• Title/Summary/Keyword: 선재온도

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superconducting properties of Bi-2223 tapes with various heat treatment condition (열처리 온도 및 분위기 변화에 따른 Bi-2223 초전도 선재에서의 특성변화)

  • 하동우;이동훈;하홍수;오상수;김홍대;양주생;윤진국;최정규;권영길
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07a
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    • pp.527-530
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    • 2002
  • A lot of efforts have been focused on the optimization of PIT parameters for Bi-2223/Ag wire. In this paper, initial annealing of Bi-2223/Ag wire to transform Bi-2212 orthorhombic from Bi-2212 tetragonal Precursor was investigated. This initial annealing step at low oxygen partial pressure were to transform Bi-2212 orthorhombic structure and to reduce the formation of second phases at superconducting wire. However Bi-2223 Phases were appeared at higher annealing temperature. Critical currents(Je) of Bi-2223/Ag tapes were sintered at low oxygen Partial pressure were higher than that of the wires sintered at atmosphere condition. In order to investigate the effect of rolling reduction ratio, Bi-2223/Ag HTS tapes were rolled with different reduction ratio. There were no clear difference of Je and filaments shape with various rolling reduction ratio.

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Zr 신합금에서 열처리변수가 부식과 미세조직에 미치는 영향

  • 백종혁;김선재;김경호;최병권;정용환;김인섭
    • Proceedings of the Korean Nuclear Society Conference
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    • 1998.05b
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    • pp.142-147
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    • 1998
  • 핵연료피복관의 부식성능은 합금원소의 조성에 매우 민감하지만 열처리변수에 따라서도 크게 좌우되므로 열처리변수가 Zr 신합금의 부식저항성과 미세조직에 미치는 영향을 조사하였다. Zr-Nb-Sn-Fe-Cr 조성을 갖는 합금을 제조하여 열처리면수($\Sigma$A)를 7.7x$10^{-l9}$~5.3x$10^{-17}$ hr로 제어한 후 400 $^{\circ}C$/10.3 MPa 분위기의 autoclave를 이용하여 부식시험을 실시 하였다. 열처리변수($\Sigma$A)가 증가함에 따라서 부식저항성은 감소하였으며 열처리변수의 값이 7.7x$10^{-l9}$와 8.8x$10^{-l9}$ hr일 때 부식저항성은 매우 우수하였다. 천이후 부식속도에 미치는 열처리변수의 영향은 무게증가량에 미치는 영향과 동일한 경향을 나타냈으며 $\Sigma$A가 1.0x$10^{-18}$ hr이하에서 매우 낮은 부식속도를 보였다. 석출물 크기의 증가는 부식저항성을 감소시키는 것으로 관찰되었다. 따라서 우수한 부식저항성을 갖는 Zr 신합금을 개발하기 위해서는 중간 열처리 온도를 적절히 조절하여 석출물의 크기를 0.05 $\mu$m이하로 제어하여야 한다.다.

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Distribution Analysis of Local Critical Temperature and Current Density in YBCO Coated Conductors using Low-temperature Scanning Laser Microscopy (저온 주사 레이저 현미경(LTSLM)을 이용한 YBCO 초전도 선재의 국소적 임계 온도 및 전류 밀도 분포 분석)

  • Park, S.K.;Cho, B.R.;Ri, H.C.
    • Progress in Superconductivity
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    • v.12 no.1
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    • pp.17-22
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    • 2010
  • Distribution of local critical temperature and current density in $YBa_2Cu_3O_{7-\delta}$ (YBCO) coated conductors was analyzed using a Low-temperature Scanning Laser Microscopy (LTSLM). We prepared YBCO coated conductors of various bridge types to study the spatial distribution of critical temperature and current density in single and multi bridges. An LTSLM system was modified for a detailed two-dimensional scan without shifting of the sample. We observed a spatial distribution of the critical temperature from the bolometric response, which arises from a focused laser beam at the sample near the superconducting transition. Also we studied the relation between the critical temperature and the current density.

Distribution Analysis of the Local Critical Temperature and Current Density in YBCO Coated Conductors using Low-temperature Scanning Laser and Hall Probe Microscopy (저온 주사 레이저 및 홀소자 현미경을 이용한 YBCO 초전도 선재의 국소적 임계 온도 및 전류 밀도 분포 분석)

  • Park, S.K.;Cho, B.R.;Park, H.Y.;Ri, H.C.
    • Progress in Superconductivity
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    • v.13 no.1
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    • pp.28-33
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    • 2011
  • Distribution of the local critical temperature and current density in YBCO coated conductors were analyzed using Low-temperature Scanning Laser and Hall Probe Microscopy (LTSLHPM). We prepared YBCO coated conductors of various bridge types to study the spatial distribution of the critical temperature and the current density in single and multi bridges. LTSLHPM system was modified for detailed linescan or two-dimensional scan both scanning laser and scanning Hall probe method simultaneously. We analyzed the local critical temperature of single and multi bridges from series of several linescans of scanning laser microscopy. We also investigated local current density and hysteresis curve of single bridge from experimental results of scanning Hall probe microscopy.

The Precipitation of Second Phases by Annealing Heat Treatment in the $(Bi,Pb)_2$${Sr_2}{Ca_2}{Cu_3}{O_{10}}$ Superconductor System (BSCCO계 초전도체에서 서냉 열처리에 의한 2차상 석출)

  • 이상희;김철진;유재무
    • Journal of the Korean Ceramic Society
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    • v.37 no.12
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    • pp.1212-1220
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    • 2000
  • Bi-2223 초전도체계에서 석출물을 flux-pinning center로 이용할 수 있는지 가능성을 타진하기 위하여 $Bi_{1.8}$P $b_{0.4}$S $r_{2}$C $a_{2.2}$C $u_3$ $O_{8}$ 조성을 가진 Bi-2223/Ag 선재를 반응온도, 산소분압, 시간 등을 변화시키면서 열처리를 행하였다. 열처리 후 석출물들은 XRD, SEM, TEM, EDS로 분석하였다. Bi-2223 모상내의 (Ca, Sr)$_2$(Pb,Bi) $O_4$, B $i_{0.5}$ P $b_3$S $r_2$C $a_2$Cu $O_{12+}$$\delta$/ (3221)와 같은 2차상들의 크기와 분포는 2223 입자들의 연결성을 파괴하지 않고 열처리 조건에 의해서 조절할 수 있었다. 서냉 열처리가 된 시편은 임계전류밀도( $J_{c}$)값이 증가하였는데, 이는 2223 입자내 나노미터 크기로 형성된 석출물들이 flux-pinning sites로 작용한 것으로 추정된다.다.

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Critical Current Degradation Characteristics by Temperature Difference of L$N_2$-Normal in Repetitive Bending Strain of High Temperature Superconducting Tape (고온 초전도 선재의 굽힘횟수와 온도차에 의한 임계전류저하특성)

  • 김해준;김석환;송규정;김해종;배준한;조전욱;성기철
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 2003.10a
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    • pp.274-277
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    • 2003
  • Critical current(Ic) degradation of HTS tapes after bending is one of the hottest issues in HTS development and application studies. Many people are measuring Ic degradations for effect of bending radius. However even if the bending radius is larger than the breaking radius a HTS tapes can be damaged by repetitive bending, which is unavoidable in the winding processes. Therefore, We studied the Ic degradation after repetitive bending. at 77K with self-field, of Bi-2223 tapes processed by "Powder-in-Tube" technique, which was made by America Superconductor Corporation(AMSC) and superconductiing tapes that strain is imposed measured critical current by temperature difference of L$N_2$ and normal temperature. Like this, critical current could measure that degradation about 1~3% by temperature difference. These results will amount the most important basis data in power electric machine of superconductivity cable, magnet, etc that winding work is require.

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Field Loss Analysis and Cooling Analysis of HTS Synchronous Motor (고온초전도 동기모터의 계자손실 해석 및 냉각 해석)

  • Kim, Ki-Chan;Lee, Dae-Dong
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.19 no.3
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    • pp.69-74
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    • 2018
  • Large industrial motors require a large area because of the high risk of shutdown accidents and large industrial accidents due to the lowering of the dielectric strength of the armature windings and overheating problems. Therefore, there is a demand for a large-capacity motor that has small size, light weight, and excellent dielectric strength compared with conventional motors. Superconducting motors have advantages of high efficiency and output power, low size, low weight, and improved stability. This results from greatly increasing the magnetic field generation by using superconductive field coils in rotating machines such as generators and motors. It is very important to design and analyze the cooling system to lower the critical temperature of the wires to achieve superconducting performance. In this study, a field loss analysis and low-temperature heat transfer analysis of the cooling system were performed through the conceptual design of a 100-HP high-temperature superconducting synchronous motor. The field loss analysis shows that a uniform pore magnetic flux density appears when high-temperature superconducting wire is used. The low-temperature heat transfer analysis for gaseous neon and liquid neon showed that a flow rate of 1 kg/min of liquid neon is suitable for maintaining low-temperature stability of the high-temperature superconducting wire.

A STUDY CONCERNING THE CHARACTERISTICS OF KOREAN NI-TI ALLOY ORTHODONTIC WIRE (국산 Ni-Ti합금 교정용 선재의 특성에 관한 연구)

  • Park, Dong-Ok;Kwon, Oh-Won
    • The korean journal of orthodontics
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    • v.25 no.2 s.49
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    • pp.187-200
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    • 1995
  • To estimate the characteristics of Korean Ni-Ti alloy orthodontic wire, this study investigated compositions, tensile properties, bending properties, heat treatment effects, and ion releasing degrees, and compared these characteristics to those of the imported Ni-Ti alloy wire. The results obtained are as follows ; 1. Ti and -Ni elements in ORTHOLLOY were in a range showing superelasticity, and there was a little difference in the Ni and Ti contents of ORTHOLLOY as compared with those of SENTALLOY. 2. The results of the tensile test concerning ORTHOLLOY exhibited a superelastic effect, indicating an area of a definite amount of stress in spite of the changes in the range from $2\%\;to\;8\%$ in the strain rate. 3. ORTHOLLOY presented higher load values than SENTALLOY in the same deflection values when the wire was tested in three-point bending. A load range displaying a superelastic effect was 80-l00g, 140-l80g, and 130-200g respectively, in wire diameters of 0.014', 0.016', and 0.018' 4. By heat treatments at $400^{\circ}C$ and at $500^{\circ}C$, a load range showing the effect of superelasticitly was lessened by the duration of the heat treatment time. The superelastic effect was destroyed as a result of the 10 minutes heat treatment at $600^{\circ}C$. 5. The quantity of the Ni ion released from ORTHOLLOY, tended to be greater than the amount of released Ni ion in SENTALLOY. The Co ion released was very little(<0.01ppm) in SENTALLOY and ORTHOLLOY irrespective of the lapse of time. Released Ni ions on the 1st day were at the maximum, and the releasing rate showed plateaus after three days. 6. The surface morphology of SENTALLOY was relatively regular irrespective of the lapse of rime, and the corrosion tendency was not observed. However, the surface morphology of ORTHOLLOY was rather irregular and shelved fitting corrosion after immersion.

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An experimental study on diameter increase of orthodontic wire by electroplating (전기도금을 이용한 스테인레스 스틸 선재의 직경 증가에 관한 실험적 연구)

  • Cho, Jin-Hyoung;Sung, Young-Eun;Lee, Ki-Heon;Hwang, Hyeon-Shik
    • The korean journal of orthodontics
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    • v.33 no.2 s.97
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    • pp.121-130
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    • 2003
  • The purpose of this study was to evaluate the possibile clinical application of electroplating to increase diameter of an orthodontic wire, through examining the change of physical properties. The diameter of stainless steel orthodontic wire was increased from 0.016 inch to 0.018 inch by electroplating in a bath of nickel sulfate 100g/L, nickel chloride 60g/L, boric acid 30g/L, and sodium chloride 50g/L, under the conditions of 1.7V, $25\~29^{\circ}C\;and\;3.1\~3.3pH$. During the electroplating, the rate of diameter increase was measured every minute. To investigate uniformity, the diameter was measured at three different locations of each wire specimen aster electroplating. An X-ray diffraction test was performed to analyze the nature of the electroplated metal. Following heat treatment to improve adhesion between the wire and electroplated metal, a three-point bending test was conducted to compare stiffness, field strength, and ultimate strength among four wire groups; 0.016 inch, electroplated 016, electroplated and heat-treated 016, and 0.018 inch wires. Through the comparison of each wire group, following results were obtained. 1. In the load-deflection graph, the curve of the electroplated group was Placed between that of the 0.016 inch group and the 0.018 inch group, and the owe was closer to the 0.018 inch group by heat treatment. 2. In the electroplated and heat-treated 016 wire group, the values of stiffness, yield strength and ultimate strength showed higher tendency than in the original 0.016 Inch group. Stiffness and ultimate strength showed statistically significant differences between two groups. 3. Stiffness, yield strength, and ultimate strength of electroplated wire presented lower values than those of 0.018 inch wire group. 4. Stiffness, yield strength, and ultimate strength of electroplated and heat-treated wire showed higher tendency than those of electroplated wire group, and ultimate strength showed statistically significant difference between two groups. 5. After electroplating, the difference in diameter between the three locations was within $0.1\~0.3\%$ variation, and showed no statistical significance.

Effect of Freezing, Thawing and Blanching on the Pigment of Purple Sweet Potato (동결, 해동 및 Blanching이 자색고구마 색소에 미치는 영향)

  • Kim, Seon-Jae;Rhim, Jong-Whan
    • Korean Journal of Food Science and Technology
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    • v.29 no.1
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    • pp.9-14
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    • 1997
  • The effect of freezing, thawing and blanching on the change of extractable pigment content of purple sweet potato (PSP) was investigated. Freezing at $-5^{\circ}C$ was more effective than freezing at $-20^{\circ}C\;or\;-40^{\circ}C$, and rapid thawing methods such as microwave heating or hat air blast heating were effective than slow thawing methods such as thawing at $4^{\circ}C\;or\;20^{\circ}C$. Inactivation of enzymes, which cause pigment destruction during thawing, by blanching before freezing was necessary to obtain the highest possible amount of extractable pigment from PSP. Microwave blanching for $3{\sim}4$ min or hot air blanching for $10{\sim}15$ min were effective in extracting pigment from PSP.

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