adhesive cocured case.

• Restorative Dentistry and Endodontics
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• v.36 no.1
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• pp.50-58
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• 2011

Objectives: The purpose of this study was to compare the microshear bond strength (uSBS) of two totaletch and four self-etch adhesive systems and a flowable resin to enamel. Materials and Methods: Enamels of sixty human molars were used. They were divided into one of six equal groups (n = 10) by adhesives used; OS group (One-Step Plus), SB group (Single Bond), CE group (Clearfil SE Bond), TY group (Tyrian SPE/One-Step Plus), AP group (Adper Prompt L-Pop) and GB group (G-Bond). After enamel surfaces were treated with six adhesive systems, a flowable composite resin (Filek Z 350) was bonded to enamel surface using Tygon tubes. the bonded specimens were subjected to uSBS testing and the failure modes of each group were observed under FE-SEM. Results: 1. The uSBS of SB group was statistically higher than that of all other groups, and the uSBS of OS, SE and AP group was statistically higher than that of TY and GB group (p < 0.05). 2. The uSBS for TY group was statistically higher than that for GB group (p < 0.05). 3. Adhesive failures in TY and GB group and mixed failures in SB group and SE group were often analysed. One cohesive failure was observed in OS, SB, SE and AP group, respectively. Conclusions: Although adhesives using the same step were applied the enamel surface, the uSBS of a flowable resin to enamel was different.

• The korean journal of orthodontics
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• v.39 no.4
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• pp.234-247
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• 2009

Objective: The purpose of this study was to evaluate the shear bond strength of rebonded ceramic brackets according to each condition and find an appropriate method to rebond ceramic brackets with proper shear bond strength in clinical practice. Methods: The study consisted of 12 experimental groups, according to the types of brackets, debonding methods, and treatment methods of the bracket base. Shear bond strength was measured, and adhesive residues left on the tooth surface were assessed. The base of the bracket was examined under scanning electron microscopy. Results: The shear bond strength of the monocrystalline ceramic bracket group was significantly higher than thatof the polycrystalline bracket group with only sandblasting (p < 0.05). There was no significant difference in shear bond strength between groups that used rebonded brackets which were debonded with shear force and debonded with laser (p > 0.05). The shear bond strength of the sandblasted/silane group was significantly higher than that of the selectively grinded group with a low-speed round bur and the sandblasted only group (p < 0.001). The retentive structure was more presented in groups where laser was applied than in groups where shear force was applied to debond brackets prior to rebonding. The bracket bases which were treated before rebonding presented smoother surfaces than new brackets. Conclusions: Shear bond strength could be increased by applying a silane coupling agent after sandblasting before rebonding. Also, the bond strength of the selectively grinded group with a low-speed round bur and the sandblasted group showed acceptable bond strength for clinical orthodontic treatment.

• Journal of the korean academy of Pediatric Dentistry
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• v.35 no.3
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• pp.389-398
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• 2008

The purpose of this study was to evaluate the effects of collagenase and esterase on dentin bond strength and nanoleakage. Resin composites were bonded to occlusal dentin of premolars with Single Bond 2(SB) and Clearfil SE Bond(SE). After the microtensile specimens were prepared and stored in PBS for 24 hours(I) or, PBS(II), collagenase(III), esterase(IV) solution for 4 weeks, the specimens were stained with silver nitrate solution. Microtensile bond strength(${\mu}TBS$) and silver penetration area were measured and, the results were as follows: 1. For group II, III, and IV, the bond strengths of SB were lower than those of SB(p<0.05). The bond strengths of SB II, III, and IV were lower than that of SB I(p<0.05). There was no difference among the bond strengths of SE $I{\sim}IV$ groups(p>0.05). 2. Silver penetration areas of SB were higher than those of SE for all storage groups(p<0.05). In SB and SE groups, there was no significant difference of silver penetration area among $I{\sim}IV$ groups(p>0.05). 3. SE I, II, and III showed inverse relationship between the bond strengths and the silver penetration areas(p<0.05).